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Sep funnels and vacuum?
Do separatory funnels generally withstand vacuum? I need to do some vacuum filtrations with larger v ...
13-6-2020 at 10:22
by: Refinery
How the L pills in WWII era were made?
I read some news article about someone finding a WWII era cyanide capsule and I began to wonder what ...
13-6-2020 at 09:54
by: Refinery
Thermometer and distillation
This is an amateur question, but:

When distilling for ex acetone, it boils at around 56 NTP, but ...
13-6-2020 at 07:33
by: Refinery
Anti bike theft agent
I see. I've heard that it smells "fishy". One of my friend hangs out with junkies so I suppose I sho ...
13-6-2020 at 05:23
by: Refinery
High precision analytical balance/scale 120g at .001g & 6kg at .01g resolution
[rquote=638183&tid=73852&author=Ubya]oh boi, you are comparing a kitchen balance to an analy ...
12-6-2020 at 09:37
by: Refinery
High precision analytical balance/scale 120g at .001g & 6kg at .01g resolution
I suppose you could calibrate the scale with weighting a known item, like coin (or a bulk of them) a ...
12-6-2020 at 08:23
by: Refinery
Anti bike theft agent
tert-Butyl Isocyanide it is, then.

If there is something that causes emergency evacuation of publ ...
11-6-2020 at 10:45
by: Refinery
Preparation of cyanides
My experience:

Theory

1mol urea (slight excess)
1mol NaOH
1mol C (slight excess)
= 1mol NaC ...
11-6-2020 at 10:32
by: Refinery
Soda lime glass workability?
I made tests and soda glass softens easily and is workable. Air cooling does not appear to cause cra ...
9-6-2020 at 10:38
by: Refinery
Hydrothermal reactor
[rquote=637886&tid=155547&author=wg48temp9]Stay safe:[/rquote]

Absolute terms, relative p ...
8-6-2020 at 06:20
by: Refinery
Hydrothermal reactor
If you have access to TIG welder it will solve all your problems. Get a thick walled SS tube, weld f ...
7-6-2020 at 23:03
by: Refinery
3D printing useful parts - anyone doing this? I'd like to print GL45 bottle caps if possible
[rquote=637795&tid=155539&author=draculic acid69]Pla and abs won't handle anything in a lab ...
7-6-2020 at 22:58
by: Refinery
Polypropylene funnel considerations
Polyethene and other same group stuff in general needs superacids to react. Polyethene handles sulfu ...
6-6-2020 at 10:00
by: Refinery
odorless heating baths?
[rquote=637414&tid=30302&author=Mateo_swe]Are you sure?[/rquote]

I used it again, so I'm ...
6-6-2020 at 06:45
by: Refinery
Crystals at bottom of ammonia?
When I made ammonia by bubbling U+NaOH+H2O reactants into cold water, I noticed a faint amount of wh ...
6-6-2020 at 06:32
by: Refinery
Polypropylene funnel considerations
Well there's that, too. I've got some parts that are contaminated by carbon, but it basically doesn' ...
5-6-2020 at 03:26
by: Refinery
Polypropylene funnel considerations
I haven't yet faced a chemical that eats polyethene at NTP, and not quite sure about polypropene eit ...
4-6-2020 at 23:01
by: Refinery
Silica gel mystery?
https://www.sciencedirect.com/topics/neuroscience/desiccants

This source cites that: "The moistur ...
4-6-2020 at 22:55
by: Refinery
Silica gel mystery?
What is the proper procedure to dry silica gel?

https://www.researchgate.net/post/How_to_extract_ ...
4-6-2020 at 11:12
by: Refinery
Vacuum Distillation of Aniline
I really must practice my vac distilling. I've had serious issues with bumping so far. I made a blee ...
3-6-2020 at 22:23
by: Refinery
Vacuum glass implosion?
I was wondering if anyone has ever had a glass implosion during vacuum process? People speak about t ...
3-6-2020 at 11:23
by: Refinery
How long can I store ethyl bromide in a mason jar at room temperature?
Place PE membrane between cap and glass rim. You can also use al foil on top of PE to reduce permeat ...
3-6-2020 at 04:36
by: Refinery
What requires a fume hood?
Certain reactions must be performed outside, you are right about that. The mere heat of carbothermic ...
3-6-2020 at 01:11
by: Refinery
What requires a fume hood?
I'm in need of a fume hood and I designed a concept already.

I make the table out of plywood with ...
3-6-2020 at 00:33
by: Refinery
Aquiring grinding material for a ball mill
Carburizing is certainly an useful option for example gun parts. (Open bolt) gun lifetime can be sig ...
3-6-2020 at 00:24
by: Refinery
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