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Setting up microwave for chemistry
Microwave Assisted Organic Synthesis (Hardcover)
by Jason P. Tierney (Author), Pelle Lidstrom (Auth ...
4-8-2010 at 21:58
by: zed
Dry ice nozzles
You don't need a dry ice dealer. You need an ice cream dealer.

I knew a woman a few years ago, t ...
4-8-2010 at 21:20
by: zed
n,n-dimethyltryptamine by Eschweiler-Clarke methylation of tryptamine
Yes, I believe it's worth the effort. A simple, high yielding, fairly non-hazardous route to N,N-Di ...
4-8-2010 at 11:37
by: zed
n,n-dimethyltryptamine by Eschweiler-Clarke methylation of tryptamine
Ummm. Transmethylation of tryptamine via a betaine. Sounds like a good idea. But, does it work? ...
3-8-2010 at 20:47
by: zed
Old Chemistry Lab Manual
Ah.... In the early 70s, when I signed on as a lab tech in the Chem Storeroom of my JC Alma Mater, ...
3-8-2010 at 14:49
by: zed
Disgusting cover-up Attempt - READ THIS
So, government witnesses lie. That's nothing new.

Sometimes folks are prosecuted for attempting ...
3-8-2010 at 14:14
by: zed
n,n-dimethyltryptamine by Eschweiler-Clarke methylation of tryptamine
Thank you Nicoderm,

I'll check those Mannich reactions out, on my next visit to the library.

I ...
3-8-2010 at 11:29
by: zed
Synthesize of triglycerides
Yup! As I recollect, anyway.
2-8-2010 at 19:13
by: zed
n,n-dimethyltryptamine by Eschweiler-Clarke methylation of tryptamine
Yup! Nitromethane will definitely react with Propiophenone, in a Henry-type condensation. Whether ...
2-8-2010 at 19:05
by: zed
Magnesium powder from magnesium pencil sharpener
Yup! Turnings have always been good enough for me. At least in the past they have.

Turns out fi ...
31-7-2010 at 20:22
by: zed
Magnesium powder from magnesium pencil sharpener
Not many things can beat out Magnesium. So, makin' it aint real easy.

Fortunately, it's commerc ...
30-7-2010 at 17:07
by: zed
No more sodium from ebay
E-bay has developed a system that encourages, back stabbing. Most likely, someone considers you a c ...
30-7-2010 at 12:26
by: zed
Borohydride synth?
Well, the drawback of the above Sodium Borohydride synthesis, is that you need an active metal hydri ...
29-7-2010 at 19:11
by: zed
Borohydride synth?
Ummmm. Most of the hot new work on Hydrides, is being done in the field of energy storage. Hydrid ...
28-7-2010 at 23:35
by: zed
Safety glasses and face shields
(petitioner)
Oh, death...
Oh, death...
Won't you spare me over til another year?

Well, what is ...
27-7-2010 at 20:53
by: zed
Safety glasses and face shields
Suit yourself.
27-7-2010 at 13:22
by: zed
Esterified fatty acids
So, it's free fatty acids you are wanting? OK. But, they do tend to stink.

Usually, this is don ...
27-7-2010 at 13:03
by: zed
how do these 2 chemicals react?
[rquote=183528&tid=14217&author=turd]Actually no, I didn't realize that this used to be a co ...
27-7-2010 at 12:50
by: zed
how do these 2 chemicals react?
http://www.sciencemadness.org/talk/search.php?token=&srchtxt=nitroethane&srchfield=body& ...
27-7-2010 at 12:42
by: zed
how do these 2 chemicals react?
Turd,

You've never heard of using Nitroethane to produce Phenyl-2-Propanone, the classic Methamp ...
26-7-2010 at 23:44
by: zed
how do these 2 chemicals react?
Nitroethane? Hmmmmm. Do you mean Nitroethane, the DEA....list 1 precursor?

The difficult to obt ...
26-7-2010 at 22:58
by: zed
True Vacuum Pump vs. Water Aspirator
I was responding to BenzylChloride1, regarding a problem I have also encountered.

I had a brand n ...
26-7-2010 at 22:41
by: zed
True Vacuum Pump vs. Water Aspirator
You probably know more about vacuum pumps than I do, but sealing the pump by means of some sort of ...
26-7-2010 at 17:38
by: zed
proposed reduction via Al/Ga
Theory is good, theory is helpful, but nothing trumps experience.

So, Melgar......Stirring? Does ...
26-7-2010 at 17:21
by: zed
Indole Synthesis
I'm going to go back and read all of the references in this thread. But I do have a number on hand. ...
26-7-2010 at 11:53
by: zed
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