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Looking for Oxalyl Chloride (Swern ox) and 3-bromoanisole
Well, judging from the title, MM's asking about m-bromoanisole too, so...

sparky (~_~)
29-1-2009 at 20:32
by: sparkgap
preparation of salicylic acid from anthranilic acid
I'm inclined to think that the "they" alluded to in the third post in this thread must be some acade ...
29-1-2009 at 19:58
by: sparkgap
preparation of salicylic acid from anthranilic acid
As to diazotizing anthranilic acid (even though I still think better things can be done with diazoti ...
29-1-2009 at 08:12
by: sparkgap
preparation of salicylic acid from anthranilic acid
Seriously? I know a number of people who'd rather use the anthranilic acid for other purposes as it ...
29-1-2009 at 07:17
by: sparkgap
The short questions thread (1)
[quote][i]Originally posted by chemrox[/i]
Ahh .. yeah .. I forgot to mention the pyrrolidine moiet ...
28-1-2009 at 19:23
by: sparkgap
The short questions thread (1)
[quote][i]Originally posted by chemrox[/i]
Acetyl chloride seems much more reactive than acetic anh ...
28-1-2009 at 18:27
by: sparkgap
preperation of cumene from isopropanol and benzene
Maybe he confused cumene with cymene (isopropylmethylbenzene, which does have three isomers)...

B ...
27-1-2009 at 06:12
by: sparkgap
DNS trouble with website
The site was dead for me the whole of yesterday. Glad to see we're back up! :)

sparky (~_~)
26-1-2009 at 19:04
by: sparkgap
Crock Pot plating bath
(sorry for off-topic-ry)

@Swede:

If you're looking to reduce your body's lead-load, may I sugg ...
23-1-2009 at 08:48
by: sparkgap
Acid Concentration/purification
If you really want on Google...

http://www.google.com/search?q=site%3Asciencemadness.org%20distil ...
21-1-2009 at 14:48
by: sparkgap
The short questions thread (1)
Well, you have to take into account that your concentrated sulfuric acid actually transforms your et ...
21-1-2009 at 14:32
by: sparkgap
2-Bromo-6-nitrotoluene
Well, in fuming sulfuric acid, your sulfonation is an equilibrium reaction. :) All Sauron needs to d ...
20-1-2009 at 17:11
by: sparkgap
Alkenes from alcohols- a problem
[quote][i]Originally posted by Artemisia[/i]
Also- sparkgap, do you have access to that syn. comm. ...
20-1-2009 at 17:04
by: sparkgap
Alkenes from alcohols- a problem
I'm still trying to look for other stuff, but nearly everybody and his grandma seems to be on the so ...
20-1-2009 at 08:37
by: sparkgap
Alkenes from alcohols- a problem
Hmm, cursory searching netted [url=http://dx.doi.org/10.1016/0040-4039(91)80200-P]this[/url] and [ur ...
20-1-2009 at 08:07
by: sparkgap
The short questions thread (1)
Apparently my question was missed, so I'm gonna post it again:

[quote]Alright, I will have to ask ...
20-1-2009 at 07:35
by: sparkgap
Dean Stark Trap
(offtopic) the "sub" and "sup" HTML tags work on this board, like so: <sup>3</sup>H<s ...
19-1-2009 at 08:31
by: sparkgap
Uses of tungsten copper alloy
Here's the Landolt-Bornstein phase diagram John was alluding to. I will merely comment that I'm cast ...
18-1-2009 at 00:49
by: sparkgap
The short questions thread (1)
[quote][i]Originally posted by solo[/i]
I need to find the CAS number for Sodium Naphthalene, `i'v ...
14-1-2009 at 17:53
by: sparkgap
Racemizing Optically Active Amines
[quote]In a dry, 500-mL, three-necked flask equipped with a mechanical stirrer, an addition funnel, ...
14-1-2009 at 17:50
by: sparkgap
Why you should always dispose properly of your chemical waste
[url=http://dx.doi.org/10.1021/es802309v]I think I posted this before...[/url]

sparky (~_~)
12-1-2009 at 18:29
by: sparkgap
Sodium Borohydride Synthesis
chemoleo, may I suggest just merging the threads and renaming the thread to "Metal Borohydrides" or ...
11-1-2009 at 20:43
by: sparkgap
The short questions thread (1)
And if you'll look at what turd posted, the extra carbon should have come from somewhere, acetic anh ...
11-1-2009 at 05:39
by: sparkgap
The short questions thread (1)
No, for one thing lead tetraacetate cannot magically convert an -OH group into a -CH3 group.

spar ...
11-1-2009 at 02:20
by: sparkgap
Terephthalic acid from PET
You're essentially driving the esterification equilibrium (Le Chatelier''s, remember?) towards acid+ ...
10-1-2009 at 18:35
by: sparkgap
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