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Lead powder
Hi,
I will try the PbO test, to be sure of its composition.
I think the lead may have contained an ...
11-2-2005 at 04:52
by: CycloKnight
Cinnamon experiment #2 results
Steam distillation has now been completed.

This is the mixture before I resumed the steam distill ...
10-2-2005 at 13:58
by: CycloKnight
Cinnamon experiment #2, update
I refluxed the mixture for 12 hours straight.
I started the reflux yesterday at 20:00,
and I swit ...
9-2-2005 at 14:01
by: CycloKnight
PbO
I know an easy way to make quite a fair amount of lead oxide, provided you have decent ventillation. ...
9-2-2005 at 10:15
by: CycloKnight
Update
This is just an update on the reaction I started this evening.

Chemical used:

~430g Cinnamon ...
8-2-2005 at 12:48
by: CycloKnight
Mass Production
For mass production of benzaldehyde from toluene, the air oxidation of toluene isn't so bad.
...
8-2-2005 at 09:23
by: CycloKnight
Benzaldehyde
If all goes well, I should have the last batch of cinnamaldehyde (to benza.)started this evening.
...
8-2-2005 at 06:44
by: CycloKnight
Increasing yield..
It would be good if it were possible to extract the benzaldehyde out as it forms, it would certainly ...
7-2-2005 at 14:49
by: CycloKnight
Benzaldehyde
Thanks for the compliments, I really enjoyed taking the pictures, I'll try to take more of futu ...
7-2-2005 at 06:20
by: CycloKnight
Extraction of psychoactive material from cannabis
I've carried out the soxhlet extraction of the psychoactive ingredients of cannabis at least a ...
7-2-2005 at 05:08
by: CycloKnight
Cinnamon experiment complete
Fractional distillation of the crude product has now been completed.
The fractional distillation wa ...
6-2-2005 at 14:26
by: CycloKnight
Manganese-Ammonium cell images
"You tell me man, I only work here." - Hudson, Aliens
[img]http://www.sciencemadness.org ...
5-2-2005 at 19:16
by: CycloKnight
Cinnamon oil experiment update.
The cinnamon oil to benzaldehyde conversion experiment is not yet complete.
So far I have extracted ...
5-2-2005 at 12:46
by: CycloKnight
Benzaldehyde from Cinnamon Oil.
Okay, this is my latest experiment, and let me say - it truly works wonders.
If you are looking fo ...
3-2-2005 at 14:38
by: CycloKnight
Benzaldehyde
Toluene oxidation...
Take 3.

Okay, regeneration is nearly complete.
[img]http://www.sciencemadn ...
3-2-2005 at 13:37
by: CycloKnight
toluene --> benzaldehyde
For the manganese-ammonium sulphate mixture, the ingredients I have used are based on the patent rat ...
1-2-2005 at 12:30
by: CycloKnight
toluene --> benzaldehyde
Okay, I did another run last night and it was a success. However, it was only a partial run.
I esti ...
1-2-2005 at 01:29
by: CycloKnight
Yield
Okay, I would just like to say that the yield was a little on the low side, however please take the ...
29-1-2005 at 15:30
by: CycloKnight
Manganese ammonium alum cell
Okay, as promised here is my photo essay of the mananese-ammonium alum cell, which can be used for t ...
29-1-2005 at 14:58
by: CycloKnight
Sassafras Albidum
Sold by Sandeman Seeds.

http://www.sandemanseeds.com/acatalog/Trees_S.html
28-1-2005 at 13:23
by: CycloKnight
toluene --> benzaldehyde
{img}http://www.sciencemadness.org/scipics/anode.jpg{/img}

[Edited on 29-1-2005 by CycloKnight]
27-1-2005 at 13:48
by: CycloKnight
Electric benzaldehyde
Yes, i agree that there is a vast excess of oxidant. Though, it is perfectly regenerable and not too ...
26-1-2005 at 06:39
by: CycloKnight
Benzaldehyde via Cl2/toluene
Hi folks,
what follows is some discouragement for the Cl2/toluene method and then a procedure for m ...
26-1-2005 at 04:56
by: CycloKnight
Nitrite
That is very informative, thanks Polverone. That is indeed the information I'm looking for. In ...
26-1-2005 at 03:20
by: CycloKnight
Sodium or potasium nitrite
Is there a reliable process for converting the nitrate into the nitrite using heat?
I recall using ...
25-1-2005 at 07:54
by: CycloKnight
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