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lithium and what to do with it
In fact there is a funny story to go along with this actually, I went back to visit my old highschoo ...
15-12-2010 at 11:30
by: ThatchemistKid
lithium and what to do with it
No, I am quite certain I was getting chunks of potassium and sodium, Actually I have pictures stored ...
15-12-2010 at 11:24
by: ThatchemistKid
lithium and what to do with it
I have previously, back a couple of years ago, been able to thermite sodium, potassium and calcium o ...
14-12-2010 at 22:05
by: ThatchemistKid
lithium and what to do with it
Lithium is not the most reactive, in the sense that it does not react the fastest or most vigorously ...
14-12-2010 at 20:43
by: ThatchemistKid
nitromethane purity for ANNM compositions
Distillation will work I think, but there is an azetrope of nitromethane and methanol that you might ...
4-12-2010 at 11:22
by: ThatchemistKid
Copper Chloride question
CuCl is a white solid not a brown solid and it rather quickly in moist air gets oxidized to Cu2+ con ...
27-11-2010 at 09:40
by: ThatchemistKid
Lithium polymer disassembling
You should probably becarful with LiPO batteries as the electrolyte consists of a compound that deco ...
7-11-2010 at 20:24
by: ThatchemistKid
magnetic field's effect on triplet state transitions
Today in class (Quantum Mechanics) we were discussing singlet and triplet state transitions in multi ...
22-10-2010 at 19:48
by: ThatchemistKid
Catechol preparation
Note by common and accessible I meant to the home amature XD

although I do know that the synthesi ...
15-10-2010 at 08:05
by: ThatchemistKid
Catechol preparation
Well is there a milder reducing that will take the ester only to the aldehyde?

hopefully ones th ...
14-10-2010 at 22:38
by: ThatchemistKid
Catechol preparation
well.. wait a moment that is counter productive.. can the bouvealt-blanc reduction not be adjusted t ...
13-10-2010 at 16:17
by: ThatchemistKid
Catechol preparation
"subsequent Dakin reaction" after oxidation to the aldehyde...
yes yes.. sorry
I agree

sorry i ...
13-10-2010 at 16:04
by: ThatchemistKid
Catechol preparation
Here is the reference to a paper about the reaction.. it mentions that aromatics are not reduced and ...
13-10-2010 at 13:19
by: ThatchemistKid
Catechol preparation
I have thought about making catechol myself from methyl salicylate using the Bouveault Blanc reduct ...
13-10-2010 at 13:02
by: ThatchemistKid
acetamidine hydrochloride preparation procedure
Well, there is a relatively simple procedure directly on orgsyn.org

http://www.orgsyn.org/orgsyn/ ...
19-8-2010 at 07:45
by: ThatchemistKid
Easiest homebrew of methyl mercaptan
Also to catch the hydrogen sulphide as it is being formed you may bubble it through a hypochlorite s ...
17-8-2010 at 19:54
by: ThatchemistKid
Easiest homebrew of methyl mercaptan
Well, the easiest way for making mercaptans that I have come up with gives you about 50% or 60% yiel ...
17-8-2010 at 19:43
by: ThatchemistKid
Pictures of your home lab
mmm sounds nice if I ever get around to buying those sensors or you ever get around to finishing the ...
22-7-2010 at 17:48
by: ThatchemistKid
Metal alkoxide to ether
The process you are describing is
called williamson ether synthesis
http://en.wikipedia.org/wiki/ ...
22-7-2010 at 17:33
by: ThatchemistKid
Pictures of your home lab
well i found some very nicely white or black (cant decide) tile 8 inch squares I think it was for 40 ...
22-7-2010 at 12:37
by: ThatchemistKid
Pictures of your home lab
uhhm that vacuum pump was 79 dollars actually, it works very well. In terms of a trap I use the pump ...
22-7-2010 at 12:03
by: ThatchemistKid
Pictures of your home lab
Ok I figured it out so here are the last couple of pictures

[file]10957[/file]

[file]10959[ ...
22-7-2010 at 07:47
by: ThatchemistKid
My little lab
Hello here are a few pics of my little lab, it is situated in a garage :D

a view of the messy lab ...
22-7-2010 at 07:44
by: ThatchemistKid
Reduction of Vanillin via Zn/AcOH problem
WOW!,... Im going to go study some more because it seem to me that I am way behind !!, I knew about ...
5-6-2010 at 18:35
by: ThatchemistKid
Testing phase-transfer catalysts.
I have read that 18-crown-6 ether specifically chelates the potassium ion and has been used to make ...
4-6-2010 at 21:01
by: ThatchemistKid
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