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Making KBrO3 using Ca(OCl)2 and bromide.
Well; once I had got the orange coloured cake into solution, in 50ml of hot water, nothing crystalli ...
16-12-2021 at 15:02
by: Boffis
Chemistry to do with thymol
Hi Tsjerk, that paper is an interesting find. That method beats the pants off making o-sulphobenzoic ...
16-12-2021 at 14:37
by: Boffis
Making KBrO3 using Ca(OCl)2 and bromide.
I was so intrigued by the OP's process I decided to have a go at producing sodium bromate by simply ...
15-12-2021 at 13:31
by: Boffis
benzil by oxidation of benzoin with NH4NO3 catalyzed by Cu(II) acetate
Hi Fery, Nice work and a good write-up.

I have run this reaction myself but never seem to have po ...
11-12-2021 at 09:16
by: Boffis
Using sodium bisulphate instead of sulphuric acid
When hydrochloric acid was produced by the salt cake process the NaHSO4 and NaCl were fused together ...
11-12-2021 at 04:36
by: Boffis
Making KBrO3 using Ca(OCl)2 and bromide.
@Angrylittlebunny; what an interesting idea! Well done. Did you find this reaction somewhere or inve ...
7-12-2021 at 06:54
by: Boffis
monoamide of terephtalic acid
Have you thought about preparing the monoamide from the diamide? The latter can be prepared from PET ...
6-12-2021 at 02:41
by: Boffis
Chemistry to do with thymol
OK Guys, I think that's enough of the side show! The label on the IP bottle is quite clear. Now can ...
26-11-2021 at 09:12
by: Boffis
Citric acid (and its uses)
There are several threads already on the conversion of citric acid into acetone dicarboxylic acid, i ...
19-11-2021 at 07:36
by: Boffis
Synthesis of Lanthanum(III) acetylacetonate
Mmm interesting, this does seem to support some kind of condensation between the ammonia and the aca ...
18-11-2021 at 07:06
by: Boffis
Synthesis of Lanthanum(III) acetylacetonate
Hi TyppiHappo, have you tried just mixing the acetylacetone and ammonia and gently warming without a ...
16-11-2021 at 02:16
by: Boffis
Synthesis of Lanthanum(III) acetylacetonate
Tippihappo, is it possible that you acetylacetone is contaminated with a little aldehyde? particular ...
13-11-2021 at 06:35
by: Boffis
Propanoic acid from plexiglass
Hello Hexabromobenzene! well done! That's an impressive amount of PMMA to distil. What sort of equip ...
13-11-2021 at 01:56
by: Boffis
Valeric acid from sugar
Very interesting Hexabromobenzene! Is this your own procedure or is it from a published source? If t ...
13-11-2021 at 01:45
by: Boffis
Synthesis of Lanthanum(III) acetylacetonate
Hi TippiHappo, I am not sure I can answer your problem completely but having read the linked thesis ...
12-11-2021 at 21:18
by: Boffis
Reducing organic compounds with devarda's alloy?
@ Swim, yes I think you are right that's why I was asking about its similarity with aluminium amalga ...
9-11-2021 at 20:09
by: Boffis
Reducing organic compounds with devarda's alloy?
Hi Fery, many thanks for that paper! I think I can feel some experimental chemistry coming on! Devar ...
8-11-2021 at 05:46
by: Boffis
Reducing organic compounds with devarda's alloy?
I have a large jar of powdered Devarda's alloy that was once used for the analysis of nitrite and ni ...
8-11-2021 at 02:10
by: Boffis
Supplier of unusual inorganic from Poland
Very many thanks! Onyxmet… God my memory is going gaga.
31-10-2021 at 03:01
by: Boffis
Supplier of unusual inorganic from Poland
Over the years a supplier of unusual inorganic compounds has been referred to on this forum but now ...
31-10-2021 at 02:29
by: Boffis
Soluble Caffeine
I seem to recall that caffeine has a normal and steep solubility gradient so I would have thought th ...
28-10-2021 at 01:35
by: Boffis
Preparation of 2-hydroxybenzylamine
@kmno4; I've been following your activities with considerable interest as I have not yet got round t ...
17-10-2021 at 01:08
by: Boffis
Organoarsenic compound
The other reducing agent used for splitting azo dyes is stannous chloride but the newer thiourea dio ...
16-10-2021 at 21:36
by: Boffis
Organoarsenic compound
Hi Vano, I an not sure what world constitute "interest" to you but dithionite with cleave the diazo ...
16-10-2021 at 08:53
by: Boffis
Glycine anhydride, its preparation and cleavage to a dipeptide
@Dr.Bob That's a good point that I hadn't thought about, however, it may not be such a problem. My i ...
5-10-2021 at 21:31
by: Boffis
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