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What does "drying over" some desiccant mean?
First let me apologize for this noob question, but I haven't been able to find a clear answer anywhe ...
19-6-2021 at 16:40
by: Monoamine
Errata
So for some reason, the system won't let me correct the original post, so consider this the errata t ...
13-6-2021 at 08:48
by: Monoamine
Sythesis proposal for preparing 1,3-benzodioxole oxidation products using simple precursors
[rquote=661625&tid=157590&author=Amos]I mean, I can appreciate that you worked hard on this, ...
12-6-2021 at 14:17
by: Monoamine
Sythesis proposal for preparing 1,3-benzodioxole oxidation products using simple precursors
1,3-benzodioxoles are a well-known class of substituted benzene derivatives. Perhaps the most useful ...
11-6-2021 at 21:11
by: Monoamine
Indole-3-Carbinol Oxidation
[rquote=661537&tid=8132&author=zed]It's a thing. https://en.wikipedia.org/wiki/Indigo_dye[/ ...
10-6-2021 at 13:22
by: Monoamine
Naive question
One thing that has foiled most of my attempts to do this oxydation so far is the fact the In-3-CH[su ...
9-6-2021 at 18:35
by: Monoamine
Purifying and recrystallizing OTC In-3-CH2-OH
[rquote=661333&tid=8132&author=mr_bovinejony]Yeah I still have them, but the color is stupid ...
9-6-2021 at 18:22
by: Monoamine
This might be worth a try. And it should be useful for oxidizing Ar-CH2-OH compounds in general.
This may be worth a shot as it uses relatively easy to obtain reagents and seems very straight forwa ...
9-6-2021 at 18:10
by: Monoamine
Indole-3-Carbinol Oxidation
[rquote=661142&tid=8132&author=Monoamine]First off, since I didn't have dichloromethane, I u ...
5-6-2021 at 03:04
by: Monoamine
Question about sulfonation of furan
[rquote=661197&tid=157555&author=UC235]Start here: DOI: 10.1021/jo01371a003

Gives prep of ...
2-6-2021 at 19:35
by: Monoamine
Question about sulfonation of furan
I recently came across some lecture notes on sulfonic acid protection of furan to control its regioc ...
2-6-2021 at 15:07
by: Monoamine
I tried this and this is what happened:
First off, since I didn't have dichloromethane, I used chloroform as my solvent.

(Also, one thing ...
1-6-2021 at 15:10
by: Monoamine

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