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Substitute for dioxane
[rquote=217309&tid=15239&author=DJF90]I've just checked myself what the issue is and it won' ...
29-7-2011 at 13:17
by: Nicodem
Substitute for dioxane
[rquote=217280&tid=15239&author=maxidastier]ok, then. How many grams of TsOH would you use f ...
29-7-2011 at 11:55
by: Nicodem
Synthesis of propanamide
[rquote=217281&tid=17139&author=Bitburger]
[b]SUMMARY[/b]
1) How to explain the low mp of ...
29-7-2011 at 11:38
by: Nicodem
Problem forming sugar azide
You are trying to make an SN2 on a sterically hindered mesylate/tosylate of a secondary and furtherm ...
29-7-2011 at 11:07
by: Nicodem
Benzylation of benzene with benzyl alcohol
While you wait for the DS trap, you could use your benzyl alcohol in other reactions, possibly requi ...
26-7-2011 at 10:15
by: Nicodem
Benzylation of benzene with benzyl alcohol
Perhaps the emulsion is only the consequence of polymeric crap that precipitates and prevents the dr ...
24-7-2011 at 07:18
by: Nicodem
Reduction of levulinic acid
[rquote=216443&tid=17051&author=Ninja]So, what do you think? Are there any low pressure redu ...
24-7-2011 at 07:04
by: Nicodem
how do i study
[rquote=216628&tid=17071&author=Mildronate]To my mind hardest thing in organic is mechanisms ...
24-7-2011 at 06:36
by: Nicodem
reduction of primary amides to amines with lithium aluminum hydride
Please UTFSE. The topic of post-LiAlH4 based reductions has been discussed several times already.
A ...
24-7-2011 at 06:01
by: Nicodem
Sodium ethoxide with NaOH and ethanol
[rquote=216687&tid=17074&author=Ninja]But i am interested in measuring the concentration of ...
23-7-2011 at 13:48
by: Nicodem
Analysis of methyl-chlorinated toluene
[rquote=216615&tid=17077&author=Melgar]Proton NMR is good at analyzing products, but not so ...
23-7-2011 at 13:37
by: Nicodem
Benzylation of benzene with benzyl alcohol
I would say the problem of using alcohols in the Friedel-Crafts alkylation is the water formed. Wate ...
20-7-2011 at 14:05
by: Nicodem
Help with quinoline synthesis
Also, while you have the nitrile, you can try reducing it with [url=http://www.orgsyn.org/orgsyn/org ...
20-7-2011 at 12:51
by: Nicodem
sodium borohydride to sodium triacetoxyborohydride
[rquote=216238&tid=17024&author=uchiacon]I'm interested in making a bit of sodium triacetoxy ...
20-7-2011 at 12:29
by: Nicodem
Reduction of levulinic acid
You want useful thoughts, but don't bother giving the pertaining references? No input, no output.
20-7-2011 at 12:23
by: Nicodem
Calcium peroxide preparaion
Reaction in aq. solution:
Ca<sup>2+</sup> + H<sub>2</sub>O<sub>2</ ...
20-7-2011 at 12:17
by: Nicodem
Help with quinoline synthesis
Don't be too disappointed, it was a far stretched suggestion anyway. I would be pleasantly surprised ...
18-7-2011 at 09:08
by: Nicodem
Diethylamine Synthesis
Good work!

You can derivatize your product in order to characterize them by a melting point measu ...
18-7-2011 at 08:42
by: Nicodem
Film about amateur scientist
[rquote=215823&tid=16986&author=flyingant]We are not intending to make a film for TV broadca ...
17-7-2011 at 09:49
by: Nicodem
How do you separate Paracetamol, Chlorphenamine maleate and Phenylephrine HCL
[rquote=215950&tid=16993&author=theSchoolGirl]Okay, so I could get Paracetamol thru that Col ...
15-7-2011 at 15:37
by: Nicodem
Synthesis N,N-Dimethyl tryptamine
That is an interesting article that I already encoutered in a different context, but forgot about th ...
15-7-2011 at 15:18
by: Nicodem
Synthesis N,N-Dimethyl tryptamine
[rquote=215913&tid=16425&author=fledarmus]I don't think he's talking about the methylation r ...
15-7-2011 at 08:54
by: Nicodem
Alcoholic nitrites from N2O3
N2O3 is generally considered a nonisolable compound at room temperature, though it is an equilibrium ...
15-7-2011 at 08:30
by: Nicodem
Ullmann Reaction Questions
[rquote=215501&tid=16951&author=smaerd]I'm having a hard-time finding out further informatio ...
15-7-2011 at 08:10
by: Nicodem
Synthesis N,N-Dimethyl tryptamine
[rquote=215879&tid=16425&author=sentinel097]What I'd like to know is what the underlying che ...
15-7-2011 at 07:46
by: Nicodem
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