Sciencemadness Discussion Board
Not logged in [Login ]
Go To Bottom

Search
[Next Page]
Azides
Hi all, i have some comments related to azides. First off all stay away from HN3, not even it is hig ...
20-2-2008 at 23:08
by: Engager
5-ATZ(5-Aminotetrazole), the nitrotetrazolate ion and friends
Today i've made batch of acid copper nitrotetrazolate for fourth time. Unlike my previous experieces ...
20-2-2008 at 20:44
by: Engager
Glyoxime, Diaminofurazan and Some Energetic Derivatives
Why you haven't tried microwave synth from glyoxime? It gives 70% yield from glyoxime to DAF vs 16% ...
6-1-2008 at 18:57
by: Engager
Digg new periodictable.com
[quote][i]Originally posted by Fleaker[/i]
Do you make those ampoules Engager, or was it a friend o ...
18-12-2007 at 11:46
by: Engager
Digg new periodictable.com
[quote][i]Originally posted by 12AX7[/i]
Awesome!

What's it look like slightly warmer? Does the ...
18-12-2007 at 08:35
by: Engager
Digg new periodictable.com
[quote][i]Originally posted by 12AX7[/i]
Is that actually liquid Xe? What's the critical temperatu ...
18-12-2007 at 05:48
by: Engager
Digg new periodictable.com
Here are some photos of my element collection (many samples are self made), it's not a full version ...
17-12-2007 at 19:21
by: Engager
5-ATZ(5-Aminotetrazole), the nitrotetrazolate ion and friends
[align=justify]Here is synthesis of 2 copper-nitrotetrazole complexes, both are efficent primaries, ...
30-10-2007 at 02:22
by: Engager
Bromine Source and Synthesis
[quote][i]Originally posted by woelen[/i]
I expect that engager will have a yield of approximately ...
12-10-2007 at 07:24
by: Engager
Preserving crystals of FeCl2*4H2O
Clever chemists use Mohr salt to store Fe(II) unoxidised. Mohr salt is simple ferric-ammonium sulpha ...
11-10-2007 at 18:31
by: Engager
Bromine Source and Synthesis
To produce large ammounts of bromine with ease i use following reaction:

5KBr + 3H2SO4(aq.) + KBr ...
11-10-2007 at 18:22
by: Engager
Interesting rare earth metals (lanthanoids) and thier salts
Most of metalls from this group can be made by reacting corresponding flouride with metallic calcium ...
11-10-2007 at 18:06
by: Engager
oleum & SO3
[quote][i]Originally posted by woelen[/i]
I now have some P2O5, and I did the experiment of adding ...
11-10-2007 at 17:22
by: Engager
5-ATZ(5-Aminotetrazole), the nitrotetrazolate ion and friends
[quote][i]Originally posted by The_Davster[/i]
HT-1 is very similar to another energetic.[/quote]
...
8-10-2007 at 06:28
by: Engager
5-ATZ(5-Aminotetrazole), the nitrotetrazolate ion and friends
There is also an interesting route from 5,5'-azotetrazole (which is made by simple oxidation of amin ...
7-10-2007 at 17:15
by: Engager
5-ATZ(5-Aminotetrazole), the nitrotetrazolate ion and friends
I've found a very interesting nitrotetrazole based compound in my russian explosive related document ...
7-10-2007 at 16:57
by: Engager
Dinitrourea
[quote][i]Originally posted by simply RED[/i]
Engager, when did the precipitate form?[/quote]

Af ...
5-10-2007 at 09:49
by: Engager
Dinitrourea
Reaciton scheme is shown below. Water at low temperature hydrolises dinitrourea to form CO2 and nitr ...
3-10-2007 at 16:11
by: Engager
Dinitrourea
[quote]<b>Russian Journal of Organic Chemistry, Vol. 38, No. 1, 2002</b>
Preparation of ...
3-10-2007 at 11:02
by: Engager
Dinitrourea
Why such difficulties are needed, it's far more simple to prepare nitramide by action of HNO3 on pot ...
30-9-2007 at 19:39
by: Engager
Hexanitroethane
What about action of KNO2 (or better AgNO2) on hexachloroethane C2Cl6 in methylene chloride? Will it ...
30-9-2007 at 19:25
by: Engager
5-ATZ(5-Aminotetrazole), the nitrotetrazolate ion and friends
[quote][i]Originally posted by Axt[/i]
Excellent posts Engager, but just a suggestion, dont use ima ...
30-9-2007 at 15:13
by: Engager
5-ATZ(5-Aminotetrazole), the nitrotetrazolate ion and friends
[b]Synthesis of acid copper 5-Nitrotetrazolate (CuNT) from 5-aminotetrazole[/b]

[align=justify]Pr ...
14-9-2007 at 03:37
by: Engager
5-ATZ(5-Aminotetrazole), the nitrotetrazolate ion and friends
Somebody interested in synthesis procedures for BNCP [Tetraamino-cis-bis(5-nitro-2H-tetrazolato-N2) ...
10-9-2007 at 22:54
by: Engager
5-ATZ(5-Aminotetrazole), the nitrotetrazolate ion and friends
[quote][i]Originally posted by The_Davster[/i]
What is the referance for this procedure? I have no ...
10-9-2007 at 22:02
by: Engager
[Next Page]

  Go To Top