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KMnO4 + HNO3
[rquote=200602&tid=15419&author=woelen] It might be an interesting experiment to add a TINY ...
4-2-2011 at 11:34
by: Formatik
The glassy carbon Anode: First test in a chlorate cell
[rquote=200377&tid=15345&author=garage chemist] Any ideas for a good method to determine chl ...
1-2-2011 at 15:55
by: Formatik
Making fire (youtube collaborative video)

[rquote=199918&tid=15370&author=garage chemist] Other than that, read the chapters about h ...
1-2-2011 at 15:45
by: Formatik
Making fire (youtube collaborative video)
[rquote=200093&tid=15370&author=mewrox99]I would imagine that DMS would be fairly reactive t ...
30-1-2011 at 08:53
by: Formatik
Making fire (youtube collaborative video)
A few drops of dimethyl sulfoxide dripped onto a small pile of sodium dichloroisocyanurate catches f ...
29-1-2011 at 08:35
by: Formatik
Synthesis of unsym.-heptachloropropane and hexachloropropene (updated)
[rquote=198987&tid=14584&author=garage chemist] I can't find any information on octachloropr ...
18-1-2011 at 16:06
by: Formatik
Isolation of urea from urine!
@Edenite:
Any base will work fine, you just boil it in solution. Something with hydroxide, like NaO ...
18-1-2011 at 16:04
by: Formatik
Isolation of urea from urine!
You need to hydrolyze the urea with a base (Ca(OH)2, K2CO3, etc) in solution to get any significant ...
15-1-2011 at 11:28
by: Formatik
How to approximate H2O2 concentration??
I would just invest in a scale, small glass 10mL graduated cylinder, etc. They are not expensive and ...
15-1-2011 at 11:25
by: Formatik
How to approximate H2O2 concentration??
There is also another way to attack this. Another method to use is mass loss. Measure the mass of th ...
14-1-2011 at 15:34
by: Formatik
Make Potassium (from versuchschemie.de)
[rquote=198525&tid=14970&author=blogfast25] A shock wave running through the mixture could g ...
14-1-2011 at 15:14
by: Formatik
Make Potassium (from versuchschemie.de)
[rquote=198375&tid=14970&author=watson.fawkes] Did these devices have standard contact area? ...
13-1-2011 at 22:57
by: Formatik
Chemical poisoning from dimethyl sulfide attempt
[rquote=198241&tid=15266&author=woelen]Good to read that you are recovering again and also g ...
12-1-2011 at 22:29
by: Formatik
Concerning test values
Staudinger was using a fallhammer method to get those values. The kilogram-meter (kgm): for every me ...
12-1-2011 at 21:28
by: Formatik
Diethylsulfide from potassium ethylsulfate and sodium sulfide
Pulmonary edema is one of the worst things one can die of. I had the fear I might have been developi ...
11-1-2011 at 20:21
by: Formatik
Chemical poisoning from dimethyl sulfide attempt
[rquote=198199&tid=15266&author=Baphomet]Cool post. Sorry to hear you nearly buried yourself ...
11-1-2011 at 19:54
by: Formatik
Make Potassium (from versuchschemie.de)
[rquote=198161&tid=14970&author=blogfast25] Edit: and in any case DCM's good for separting t ...
11-1-2011 at 19:31
by: Formatik
Diethylsulfide from potassium ethylsulfate and sodium sulfide
[rquote=169495&tid=13159&author=Myfanwy]Yes i got now 18g Diethyl sulfide.

http://www.you ...
11-1-2011 at 14:08
by: Formatik
Chemical poisoning from dimethyl sulfide attempt

I recently had some very unpleasant experiences after attempting to synthesize a compound.

Some ...
11-1-2011 at 13:52
by: Formatik
Endothermic freezing mixtures
Some more action from me. I've quantified it well compared to last attempts from some time ago. I re ...
17-12-2010 at 23:49
by: Formatik
Sulfuric Acid from Magnesium Sulfate
I've used magnesium sulfate to get to Na2SO4 by mixing it (aq.) with NaOH, filtering the Mg(OH)2 and ...
12-12-2010 at 15:53
by: Formatik
Endothermic freezing mixtures
[rquote=191110&tid=10444&author=S.C. Wack]By Mr. Richard Walker:

Observations on the best ...
12-12-2010 at 15:48
by: Formatik
Steel retort design for making Na metal for review
Zinc will alloy sodium at red-glow according to literature.
25-9-2010 at 14:30
by: Formatik
Steel retort design for making Na metal for review
[rquote=187947&tid=14491&author=metalresearcher] Unlike the Na3CO3 + charcoal mix, no fumes ...
22-9-2010 at 14:40
by: Formatik
Steel retort design for making Na metal for review
[rquote=187839&tid=14491&author=metalresearcher]@Formatik

The reaction *is* favorble @11 ...
19-9-2010 at 06:53
by: Formatik
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