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5-Bromoindole preparation
I cant think of all the indole i have readily, and just seem unable to put an acetyl-group on the ni ... |
23-3-2015 at 10:00
by: karlos³ |
5-Bromoindole preparation
LiAlH4 Reduction leaves the Bromine atom untouched, and i think Red-Al will too.
Ive worked with ... |
22-3-2015 at 22:23
by: karlos³ |
5-Bromoindole preparation
[quote]Fischer and indole bromination are still top contenders.[/quote]
I am currently mostly int ... |
22-3-2015 at 10:34
by: karlos³ |
5-Bromoindole preparation
Yeah Im looking into it right now... I guess their use of Pd/C was the cause for the dehalogenation ... |
21-3-2015 at 19:10
by: karlos³ |
5-Bromoindole preparation
Well ive seen the report somebody sent to Halmilton Morris from Vice on 5-Bromo-DMT which personal d ... |
21-3-2015 at 16:04
by: karlos³ |
5-Bromoindole preparation
[rquote=397791&tid=61802&author=CuReUS]
could Zn/Hg or Al/Hg in conc HCl be used instead of ... |
21-3-2015 at 12:51
by: karlos³ |
5-Bromoindole preparation
Thank you CuReUS, stupid me forgot that theres a Orgsyn preparation for 3-halogenation of benzaldehy ... |
20-3-2015 at 04:58
by: karlos³ |
5-Bromoindole preparation
Thank you for replying!
I thought about the Fischer-Indole synthesis as well, hey, i´ve even prin ... |
19-3-2015 at 21:37
by: karlos³ |
5-Bromoindole preparation
Hello!
I would like to prepare 5-Bromoindole, and the usual procedure from Indole ive found, in mea ... |
15-3-2015 at 11:18
by: karlos³ |
Yeast reduction of Isonitrosopropiophenone
Hello Dear fellow Mad Scientists,
I´ve prepared a small quantity of Isonitrosopropiophenone, from ... |
1-3-2015 at 09:42
by: karlos³ |
First crack at biosynthing 1-hydroxy-1-phenyl-propan-2-one (l-PAC)
Way too complicated. Where´s the sodium pyruvate?
Just use peptone as nutrient source.
Can be don ... |
26-1-2015 at 10:47
by: karlos³ |
Conversion of Aldehydes to Nitriles
[rquote=298984&tid=26038&author=Rich_Insane] I am familiar with a TCCA/aq NH3 mechanism of c ... |
8-9-2013 at 02:21
by: karlos³ |
The Short Questions Thread (4)
Yes indeed, my reference use sulfuric acid as well as catalyst, forgot about the conditions needed, ... |
3-9-2013 at 04:42
by: karlos³ |
The Short Questions Thread (4)
Hello people,
I would like to know if an aromatic amide can in a one-pot reaction be halogenated to ... |
2-9-2013 at 19:47
by: karlos³ |
5-alkylbenzen-1,3-diol synthesis
It could even cleave an MeO-group on 4-, it depends on the position in this reaction...
Theres a me ... |
31-5-2013 at 16:52
by: karlos³ |
5-alkylbenzen-1,3-diol synthesis
I shouldnt have chosen this method of O-demethylation, instead a cleaner and higher yielding catalys ... |
19-5-2013 at 10:43
by: karlos³ |
5-alkylbenzen-1,3-diol synthesis
Well I finished the whole synthesis more than a half year ago and simply hadnt the time to update th ... |
18-5-2013 at 05:10
by: karlos³ |
7-bromo-2-heptanone preparation
Thank you for the input Nicodem. |
6-8-2012 at 09:57
by: karlos³ |
7-bromo-2-heptanone preparation
Hm this sucks, is there any other option to make the title compound out of 6-bromohexanoic acid? Met ... |
5-8-2012 at 13:35
by: karlos³ |
7-bromo-2-heptanone preparation
So
Tran, K.; Bickar, D. J. Org. Chem. 2006, 71, 6640–6643. (doi:10.1021/jo0607966)
my general q ... |
4-8-2012 at 10:56
by: karlos³ |
7-bromo-2-heptanone preparation
Hi!
I want to prepare the title compound, from 6-bromo hexanoic acid and acetic acid anhydride. My ... |
4-8-2012 at 07:19
by: karlos³ |
5-alkylbenzen-1,3-diol synthesis
Hello there,
time has passed and i am almost there, and yes a grignard was needed, I dont have my p ... |
3-4-2012 at 15:16
by: karlos³ |
5-alkylbenzen-1,3-diol synthesis
Hello dear mad scientist colleagues!
I was thinking of a feasible route to some 5-alkylresorcinol d ... |
16-6-2011 at 16:17
by: karlos³ |
problems with ring-closing of n-carbamoyl-phenylethanolamin
well, thank you jon this was really helpfull, i finally figured out according to your post how to ma ... |
14-6-2011 at 06:23
by: karlos³ |
successfull synthesis of 3-hexyl-5-(indol-3-yl)imidazolidin-2,4-dion
Sorry I have tried to make my references userfriendly as possible so a quick google search will give ... |
11-1-2011 at 01:05
by: karlos³ |
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