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Bromination of Vanillin without bromine Hello everyone,
It has been a while since I have posted anything of interest, so I thought I woul ... |
23-2-2012 at 22:08 by: mnick12 |
Cheap, Quality Glass Source (Laboy Glass) Just a quick update,
I would like to retract my earlier statement about Laboy, it appears as thou ... |
22-2-2012 at 18:17 by: mnick12 |
NaBH4 I know of few places, but it depends where you live. |
22-2-2012 at 15:00 by: mnick12 |
Cheap, Quality Glass Source (Laboy Glass) Just a word of caution,
I have ordered from Laboy a number of times, through ebay and the the onl ... |
18-2-2012 at 10:40 by: mnick12 |
Good substrate to test Urushibara Nickel? Yea so far this is looking like it is not going to work.
I tried hydrogenating 1.4ml of nitrobenz ... |
26-11-2011 at 21:33 by: mnick12 |
Good substrate to test Urushibara Nickel? I have a few ml of eugenol I could try reducing, but I am not quite sure how to test if hydrogenatio ... |
17-11-2011 at 17:22 by: mnick12 |
Good substrate to test Urushibara Nickel? Just a little update,
Not having any styrene or permanganate, I opted for 4-butoxy-3-methoxypheny ... |
16-11-2011 at 18:59 by: mnick12 |
Good substrate to test Urushibara Nickel? Hello everyone,
I have a question which I hope some of you may be able to help me with. It has be ... |
14-11-2011 at 20:36 by: mnick12 |
Oxidizing Naphthalene to Phthalic anhydride Phthalic anhydride? You mean phthalic acid. Anhydrides cannot be precipitated from aqueous solutions ... |
31-10-2011 at 18:52 by: mnick12 |
1-bromo-3-methoxybenzene I had an interest in this compound a while ago, and while I never completed the synthesis I had good ... |
10-10-2011 at 16:26 by: mnick12 |
4-ethoxyphenol No I partially neutralized the H2SO4, distilled of 55ml of ethanol, poured the solution into brine t ... |
11-9-2011 at 20:50 by: mnick12 |
4-ethoxyphenol Hello everyone,
I am having a little bit of trouble with 4-ethoxyphenol. There are a number of thr ... |
10-9-2011 at 11:13 by: mnick12 |
Latest chemical order? My last orders:
Dimethyl formamide-500ml
Nitromethane-500ml ACS
Methanol-1L
GAA-1L
Methylene ... |
8-8-2011 at 19:18 by: mnick12 |
Request for The Preparation and Testing of Nickel Catalysts for Hydrogenation Ahhh if your interested in nickel and other transition metal based catalsts there are quite a few fr ... |
29-6-2011 at 18:01 by: mnick12 |
Which is your year of birth? 17 years old, born in 94.
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8-6-2011 at 12:39 by: mnick12 |
Formaldehyde at home - how safe is it? I have a gallon or so of the stuff in my fridge, and have had it there for about 2 years. So far no ... |
6-6-2011 at 13:30 by: mnick12 |
Preparation of 1-bromo-3-nitrobenzene I wont be able to do any lab stuff for about 2 months , but I will tell some
things I did which m ... |
4-6-2011 at 19:42 by: mnick12 |
urea to ammonia to nitrate There are some species of nitro and nitrosobacter which are able to use urea directly as their nitro ... |
13-5-2011 at 19:20 by: mnick12 |
recution of 1-bromo-3-nitrobenzene Hello everyone,
I recently prepared a small amount of 1-bromo-3-nitrobenzene from sulfuric acid, ... |
1-5-2011 at 13:36 by: mnick12 |
Preparation of 1-bromo-3-nitrobenzene Good news, and sorry for the triple post.
Anyway I did a small scale run of the procedure describ ... |
1-5-2011 at 13:29 by: mnick12 |
Making fire (youtube collaborative video) I dont think recrystallization would work for Ca(ClO)2, hypochlorites are very unstable in aqueous s ... |
16-4-2011 at 22:36 by: mnick12 |
Problems nitrating acetophenone Hello everyone,
I have an annoying problem that I hope you all may be able to help me with. I am in ... |
6-4-2011 at 18:46 by: mnick12 |
Making fire (youtube collaborative video) Well if anyone is looking for ideas CrO3 and acetone makes a spectacular fireball-whoooosh if done i ... |
27-3-2011 at 13:07 by: mnick12 |
home brew silica supported hydrogenation catalysts I've tried urushibara nickel and have had mixed results.
On the subject of nickel oxide I am cert ... |
23-3-2011 at 22:11 by: mnick12 |
Nitroethane from ethylsulfate, Desseigne variation. Yea its a good idea to use a large excess of ethanol, it makes stirring easier, and the end product ... |
22-3-2011 at 20:15 by: mnick12 |
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