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Friedel-Crafts acylation
I recently made acetophenone using the procedure in Vogel’s 3rd (forum library). Vogel stated tha ...
4-8-2015 at 16:10
by: Magpie
HELP! Vacuum distillation!
With normal chemical glassware you can't expect to not have some leakage. For most vacuum distillati ...
4-8-2015 at 13:41
by: Magpie
HELP! Vacuum distillation!
What is the thermometer measuring, ie, where is the thermometer bulb located?

[Edited on 4-8-2015 b ...
4-8-2015 at 11:45
by: Magpie
Hydrazine
Using the Hofmann degradation process at the 36g batch size I have no foaming problem. I use a 1L s ...
4-8-2015 at 08:26
by: Magpie
mystery writer has cyanide question
[rquote=414573&tid=63198&author=diggafromdover] We need a murder and morbidity forum!
[/rqu ...
3-8-2015 at 14:41
by: Magpie
mystery writer has cyanide question
As a side note I remember watching an Agatha Christie murder mystery on TV. Cyanide (can't remember ...
3-8-2015 at 12:24
by: Magpie
mystery writer has cyanide question
nell, I like the storyline of your novel. The little old lady is simply making use of common food t ...
3-8-2015 at 08:30
by: Magpie
Good Chemical Respirator for Home Labs?
If you do organic syntheses you will use and appreciate all that space. My hood is barely tall enou ...
29-7-2015 at 12:50
by: Magpie
Good Chemical Respirator for Home Labs?
A new single hung window with a rough opening of 4 foot x 5 ft is going to cost more than a few doll ...
28-7-2015 at 07:45
by: Magpie
Good Chemical Respirator for Home Labs?
[rquote=413847&tid=61807&author=gatosgr]Looks like a nice fume hood magpie, what are the di ...
27-7-2015 at 13:05
by: Magpie
Hydrazine
I have used the chloramine process and the Hofmann degradation process to produce hydrazine. This i ...
27-7-2015 at 08:54
by: Magpie
Good Chemical Respirator for Home Labs?
[rquote=413678&tid=61807&author=gatosgr]
Where is it? I will try to build a fume hood my o ...
26-7-2015 at 15:25
by: Magpie
Quantum Mechanics/Wave Mechanics in Chemistry Beginners Thread
Can electron spin be described in classical terms? If not, what is it other than -1/2 or +1/2?
26-7-2015 at 08:59
by: Magpie
Good Chemical Respirator for Home Labs?
[rquote=413496&tid=61807&author=zed]
A good hood is nice. Though usually at some window p ...
24-7-2015 at 18:17
by: Magpie
Preparation of Hydrazine Sulfate (Hofmann Degradation)
Here's pictures of the hydrazine sulfate I made yesterday. The pictures show the product before and ...
23-7-2015 at 19:31
by: Magpie
Name that rock
Are you drunk?
23-7-2015 at 15:19
by: Magpie
Name that rock
chalcopyrite?
23-7-2015 at 14:43
by: Magpie
benzyl alcohol oxidation
Very nice! You folks really took the time to investigate the nuances of this synthesis.

How did ...
23-7-2015 at 10:48
by: Magpie
More Ghetto Glassware
Don't forget the Ronco glass cutter from Ron Popeil. He also gave us the Vegamatic and the Pocket F ...
22-7-2015 at 21:08
by: Magpie
Preparation of Hydrazine Sulfate (Hofmann Degradation)
I'm preparing to make some hydrazine sulfate.

To do this I bought a fresh gallon of 13.5% swimmin ...
20-7-2015 at 11:00
by: Magpie
Phosphorus halides from phosphine
Hot phosphine self-ignites in atmospheric air producing a loud "pop."- I know this by experience whe ...
20-7-2015 at 10:44
by: Magpie
Phosphorus halides from phosphine
You are planning to generate three gas streams simultaneously, regulating flow of each to obtain the ...
20-7-2015 at 09:15
by: Magpie
Name that rock
Slate it is. It is from a lakeshore beach of slate pieces about that size. Nothing but slate piece ...
19-7-2015 at 14:51
by: Magpie
Name that rock
Here's an easy one for you:



[file]41976[/file]
19-7-2015 at 12:27
by: Magpie
Searching for large glassware
[rquote=412679&tid=62928&author=aga]
You tend not to see any industrial sites with 200,000 ...
18-7-2015 at 13:51
by: Magpie
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