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Preparation of propionic acid
I see where Ca propionate is available on eBay for about $11/500g w/free shipping. But I don't have ...
4-4-2015 at 09:07
by: Magpie
What does refluxing do exactly
[rquote=399688&tid=62020&author=DraconicAcid]It keeps it at a constant temperature without h ...
4-4-2015 at 08:44
by: Magpie
Nitromethane, nitroethane, nitropropane synthesis via industrial route
I would be wary of using nitrites for this because of the possibility of forming carcinogenic nitros ...
2-4-2015 at 10:54
by: Magpie
Steam Distillation advice
[b]Always[/b] vent through the stopcock after shaking until you get no more gas release. This is es ...
2-4-2015 at 08:20
by: Magpie
Preparation of Salicylaldehyde
Thanks Jimmy. No, I have no plans to make acetaldehyde at this time. But I might in the future, as ...
1-4-2015 at 10:08
by: Magpie
Steam Distillation advice
[rquote=399256&tid=61988&author=nowlan]
Filled the 500ml receiving flask with water and pou ...
1-4-2015 at 08:00
by: Magpie
Nitromethane, nitroethane, nitropropane synthesis via industrial route
Jimmy I don't know anything about what you are doing here but I'm impressed with your technochemistr ...
1-4-2015 at 05:17
by: Magpie
Preparation of Salicylaldehyde
Thank you Nexus.

After recovering the 2nd batch of DCM (40 mls) I gave it a sniff test (not rec ...
31-3-2015 at 18:45
by: Magpie
Moonshiners' 'Thumpers': Myth or Reality?
[rquote=399213&tid=61566&author=Zombie]
Anyway... I'm glad to be back posting. I spent the ...
31-3-2015 at 18:31
by: Magpie
toluene --> benzaldehyde
No, hiring a glassblower is not a big deal and I encourage it. I have hired glassblowers to make bo ...
31-3-2015 at 14:02
by: Magpie
Preparation of Salicylaldehyde
[rquote=399175&tid=61964&author=Waffles SS]Are you sure Benzaldehyde is stable in oxidation? ...
31-3-2015 at 11:23
by: Magpie
Preparation of Salicylaldehyde
Thank you waffles and lullu. I used the Reimer-Tiemann for the reasons stated in the "Discussion" s ...
31-3-2015 at 08:42
by: Magpie
isoamyl alcohol
I'm now remembering that the industrial alcohol producers who produce large quantities use continuou ...
31-3-2015 at 08:23
by: Magpie
Moonshiners' 'Thumpers': Myth or Reality?
A thumper should work on any binary system. After all it is just a second stage. It's especially e ...
30-3-2015 at 19:49
by: Magpie
Preparation of Salicylaldehyde
No, I did not. The adduct that slipped under the filter paper would have been in there too, along w ...
30-3-2015 at 19:00
by: Magpie
isoamyl alcohol
I think it depends on how much of it they generate. It's mostly isoamyl alcohol which has quite a f ...
30-3-2015 at 17:48
by: Magpie
Preparation of Salicylaldehyde
Thank you blogfast, morganbw and Loptr. ;)

I hope JimmyMajesty tries isolating his acetaldehyde ...
30-3-2015 at 17:38
by: Magpie
Preparation of Salicylaldehyde
[b]Continuation[/b]

[b]f. Sulfite adduct formation[/b]
The sulfite adduct is now formed to separ ...
30-3-2015 at 14:58
by: Magpie
Preparation of Salicylaldehyde
a lab report


[b]A. Introduction[/b]
Salicylaldehyde (SA) can be prepared using a Reimer-Tieman ...
30-3-2015 at 14:18
by: Magpie
Preparation of propionic acid
I just checked Safeway bakery again - no propionates or azodicarboamide - also unbrominated - and br ...
30-3-2015 at 10:24
by: Magpie
Preparation of propionic acid
I asked one of the baking staff at my local Safeway if she used calcium propionate or azodicarbonami ...
30-3-2015 at 08:03
by: Magpie
Moonshiners' 'Thumpers': Myth or Reality?

Very nice work, boys! - very professional.

[rquote=398991&tid=61566&author=aga]
Anyon ...
29-3-2015 at 16:34
by: Magpie
Looking over the border: EU-Regulations
[rquote=398866&tid=23212&author=aga]
It also said 'Agricultural use only' ![/rquote]

Tha ...
29-3-2015 at 10:27
by: Magpie
toluene --> benzaldehyde
[rquote=398926&tid=2223&author=Jimmymajesty]
I like how easy is to replicate "complicated" ...
29-3-2015 at 10:12
by: Magpie
toluene --> benzaldehyde
Jimmy you are really pioneering many uses for your catalytic device!

I am currently in the middle ...
28-3-2015 at 08:50
by: Magpie
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