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(HPO3)n Dehydrating agent (polyphosphoric or metaphosphoric acid)
Alright, well I really doubt anyone here can answer from experience. In all likelihood the answer is ...
1-5-2021 at 14:28
by: njl
Synthesis of Ethyl Methylphenylglycidate
[rquote=659221&tid=157363&author=Amos] The actual phenylacetone precursor found in clandesti ...
1-5-2021 at 14:23
by: njl
Acetic anhydride preparation
Yes I believe in earlier pages of this thread. Sometimes a pain to read through, but I remember it b ...
1-5-2021 at 14:15
by: njl
(HPO3)n Dehydrating agent (polyphosphoric or metaphosphoric acid)
You're gonna have to elaborate on "sulfuric monochloride". Do you mean chlorosulfuric acid? Or disul ...
1-5-2021 at 12:37
by: njl
Synthesis of Ethyl Methylphenylglycidate
Yes, my mistake. The precursor compound is sold as a phenylacetone precursor under the name "BMK gly ...
30-4-2021 at 19:01
by: njl
Ketalization of Phenol
Cyclohexanone is just a regular ketone, it will form a ketal under the conditions commonly used for ...
30-4-2021 at 15:00
by: njl
Synthesis of Ethyl Methylphenylglycidate
Cool your jets SC. I also thought this thread was about [b]benzyl[/b] glycidate (the compound you're ...
30-4-2021 at 14:57
by: njl
Methyl iodide (iodomethane) woes (Red P method)
A funnel clogged with red p sounds like a pain... the phosphorus might slowly react to various oxide ...
30-4-2021 at 06:19
by: njl
Most toxic compound OTC?
We need a stickied thread on OTC antimatter ASAP
30-4-2021 at 04:35
by: njl
preparation/acquisition of acetone (weird problem ik)
Ketonic decarboxylation is a known reaction that has been thoroughly documented. While it may be a s ...
29-4-2021 at 10:23
by: njl
Recovery of styrene monomer from polystyrene
Off topic to this thread, but what did you end up doing with it?
29-4-2021 at 04:50
by: njl
Acetic anhydride preparation
Atara is referring to a thread on the vespiary by user Scarecrow called "Reliable OTC Acyl chloride ...
29-4-2021 at 02:57
by: njl
preparation/acquisition of acetone (weird problem ik)
This is just the beginning of an idea (can't give you any conditions at the moment), but perhaps the ...
29-4-2021 at 02:46
by: njl
distilling Metheglin
I am speaking from my experience with [url=https://www.walmart.com/ip/Great-Value-Distilled-White-Vi ...
28-4-2021 at 14:12
by: njl
Recovery of styrene monomer from polystyrene
[rquote=659009&tid=157360&author=unionised]
Also works with PMMA
[/rquote]

Yielding met ...
28-4-2021 at 14:01
by: njl
Recovery of styrene monomer from polystyrene
The gist of polystyrene to styrene monomer is mostly thermal cracking as far as I know. There are so ...
28-4-2021 at 05:08
by: njl
Making n-butyl bromide (1-bromobutane) for TBAB (Tetrabutylammonium bromide) synthesis
There are good reviews for chemcraft in one of the reagents acquisition threads.
27-4-2021 at 17:00
by: njl
Isolation of 1,1-diphenyl ethanol
If what I suggested works I don't see why you shouldn't go for it, however I think Drac is right in ...
27-4-2021 at 16:58
by: njl
Isolation of 1,1-diphenyl ethanol
You can try removing more of the hexane then cool as low as possible and wait. To improve yield and ...
27-4-2021 at 13:09
by: njl
distilling Metheglin

[quote]
The problem here is vocabulary and definitions. The sour end liquid is called badly "vine ...
27-4-2021 at 10:54
by: njl
Preparation of elemental phosphorus
Yes, I think it would be necessary to remove the phosphorus as it forms by distilling it off. But th ...
27-4-2021 at 10:37
by: njl
distilling Metheglin

[quote]
Metheglin / meed?
me·theg·lin

[Welsh meddyglyn : meddyg, medicinal (from Latin medi ...
27-4-2021 at 08:18
by: njl
Path to 4-Anisaldehyde
Mass harder to visualize for me than volume, so for reference (with a density of 1.6 g/cc) .2 grams ...
27-4-2021 at 07:48
by: njl
Preparation of elemental phosphorus
Atara, if you do the math: 2 percent solution of Ca3(PO4)2 in 1 Kg molten salt = 20 grams Ca3(PO4)2 ...
27-4-2021 at 06:18
by: njl
Effecting a separation of two, nearly identical compounds
PubChem claims that AN is somewhat soluble in acetone, while urea is not.
27-4-2021 at 04:59
by: njl
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