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Cesium from CsCl
Hi Blogfast25
I've only converted a small portion of the CsCl to metal. And only part of the last b ... |
21-1-2012 at 12:06
by: Zan Divine |
Cesium from CsCl
[rquote=230800&tid=6981&author=Fleaker]Welcome to the cesium club! As congratulations, I can ... |
20-1-2012 at 16:47
by: Zan Divine |
Tert-Butyl Lithium
Hexavalent,
It's been known for a long time that many Grignard reagents can be prepared in toluen ... |
14-1-2012 at 13:15
by: Zan Divine |
Cesium from CsCl
I have no means of accurately measuring purity. The samples listed as 99% were prepared according to ... |
6-1-2012 at 20:03
by: Zan Divine |
Cesium from CsCl
And here is the final commercial product.... |
5-1-2012 at 17:26
by: Zan Divine |
Cesium from CsCl
As I needed to handle, purify and (for another outlet), package exhibitable samples of shiny lithium ... |
1-1-2012 at 10:29
by: Zan Divine |
Cesium from CsCl
Hi Fleaker,
Yes, I saw the reference to Len's work earlier.
I'd be interested in hearing any sug ... |
27-12-2011 at 12:03
by: Zan Divine |
Cesium from CsCl
Blogfast25...
Yes, I think this is the answer. Why strive to exclude all O2 from a big fat bag when ... |
24-12-2011 at 10:19
by: Zan Divine |
Cesium from CsCl
I bought the Li this time, from GalliumSource in Ca. I've never found a better source for Li, Na or ... |
22-12-2011 at 07:47
by: Zan Divine |
Cesium from CsCl
This is a shot of the metal from my first production run. Pre-drying of the reactor, flame drying of ... |
21-12-2011 at 20:49
by: Zan Divine |
Cesium from CsCl
This may be new to the foum... |
15-12-2011 at 21:25
by: Zan Divine |
Cesium from CsCl
What I use as a sealing technique is to put a compressed pipette bulb over the end of the ampoule. A ... |
6-12-2011 at 09:23
by: Zan Divine |
Cesium from CsCl
Interestingly, I'm in charge of installation & servicing for our company in the US....our produc ... |
5-12-2011 at 15:12
by: Zan Divine |
Cesium from CsCl
Calcium was my second choice. Due to lithium's higher % yield and the fact that it would be liquid a ... |
5-12-2011 at 11:08
by: Zan Divine |
Cesium from CsCl
[IMG]http://i42.tinypic.com/2j2barl.jpg[/IMG]
These are a couple ampoules I made up by melting th ... |
4-12-2011 at 16:40
by: Zan Divine |
Cesium from CsCl
That's an interesting point you raise. The reaction may proceed fastest at around 600 or above but b ... |
4-12-2011 at 11:43
by: Zan Divine |
Cesium from CsCl
I'm aware of the method. It was actually the method I was going to use before I remembered that I ha ... |
4-12-2011 at 10:35
by: Zan Divine |
Cesium from CsCl
[IMG]http://i44.tinypic.com/25584ti.jpg[/IMG]
This is a screenshot of the US patent. With % yield ... |
4-12-2011 at 08:09
by: Zan Divine |
Cesium from CsCl
Just made Cesium
Well, it was too damn easy.
Used patent US3164461.
This is a Li metallotherm ... |
3-12-2011 at 21:21
by: Zan Divine |
