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Preparation of anhydrous AlCl3 in DCM - photos
[rquote=181741&tid=14111&author=blogfast25]You should be able to leach out any FeCl3 with dr ...
6-7-2010 at 10:56
by: peach
Acetic anhydride preparation
Teflon is an idea. I was just wondering about DIY'ing my own HF distillation setup using some.

I ...
6-7-2010 at 06:45
by: peach
Temperature controller for an Ikamag hotplate?
The mantle idea is excellent! I'd be willing to help out with that, sourcing cheap components and ch ...
6-7-2010 at 06:18
by: peach
Laser-Diode based Raman Spectroscopy
You could have the the higher power components run from an on board power supply, powered by the USB ...
5-7-2010 at 19:01
by: peach
Low-Pressure Gas @ home
First of all, go to google and type in "hcl gas generators clandestine".

Read the whole document. ...
5-7-2010 at 18:06
by: peach
Gas-phase apparatus construction
Have you ever taken a good lungful of rich HCl(g)? How doest ketene comparuth?
5-7-2010 at 17:16
by: peach
Temperature controller for an Ikamag hotplate?
I think you're probably right.

And I KNOW that IKA is run by a bunch of annoying turds.

Their ...
5-7-2010 at 16:20
by: peach
troubleshooting a homemade hotplate
[edit: I'm glad to see you're using a transformer; providing an isolated floating voltage. I expect ...
5-7-2010 at 16:07
by: peach
Who makes Quickfit?
Good find, noise!

And that's the same site that's linked to from the pyrex.com site for their EU ...
5-7-2010 at 15:30
by: peach
Preparation of anhydrous AlCl3 in DCM - photos
[every post needs a photo]

[rquote=181667&tid=14111&author=Sedit]Next time add abit of ac ...
5-7-2010 at 14:31
by: peach
Preparation of anhydrous AlCl3 in DCM - photos
[edit: if the videos say "daily download limit reached" please let me know and don't worry, they're ...
5-7-2010 at 07:01
by: peach
Who makes Quickfit?
Thanks undead, although Quickfit specifically states 'Made in England' on the glass. Pyrex.com is st ...
5-7-2010 at 06:03
by: peach
Acetic anhydride preparation
[rquote=181518&tid=9&author=densest]"call for quote" = you can't afford it, you peasant... I ...
3-7-2010 at 16:33
by: peach
Bad Chemistry on TV
Given how many people think Ecstasy pills have heroin and rat poison in them, it's probably working. ...
3-7-2010 at 16:16
by: peach
ChemicalsRUs and KaiChem buying
Yep... I2 and red phosphorus on one site with little else = meth cooks

You know that recipe is fr ...
3-7-2010 at 16:08
by: peach
Who makes Quickfit?
I read an article that says the same. But if I visit the Bibby Sterilin site, there doesn't seem to ...
3-7-2010 at 14:28
by: peach
troubleshooting a homemade hotplate
Right, that's nowhere near enough watts. My hotplate is double that and it's element is attached to ...
3-7-2010 at 14:10
by: peach
Police notified about buying beakers!
Don't worry hissingnoise, that was after two decades of putting up with entirely random, literally p ...
3-7-2010 at 13:48
by: peach
Gas-phase apparatus construction
You don't need a fume hood if you select scrubbers / washes properly. Use a wash, after the one for ...
2-7-2010 at 13:56
by: peach
Acetic anhydride preparation
[b]Watson[/b]
Thanks for the explanation, things like carbon are also incredibly important with ste ...
2-7-2010 at 11:43
by: peach
troubleshooting a homemade hotplate
Good point tumadre, cement is relatively caustic.

The non-porous stuff you're talking about would ...
2-7-2010 at 09:57
by: peach
Who makes Quickfit?
I did some more UTFSE and realized Pyrex has their own site, that they're responsible for Quickfit a ...
2-7-2010 at 06:32
by: peach
Who makes Quickfit?
I see the name all the time on glassware, and then discovered it's actually a brand, not a descripti ...
2-7-2010 at 06:28
by: peach
Nitromethane extraction
[rquote=180837&tid=13408&author=not_important]
Given the existence of a low boiling azeotro ...
2-7-2010 at 06:22
by: peach
troubleshooting a homemade hotplate
I think you're loosing too much heat through radiation / convection / conduction. And the heat gener ...
2-7-2010 at 05:37
by: peach
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