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Selective Amination of Benzoic Acid
Hmmm more armchair chemistry!
This topic has been discussed quite a few times in the past, I sugg ... |
26-6-2012 at 00:27
by: mnick12 |
5-hydroxylation of dopamine
Oh hmmm looking for some 3,4,5- tri substituted phenethylamines? There are better ways which are kno ... |
17-6-2012 at 20:18
by: mnick12 |
Lava sediment in Ferric Nitrate solution
Solutions containing the Fe3+ ion often form precipitates when exposed to air for extended periods o ... |
17-6-2012 at 11:18
by: mnick12 |
Water flouridation
Really five posts in a row? Why not just include all this "information" in a single post and prevent ... |
7-6-2012 at 14:59
by: mnick12 |
Yeast corroding aluminium?
Hi everyone I just had a peculiar incident and wanted to get other peoples opinions on what has occu ... |
31-5-2012 at 12:31
by: mnick12 |
Some more encouraging news
Well I just finished another attempt at a methylation with TMP, but with a different substrate.
... |
12-5-2012 at 18:59
by: mnick12 |
Attempted Methylation of Paracetamol with TMP
Hi thank you for the replies.
Nicodem,
I did not run TLC during the course of this synthesis, bu ... |
3-5-2012 at 18:09
by: mnick12 |
Attempted Methylation of Paracetamol with TMP
Hello everyone, I would like to share my experience of methylating paracetamol with trimethyl phosph ... |
2-5-2012 at 19:31
by: mnick12 |
Laboy glass: coiled condensers?
I have 200mm graham condenser from Laboy, and so far it has held up very well. All of the products w ... |
1-5-2012 at 20:32
by: mnick12 |
Paracetamol + NaOH
Excess NaOH would deprotonate the phenol, and the resulting phenoxide is susceptible to atmospheric ... |
21-4-2012 at 20:12
by: mnick12 |
2-(propylsulfanyl)benzene-1,4-diol mp?
Thanks,
Unfortunately the product I isolated had a mp which was way off. Im not quite sure what w ... |
21-4-2012 at 16:00
by: mnick12 |
How to kick start the haloform reaction
Solid sodium hypochlorite? Hmmm considering the instability of hypochlorites I doubt you have pure s ... |
21-4-2012 at 15:52
by: mnick12 |
balancing equations
Well while that equation is essentialy correct it is lacking the proper coefficients, the balanced e ... |
12-4-2012 at 14:46
by: mnick12 |
2-(propylsulfanyl)benzene-1,4-diol mp?
Hello just a quick question regarding the physical properties of 2-(propylsulfanyl)benzene-1,4-diol. ... |
12-4-2012 at 07:01
by: mnick12 |
Last Man Standing, Anti Hangover Formulation.
Ethanol is also a dehydrogenase inhibitor. So the way to cure your hangover is to a have a few shots ... |
11-4-2012 at 06:55
by: mnick12 |
Anthranilic Acid Synthesis
[rquote=244657&tid=19662&author=Hexavalent]I do not have access to phthalimide, benzoic acid ... |
10-4-2012 at 18:50
by: mnick12 |
Anthranilic Acid Synthesis
Yes nitration of benzoic acid or its esters will yield the 3-nitro compound. However if you are inte ... |
9-4-2012 at 06:51
by: mnick12 |
ParaFormaldehyde preparation from formaline
Well, boiling a formalin solution under atmospheric pressure will result in massive amounts of forma ... |
30-3-2012 at 14:58
by: mnick12 |
Urea pyrolysis
I would imagine the pyrolysis of urea would be a very messy set of reactions. When heated strongyl u ... |
29-3-2012 at 19:52
by: mnick12 |
ParaFormaldehyde preparation from formaline
The simplest way to prepare paraformaldehyde from a formalin solution is through vacuum distillation ... |
29-3-2012 at 19:40
by: mnick12 |
Preparation of trimethyl phosphate
From my own expirience I can say that TMP is a decent methylating agent. It is capable of methylatin ... |
26-3-2012 at 18:46
by: mnick12 |
Amide hydrolysis help
entropy51 thank you for the advise.
Following your suggestion of aqueous NaOH, I tried a base cat ... |
18-3-2012 at 21:21
by: mnick12 |
Amide hydrolysis help
I am a little embarrassed to ask a question like this, but I need some advice.
Lately I have been ... |
18-3-2012 at 13:27
by: mnick12 |
Bromination of Vanillin without bromine
About two weeks ago I tried a modified scaled up version of my original procedure based on the advis ... |
18-3-2012 at 13:10
by: mnick12 |
Persulfate oxidation of hydroquinone
It is most likely quinhydrone which is a complex of hydroquinone and benzoquinone. It is often the p ... |
2-3-2012 at 19:36
by: mnick12 |
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