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Table salt heating bath?
[rquote=433779&tid=64841&author=DraconicAcid]
Molten aluminum in water??? Sounds like a ve ...
2-1-2016 at 12:44
by: blogfast25
Synthesis of longer chain tertiary alcohols
[rquote=433769&tid=15171&author=aga]

[b]I.[/b] Distilling the upper layer from the post-r ...
2-1-2016 at 12:42
by: blogfast25
Prediction of chemical reaction
[rquote=433751&tid=64878&author=Doyle3694]Are there any rules at all or is it simply a case ...
2-1-2016 at 08:55
by: blogfast25
Prediction of chemical reaction
[rquote=433749&tid=64878&author=MolecularWorld]Or add sufficient sodium carbonate to react w ...
2-1-2016 at 08:49
by: blogfast25
Prediction of chemical reaction
[rquote=433734&tid=64878&author=Doyle3694]

I have a passionate interest in chemistry and ...
2-1-2016 at 07:53
by: blogfast25
Synthesis of longer chain tertiary alcohols
[rquote=433688&tid=15171&author=aga]
The Upper phase that separated after the reflux Must b ...
1-1-2016 at 18:08
by: blogfast25
Synthesis of longer chain tertiary alcohols
A teensie bit disappointing, this crystals-no-show.

I suggest to pool all organic phases together ...
1-1-2016 at 14:29
by: blogfast25
Extraction of fumaric acid
Crush the tablets and make a thin slurry with water.

Treat with strong ammonia. This will give hi ...
31-12-2015 at 18:05
by: blogfast25
Synthesis of longer chain tertiary alcohols
[rquote=433563&tid=15171&author=aga]Bad news : the crystals have buggered off.

Do they de ...
31-12-2015 at 11:22
by: blogfast25
Synthesis of longer chain tertiary alcohols
[rquote=433541&tid=15171&author=aga]There are some crystals this morning.

Not all of the ...
31-12-2015 at 06:06
by: blogfast25
Synthesis of longer chain tertiary alcohols
[rquote=433478&tid=15171&author=aga]
I like trees, and will enjoy going to have a look at i ...
30-12-2015 at 16:45
by: blogfast25
Synthesis of longer chain tertiary alcohols
[rquote=433480&tid=15171&author=gdflp]Indeed, since the reaction will happen at RT, you migh ...
30-12-2015 at 16:37
by: blogfast25
Synthesis of longer chain tertiary alcohols
@gdflp:

What I might try is to treat my commercial isomeric terpineol mixture with 20 % HCl at RT ...
30-12-2015 at 16:12
by: blogfast25
Synthesis of longer chain tertiary alcohols
[rquote=433454&tid=15171&author=aga]Think i'll go and have a word with a pine tree in the mo ...
30-12-2015 at 16:01
by: blogfast25
Purple floating liquid on CuCO3?
[rquote=433460&tid=64846&author=Boffis]There are several normal double carbonates of copper ...
30-12-2015 at 15:55
by: blogfast25
Esterification of a t-alcohol (carbinol) with benzoyl chloride
(I think ;))

[file]46820[/file]

The question is, how [i]selective[/i] would such an esterif ...
30-12-2015 at 13:44
by: blogfast25
Synthesis of longer chain tertiary alcohols
[rquote=433390&tid=15171&author=gdflp]Blogfast, it sounds as though the mixed isomers in you ...
30-12-2015 at 11:12
by: blogfast25
Synthesis of longer chain tertiary alcohols
[rquote=433383&tid=15171&author=aga]As we already have a separation of two phases, surely th ...
30-12-2015 at 11:11
by: blogfast25
Synthesis of longer chain tertiary alcohols
[rquote=433381&tid=15171&author=aga]We got 185ml of post-reflux mixture which has a clear up ...
30-12-2015 at 09:46
by: blogfast25
Synthesis of longer chain tertiary alcohols
Nice work.

I is a tizzy cornfused now. By rights we should have 10 to 20 ml of organic phase now, ...
30-12-2015 at 09:20
by: blogfast25
Synthesis of longer chain tertiary alcohols
aga:

What happened to the rest of the 310 ml of post-reflux mixture? That contains about half of ...
30-12-2015 at 08:07
by: blogfast25
Synthesis of longer chain tertiary alcohols
Awaitng progress report in Real Time. :D
30-12-2015 at 07:03
by: blogfast25
Purple floating liquid on CuCO3?
[rquote=433354&tid=64846&author=MolecularWorld]Remarkable.

[/rquote]

No.

Many know ...
30-12-2015 at 06:06
by: blogfast25
Purple floating liquid on CuCO3?
[rquote=433333&tid=64846&author=Copper]It's the standard NaHCO3 and CuSO4 precipitation. [/r ...
29-12-2015 at 19:42
by: blogfast25
Purple floating liquid on CuCO3?
You need to describe your synthesis first. W/o it no one can make any significant pronouncements re. ...
29-12-2015 at 19:23
by: blogfast25
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