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Can benzaldehyde be saturated with HCl?
Yes, self condensation. How will you saturate it, is HCl any soluble in it?
You will get benzoin.
20-11-2015 at 04:19
by: karlos³
Bromoacetyl Bromide
You could use PBr3 or PBr5 if you can buy this.
19-11-2015 at 22:15
by: karlos³
The Short Questions Thread (4)
Can somebody tell my if its possible to prepare mandelic acid from styrene?
I need some mandelic ac ...
12-11-2015 at 11:05
by: karlos³
Storing low bp chemicals?
If you store low boiling chemicals in the fridge, make sure its a special one for chemical storage!
...
11-11-2015 at 14:12
by: karlos³
Chromatography base substitution question
Triethylamine is not very harmful, you definitely don´t need a fume hood when you are working with ...
9-11-2015 at 12:48
by: karlos³
Thought from "Fisher esterificatioon of ethylene glycol"
One should add that 2-haloethanols are very toxic.
6-11-2015 at 14:55
by: karlos³
When Chemistry Goes Wrong
Oh I have a nice example!
Once, in the lab, whole class being there, a girl put a beaker full with ...
6-11-2015 at 06:59
by: karlos³
Thought from "Fisher esterificatioon of ethylene glycol"
Ethylene glycol is as a dialcohol not without a reason part of the polyester PET.
I guess separatio ...
4-11-2015 at 22:05
by: karlos³
What causes TMT insolubility in Isopropanol?
Its a quarternary [b]salt[/b]. Logically, salts are known to differ in solubility to their free acid ...
4-11-2015 at 08:19
by: karlos³
Theoretical Synthesis of Phosgene
As it is autumn, I have seen toadstools that big, might have been a hallucination like OP´s attempt ...
21-10-2015 at 10:46
by: karlos³
KNO3 fert production (old school) urine + straw vs grass vs leaves
This is anorganic chemistry, also without references you should post in beginnings.
20-10-2015 at 22:54
by: karlos³
Phenethanolamine synthesis is frustrating me!
Ok CuReUS, I thougt you´ve meant DMF for the Delepine, not Gabriel synthesis. Thank you for clearin ...
20-10-2015 at 09:18
by: karlos³
Phenethanolamine synthesis is frustrating me!
First of all, I would like to thank all of you for the great ideas thrown in, the useful references ...
17-10-2015 at 07:58
by: karlos³
Phenethanolamine synthesis is frustrating me!
Those contributions are very worthful, thank you all very much!

@CuReUS: Thats because benzyl alc ...
13-10-2015 at 12:40
by: karlos³
Phenethanolamine synthesis is frustrating me!
Well, certainly not in an aqueous environment, if you want to chlorinate such an alcohol, you would ...
8-10-2015 at 10:50
by: karlos³
Phenethanolamine synthesis is frustrating me!
Thank you, very informative!
So the chloride ion really comes from the chloroform, and phosgene is ...
7-10-2015 at 04:26
by: karlos³
Phenethanolamine synthesis is frustrating me!
Well, yeah hydrazine would be an idea for gabriel synthesis of phthalimide, or even HCl for the succ ...
6-10-2015 at 09:28
by: karlos³
Phenethanolamine synthesis is frustrating me!
I found this interesting paper, it gives yield and reaction times for the ammonolysis of styrene epo ...
5-10-2015 at 23:10
by: karlos³
Unknown oxidises to Benzaldehyde
He meant density probably...
If its a liquid, how much weighs a mlilli,iter what volume takes a gra ...
3-10-2015 at 14:42
by: karlos³
Phenethanolamine synthesis is frustrating me!
Related to some methadone analogue? No, not the tiniest bit.

Yes, the method for styrene epoxide ...
2-10-2015 at 08:55
by: karlos³
Phenethanolamine synthesis is frustrating me!
I used the henry reaction to obtain the nitroalcohol for p-fluorophenethanolamine, with triethylamin ...
2-10-2015 at 03:25
by: karlos³
Phenethanolamine synthesis is frustrating me!
So, I have made some 1-(4-fluoro)phenyl-2-nitroethan-1-ol, and reduced the nitroalcohol with Red-Al. ...
1-10-2015 at 12:30
by: karlos³
Phenethanolamine synthesis is frustrating me!
Yes I did use this route, MeNO2/EtNO2 with Et3N catalysis, then reduced it to the Aminoalcohol.
Fo ...
29-9-2015 at 21:03
by: karlos³
Phenethanolamine synthesis is frustrating me!
It´s an indian paper, I have problems with their general trustworthiness (is this even a word?).
B ...
26-9-2015 at 02:30
by: karlos³
Phenethanolamine synthesis is frustrating me!
Hi!
I am looking for a good synthesis of Phenethanolamine (CAS 7568-93-6), I´ve already tried to m ...
25-9-2015 at 09:50
by: karlos³
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