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Acetaldehyde synthesis
I gave the acetaldehyde synthesis a try today. I hooked up an apparatus which consisted of a flask ...
26-6-2004 at 11:30
by: Mendeleev
Phenylacetone synthesis?
Damn, sorry again about the double post, but my personal preference would have been the hydrolysis o ...
24-6-2004 at 17:56
by: Mendeleev
Phenylacetone synthesis?
http://www.rhodium.ws/chemistry/phenylacetone.html

This should cover most of them.
24-6-2004 at 17:54
by: Mendeleev
Battery acid
My acid also turns yellowish, but it is only a slight tinge and it goes away once it cools down, it ...
24-6-2004 at 07:02
by: Mendeleev
Good way to Methylamine HCl?
Sorry for double postin everyone, I am on an old computer with an old browser and everything is very ...
23-6-2004 at 14:32
by: Mendeleev
Good way to Methylamine HCl?
I was wondering if the formaldehyde and ammonium chloride method could be done with lower concentrat ...
23-6-2004 at 07:23
by: Mendeleev
aromatic sidechainchlorinations - Toluene - Benzylchloride, Benzalchloride, Benzotrichloride and followup reactions yielding Ben
According to this link:

http://www.intox.org/databank/documents/chemical/calchypo/cie100.htm

b ...
22-6-2004 at 12:11
by: Mendeleev
aromatic sidechainchlorinations - Toluene - Benzylchloride, Benzalchloride, Benzotrichloride and followup reactions yielding Ben
Here's the patent, straight from the hive.



Be it known that I, CHAUNCEY C. Loomis, a cit ...
21-6-2004 at 12:38
by: Mendeleev
aromatic sidechainchlorinations - Toluene - Benzylchloride, Benzalchloride, Benzotrichloride and followup reactions yielding Ben
This is a nightmare, I went through 15 US pool suppliers and 3 UK suppliers, and the highest they ha ...
20-6-2004 at 15:25
by: Mendeleev
Acetaldehyde synthesis
Madscientist, you stated you managed to get 60 mL of liquid once you began to effectively cool the d ...
19-6-2004 at 11:49
by: Mendeleev
Dichloromethane from methanol?
Well here's an MSDS for KS3 paint remover, around 80-85% DCM.
19-6-2004 at 11:21
by: Mendeleev
aromatic sidechainchlorinations - Toluene - Benzylchloride, Benzalchloride, Benzotrichloride and followup reactions yielding Ben
My goal is neither benzal chloride nor benzaldehyde, at the moment, right now I am trying to get ben ...
19-6-2004 at 09:31
by: Mendeleev
aromatic sidechainchlorinations - Toluene - Benzylchloride, Benzalchloride, Benzotrichloride and followup reactions yielding Ben
I downloaded Vogel's Third Edition in pdf, it is my holy book now. I also realized the passage ...
18-6-2004 at 20:55
by: Mendeleev
Dichloromethane from methanol?
This is probably less relevant to the author of this thread as he lives in Great Britain, and most l ...
18-6-2004 at 09:35
by: Mendeleev
Zn from US pennies
The HCl will not do anything to the copper, it will react with the zinc however. It's a great ...
17-6-2004 at 13:52
by: Mendeleev
aromatic sidechainchlorinations - Toluene - Benzylchloride, Benzalchloride, Benzotrichloride and followup reactions yielding Ben
I did provide a direct link, see my first post in this thread :).
15-6-2004 at 17:18
by: Mendeleev
aromatic sidechainchlorinations - Toluene - Benzylchloride, Benzalchloride, Benzotrichloride and followup reactions yielding Ben
Just to clarify my earlier post, I found out that equal masses of toluene and calcium hypochlorite a ...
15-6-2004 at 06:59
by: Mendeleev
Ethyl ether distillation and synthesis
Hooray, it was 35, that's high enough to make me feel comfortable. Do you not have dry ice in ...
14-6-2004 at 11:51
by: Mendeleev
Experiements
The fog is from the CO2 boiling off more rapidly in water than in air, that comment was independent ...
14-6-2004 at 10:25
by: Mendeleev
Experiements
Well this depends on what you mean by "basic". Basic can either mean safe, easy, legal, a ...
13-6-2004 at 22:13
by: Mendeleev
Ethyl ether distillation and synthesis
I have some flasks, rubber stoppers, plastic hosing, and a liebig condenser, so I do have a distilla ...
13-6-2004 at 21:28
by: Mendeleev
Ethyl ether distillation and synthesis
Ether can also be bought as engine starting fluid. It's about 60-70% ethyl ether, 5% CO2 and t ...
13-6-2004 at 17:44
by: Mendeleev
"controlled substances & "listed" subtances
See, the difference in our thinking is you are conducting analytical experiments, I am producing sub ...
13-6-2004 at 14:07
by: Mendeleev
aromatic sidechainchlorinations - Toluene - Benzylchloride, Benzalchloride, Benzotrichloride and followup reactions yielding Ben
What is the ftp address, I couldn't find a link or the actaul address anywhere on the forum des ...
13-6-2004 at 09:22
by: Mendeleev
"controlled substances & "listed" subtances
Well, the chemicals may or may not be watched, but they are not listed, which means I could order 8 ...
12-6-2004 at 22:15
by: Mendeleev
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