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Benzyl Iodide/Benzyl Cyanide Synthesis
It would be simpler to react benzyl alcohol with hydrochloric acid. Using chlorine gas and toluene w ...
1-10-2014 at 02:09
by: forgottenpassword
Haloform with IPA 3&4 could really do with some help
Chloroform is soluble in IPA. You could dilute your solution with water to precipitate it again.
A ...
1-10-2014 at 02:03
by: forgottenpassword
Have I made drinkable ethanol from metylated spirits
Obviously claims of cyclohexane oxidation are a nonsense, but the method of extracting it (or any al ...
30-9-2014 at 01:00
by: forgottenpassword
Setting up a UK chemical supply company
What I would find useful is the ability to place custom orders. Several times I have had to resort t ...
25-9-2014 at 09:44
by: forgottenpassword
Ergotamine extraction
Yes.
20-9-2014 at 10:41
by: forgottenpassword
Ergotamine extraction
The only tip I could give you is that ergotamine is insoluble in petroleum ether/naphtha.
20-9-2014 at 09:59
by: forgottenpassword
Ergotamine extraction
I very much doubt that ergotamine is soluble in naphtha. Why did you not research the extraction met ...
20-9-2014 at 07:57
by: forgottenpassword
Exhaust fumes through the kitchen fan?
Firstly you should plan to create as few fumes as possible. When distilling you can have a length of ...
20-9-2014 at 07:43
by: forgottenpassword
99% IPA in store?
How can a 1% impurity cause a lot of trouble?
20-9-2014 at 00:55
by: forgottenpassword
How do I titrate Sodium Hypochlorite?
Google it. This is a common school based practical, and as such there are many detailed procedures.
19-9-2014 at 03:28
by: forgottenpassword
Has anyone here attempted to build a DIY HPLC contraption?
If you are using TLC to assess the effectiveness of the separation, why not just use TLC instead of ...
18-9-2014 at 13:30
by: forgottenpassword
and i Thought i just bought some Toluene ...
Methanol 64.7
Methyl acetate 57.0
Acetone 56.5
Methyl acetate / water 56.1
Methanol / acetone 5 ...
16-9-2014 at 14:26
by: forgottenpassword
and i Thought i just bought some Toluene ...
Some are listed on the Wikipedia azetrope (data) page. I don't think that the relevant ternary azeot ...
16-9-2014 at 14:11
by: forgottenpassword
and i Thought i just bought some Toluene ...
Maybe they are azeotropes then. If you are certain that they are fractions then looking up data for ...
16-9-2014 at 14:06
by: forgottenpassword
and i Thought i just bought some Toluene ...
[rquote=345719&tid=33672&author=aga]

Varying ratios of 4 ingredients leading to 11 multi- ...
16-9-2014 at 13:51
by: forgottenpassword
and i Thought i just bought some Toluene ...
It doesn't contain ethyl acetate. The 'fractions' comprise a continous range from 53 to 86 Celsius - ...
16-9-2014 at 13:21
by: forgottenpassword
and i Thought i just bought some Toluene ...
If chloroform, carbon tetrachloride and benzene were present, they would surely be soluble in the to ...
16-9-2014 at 10:29
by: forgottenpassword
Laboratory Rack Mounts? - What is the sales name for this?
Something like this?
http://www.ebay.com/itm/Stainless-Steel-Beauty-Salon-Spa-Trolley-Storage-Cart- ...
13-9-2014 at 16:16
by: forgottenpassword
distillation problems
[rquote=345217&tid=33415&author=Little_Ghost]
I am not having much luck with TLC, the main ...
13-9-2014 at 10:00
by: forgottenpassword
distillation problems
He is trying to determine the boiling points as a means to identify the fractions. Distilling at an ...
11-9-2014 at 03:56
by: forgottenpassword
distillation problems
Put petroleum jelly on all of the joints and wrap a lot of aluminium foil around the joint of the fl ...
10-9-2014 at 23:58
by: forgottenpassword
3-methyl-1-phenylbut-2-en-1-one
[rquote=344888&tid=33410&author=Eddygp]
What can I do with the product? [/rquote]
You've p ...
10-9-2014 at 07:54
by: forgottenpassword
Lithium + xylene = ?
[rquote=344673&tid=33349&author=Brain&Force]a small amount of xylene was ignited in the ...
8-9-2014 at 13:49
by: forgottenpassword
need a little analytical help
Did you put petroleum jelly on the joints of the glassware?
If I understand you correctly, you are ...
5-9-2014 at 12:13
by: forgottenpassword
Solvents for Sodium Borohydride - why is methanol often included even with non-reactive polar aprotic solvents to dissolve the B
If you'd have clicked the link you would know that it is soluble to the extent of 0.1 g in 100g of T ...
4-9-2014 at 23:57
by: forgottenpassword
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