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Glyoxylic acid by magnesium reduction
You dont need to use H2SO4 or HCl.just use US3779876 workup in example 2

Barium glyoxylate is sol ...
10-8-2016 at 19:41
by: Waffles SS
Glyoxylic acid by magnesium reduction
[rquote=457338&tid=66504&author=gravityzero]If anyone cares to shed a little more light on t ...
10-8-2016 at 09:41
by: Waffles SS
Preparation of Bismuth chloride
Today i tried to make BiCl3 from Bismuth metal .

I used 0.1 mol(20.9gr) Bismuth metal , 0.3mol(~1 ...
26-7-2016 at 06:35
by: Waffles SS
Sulfonation of Phenol
Separation of isomer is not easy and i really could not find trustable method.

I usually separate ...
25-7-2016 at 09:09
by: Waffles SS
Preparation of Bismuth chloride
Thanks @zts16,

Can you explain more your method? (ratio and temp)
24-7-2016 at 10:49
by: Waffles SS
Preparation of Bismuth chloride
Bismuth Chloride hydrolysis to Oxychlorid in aqueous solution and i think this is not possible to us ...
24-7-2016 at 10:38
by: Waffles SS
Preparation of Bismuth chloride
[align=center][img]https://upload.wikimedia.org/wikipedia/commons/3/3a/Chlorid_bismutit%C3%BD.PNG[/i ...
24-7-2016 at 09:10
by: Waffles SS
Making Determination Kit
@NEMO-Chemistry thanks,

It will help us to find out what is material of each one

I really want ...
1-7-2016 at 09:10
by: Waffles SS
Making Determination Kit
[b]Total hardness[/b]

I found below procedure after searching in google.

If someone have bette ...
30-6-2016 at 22:55
by: Waffles SS
Making Determination Kit
I create this topic for collecting information about making Determination Kits

Please post your i ...
30-6-2016 at 22:46
by: Waffles SS
Glyoxylic acid by magnesium reduction
Glyoxylic acid is unstable compound and has different odor than most of aldehydes.it has yellow colo ...
12-6-2016 at 19:06
by: Waffles SS
Glyoxylic acid by magnesium reduction
I did [url=https://en.wikipedia.org/wiki/2,4-Dinitrophenylhydrazine]Brady's test[/url]
12-6-2016 at 10:12
by: Waffles SS
Glyoxylic acid by magnesium reduction
I attached all possible way for synthesis of glyoxylic acid.

[file]51415[/file]

One of intere ...
12-6-2016 at 09:49
by: Waffles SS
Glyoxylic acid by magnesium reduction
I tried this method several times and each time i got unchanged oxalic acid
reference of that video ...
12-6-2016 at 05:26
by: Waffles SS
Acetic anhydride preparation
@chemplayer,

I watched your video on Youtube and i am sure your final product is Ac2O.(I have exp ...
6-3-2016 at 21:37
by: Waffles SS
2,2-dinotropropanol synthesis
[rquote=439273&tid=65352&author=franklyloveyou]Hey All
I'm looking for tips on 2,2-dinotrop ...
19-2-2016 at 07:41
by: Waffles SS
Grignard successes and failures
I have a good experience on Grignard reactions and i have to say there is no need for use high purit ...
18-2-2016 at 23:18
by: Waffles SS
2,5-dihydroxycinnamic acid
[align=center][img]https://upload.wikimedia.org/wikipedia/commons/thumb/1/1a/2%2C5-Dihydroxycinnamic ...
5-2-2016 at 07:32
by: Waffles SS
keten lamp
Thanks Praxichys,

I used 2.5mm diameter Ni/Cr wire and i built this system according to Vogel Ket ...
5-1-2016 at 09:34
by: Waffles SS
keten lamp
My old Facilities for making Keten by Furnace (6 years ago):

[file]46955[/file]
[file]46957[/fi ...
4-1-2016 at 11:15
by: Waffles SS
MEK---->DEK Conversion?
[rquote=432885&tid=64765&author=MeshPL]

2. Turn propanoic acid into calcium propionate, p ...
26-12-2015 at 10:33
by: Waffles SS
Gelling agents
Yes,
I found out kraton 1650 is answer and i am using it
5-12-2015 at 10:45
by: Waffles SS
ethylene oxide

https://www.youtube.com/watch?v=bKiXxoRZ_VQ

http://www.sciencemadness.org/talk/viewthread.php?t ...
16-11-2015 at 21:32
by: Waffles SS
ethylene oxide
I did some reaction with EO.That is really nasty and dangerous stuff(be careful)

I attached reaxy ...
14-11-2015 at 19:57
by: Waffles SS
P2P from recycled styrene?
Reaxys search of all possible ways for synthesis Phenylacetone (P2P)
(Please don use it for illegal ...
1-11-2015 at 08:50
by: Waffles SS
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