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Would it be possible to make 2-bromobenzoyl chloride from salicylic acid
@chemi pharma,

Why do you think that reagent pair will form the acyl halide? I only see an exampl ...
26-12-2018 at 12:19
by: Loptr
Free fume hoods in NC
Looking into it. Thank you.
26-12-2018 at 08:28
by: Loptr
synthesis of 2-bromobenzoyl chloride
[rquote=564628&tid=114013&author=jmister28]I am using the 2-bromobenzoyl chloride in a react ...
20-12-2018 at 13:58
by: Loptr
Under what conditions do alkyl azides rearrange to imines?
What bothers me about this is how weak of an acid HN3 is. How would it easily add to an alkene?
20-12-2018 at 13:44
by: Loptr
Under what conditions do alkyl azides rearrange to imines?
Here is a pretty interesting overview of the Schmidt reaction.
20-12-2018 at 05:01
by: Loptr
Would it be possible to make 2-bromobenzoyl chloride from salicylic acid
[rquote=564925&tid=114280&author=Nakhimov]Depends on what you have available to remove the P ...
19-12-2018 at 10:08
by: Loptr
Would it be possible to make 2-bromobenzoyl chloride from salicylic acid
Nope, not like that.

Phenol cannot undergo an SN1, E1 or SN2 reaction. For SN1 and E1, it's becau ...
19-12-2018 at 09:55
by: Loptr
synthesis of 2-bromobenzoyl chloride
Sure. What do you have?

SOCl2 + 2-bromobenzoic acid

You have SOCl2, right?
18-12-2018 at 16:00
by: Loptr
Demethylation of Vanillin and Eugenol
[rquote=564332&tid=92847&author=clearly_not_atara]DIC in that article stands for what I expe ...
18-12-2018 at 03:17
by: Loptr
Trying to start a catalysts business.
I would love some cheap catalysts lol. I know that when I start using them I will likely destroy a b ...
18-12-2018 at 03:14
by: Loptr
Demethylation of Vanillin and Eugenol
Has anyone seen this paper about demethylation of methyl vallinate, and eugenol, using AlI3, ethyl a ...
17-12-2018 at 15:30
by: Loptr
Whats the right method to make reaction between ethanol and phosphoric acid
I dont think phosphate esters can be made with the acid, but instead require a phosphorus halide. I ...
16-12-2018 at 16:55
by: Loptr
Proline decarboxylations
Thank you for your work. This is very interesting and something I would like to attempt.
16-12-2018 at 16:33
by: Loptr
Under what conditions do alkyl azides rearrange to imines?
Under what conditions do alkyl azides rearrange to imines? I am having some difficulty finding detai ...
15-12-2018 at 19:43
by: Loptr
Post #2000 and an apology for accidentally deleting a thread
I think this has to do with the posts that Melgar made about his drug synthesis accusations from his ...
15-12-2018 at 08:33
by: Loptr
Lot of Chemglass flasks - anyone interested in any of these?
How much would the 5L flask be?
14-12-2018 at 11:55
by: Loptr
Pulverizing Ni/Al for Raney Nickel
Yeah, I have fought eBay on Sodium metal and NaBH4, but as it turns out their policy is very straigh ...
2-12-2018 at 20:04
by: Loptr
Pulverizing Ni/Al for Raney Nickel
This is the claimed composition

Size 10-25mm
Composition: nickel 46.7%
...
2-12-2018 at 11:07
by: Loptr
Pulverizing Ni/Al for Raney Nickel
You dont. You dissolve the aluminum away using a base bath.
30-11-2018 at 13:29
by: Loptr
working with drums
Pipetting by mouth used to be the technique!
27-11-2018 at 10:41
by: Loptr
what form of formaldehyde is used in grignards?
Yeah, 1,3,5-trioxane and paraformaldehyde can be used in Grignard reactions. I have looked into this ...
27-11-2018 at 07:05
by: Loptr
working with drums
[rquote=556587&tid=106959&author=DrP]
I don't like the syphon idea - it is dated - we have ...
27-11-2018 at 05:15
by: Loptr
Water cooling for reflux condenser for 24 hours? Ice melts quickly, other set and forget options?
I have a mini chiller that I got off eBay.

https://www.amazon.com/Huber-Minichiller-Water-cooled- ...
26-11-2018 at 08:06
by: Loptr
working with drums
A siphon is a quick/easy and cheap option. I use one I got from an auto parts store for use with my ...
26-11-2018 at 06:10
by: Loptr
Cheap Potassium Iodide
I also ordered from JJay's link and received my order fairly quickly. This was very early on, about ...
26-11-2018 at 06:07
by: Loptr
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