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Alibaba [rquote=656170&tid=157141&author=Fyndium]A question just out of curiosity, how often do you ... |
7-8-2021 at 19:06 by: Monoamine |
Alibaba I've ordered from companies in China several times now, and so far my experience has been very good. ... |
7-8-2021 at 19:00 by: Monoamine |
Thionly chloride from batteries
[file]89716[/file] |
7-8-2021 at 18:37 by: Monoamine |
Extraction and crude purification notes and procedure Ok, so I finally got around to cracking some of these batteries open to try to get some SOCl[sub]2[/ ... |
7-8-2021 at 18:21 by: Monoamine |
Protection of the the indole nitrogen I've been thinking about this a bit more lately, and I'm starting to suspect that the nitrogen in th ... |
7-8-2021 at 07:36 by: Monoamine |
Protecting groups for tertiary amines [rquote=662983&tid=157678&author=EverythingAl2O3]Is there anything stopping you from doing a ... |
7-8-2021 at 07:20 by: Monoamine |
Protecting groups for tertiary amines [rquote=663131&tid=157678&author=clearly_not_atara][rquote=662990&tid=157678&author= ... |
30-7-2021 at 18:13 by: Monoamine |
This seems like a pretty straight forward way to make acetal protected amines This may be a bit late, but it seems pretty useful, so I'll post this here anyay:
[file]89605[/f ... |
30-7-2021 at 18:04 by: Monoamine |
Thionly chloride from batteries Also, I came across a chemical vendor in India who sells SOCl2 and seems quite legit. In my experien ... |
30-7-2021 at 17:19 by: Monoamine |
Thionly chloride from batteries Interesting! And yes, definitely want to be careful with the lithium, although considering that not ... |
30-7-2021 at 17:16 by: Monoamine |
Replacing halogen by hydrogen Ah cool, Grignard may be the way to go then. Thanks for the tip!
Basically, I was hoping to make ... |
30-7-2021 at 17:05 by: Monoamine |
Replacing halogen by hydrogen I've been looking far and wide for a method to perform the following reaction:
R-O-CH[sub]2[/sub] ... |
30-7-2021 at 13:55 by: Monoamine |
Quenching excess H2 in a reaction. Following an earlier post for the catalytic preparation of NaH at room temperature.
The think is ... |
30-7-2021 at 04:38 by: Monoamine |
Electrophilic chlorination [rquote=663132&tid=157734&author=clearly_not_atara]I'm not convinced that aldimino/ketimino ... |
21-7-2021 at 14:09 by: Monoamine |
FeBr3 from Fe [rquote=108453&tid=9323&author=Klute]I decided on using the 37% just because it was closer a ... |
21-7-2021 at 13:42 by: Monoamine |
FeBr3 from Fe Once you have some Br[sub]2[/sub], couldn't you just dry it by washing it with concentrated sulfuric ... |
21-7-2021 at 13:33 by: Monoamine |
Electrophilic chlorination [rquote=663119&tid=157734&author=clearly_not_atara]Snap back to reality: [i]why[/i] are you ... |
20-7-2021 at 19:23 by: Monoamine |
Electrophilic chlorination
[rquote=663104&tid=157734&author=Monoamine]
PS:[b]An even more important question (and ma ... |
20-7-2021 at 15:41 by: Monoamine |
Possible recipe to do this: Ok, so I thought about it a bit, and I think that it may be possible to do like this:
I tried to ... |
20-7-2021 at 15:22 by: Monoamine |
Electrophilic chlorination So I'm starting to draw up all the prerequisites for a planned electrophilic chlorination off an aro ... |
20-7-2021 at 13:45 by: Monoamine |
Protecting groups for tertiary amines [rquote=662985&tid=157678&author=njl]Or deprotonate and perform William ether synthesis[/rqu ... |
20-7-2021 at 09:51 by: Monoamine |
Protecting groups for tertiary amines [rquote=662526&tid=157678&author=karlosĀ³]Boil it in ethanolamine to dequaternise.[/rquote]
... |
20-7-2021 at 09:46 by: Monoamine |
Another possible way to for protection: Just saw this: (https://www.organic-chemistry.org/protectivegroups/amino/toluenesulfonamides.htm).
... |
11-7-2021 at 20:21 by: Monoamine |
Protecting groups for tertiary amines [rquote=662544&tid=157678&author=Jenks][rquote=662537&tid=157678&author=Monoamine][r ... |
11-7-2021 at 20:04 by: Monoamine |
Answer: According to this product safety sheet
([url=https://ehslegacy.unr.edu/msdsfiles/23752.pdf]Zn-H ... |
11-7-2021 at 18:17 by: Monoamine |
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