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Reagents for the preparation of acid chlorides: pros and cons
Nice.

Though..... some of the guys at home, have real problems obtaining red-phosphorus.

Wel ...
20-7-2016 at 16:14
by: zed
wikipedia page about Vinyl acetate
Indeed.

Entries all looks the same.

There are so many warnings, about so many materials....th ...
20-7-2016 at 15:22
by: zed
modifying a microwave for extractions
Folks sometimes use elaborate precautions to make sure errant microwaves don't escape their containm ...
19-7-2016 at 17:41
by: zed
High pressure Wacker O2 generator/RV
As I recall, the explosion took place using O2 under pressure.

I have no details. The explosion ...
19-7-2016 at 17:19
by: zed
High pressure Wacker O2 generator/RV
Ummm. The earliest personal verbal report I got on the O2-Wacker, involved an explosion.

Keeping ...
16-7-2016 at 14:08
by: zed
Ethyl Vanillin Crystallization?
Not water soluble? Might be able to steam distill it. Problem is, there might not be much of it to ...
16-7-2016 at 13:58
by: zed
Safe disposal question: Long-standing sodium in THF/Ether
Peroxide explosions pack a wallop. Equally of concern, is the ignition of the flammable solvent clo ...
12-7-2016 at 15:27
by: zed
Thermally induced racemization
Well, the premise is that once an imine/enamine is formed, the bond is capable of shifting.

If th ...
8-7-2016 at 14:40
by: zed
So I Have a Microwave.
wg48, "Pyrex" ovenware is a deceptive term. Pyrex ovenware is NOT made of borosilicate glass. Very ...
2-7-2016 at 14:58
by: zed
Black Pepper Extraction results!
I have a question about your name. I have queried several posters about the odor of Myristicinaldeh ...
2-7-2016 at 14:43
by: zed
Neutralizing NOx fumes
Aw. Fumes of that type can often be neutralized via using a mild vacuum to pull (bubble) exhaust ga ...
2-7-2016 at 14:36
by: zed
So I Have a Microwave.
An interesting point Blogfast. I microwave food in "soft" glass containers all of the time. The gl ...
30-6-2016 at 14:00
by: zed
So I Have a Microwave.
Monkeying with the innards of microwave ovens can be touchy business.

Some of the fellers on yout ...
28-6-2016 at 17:27
by: zed
Reagents for the preparation of acid chlorides: pros and cons
Some of the guys are inundated with Acetonitrile. Seems it is used as solvent in certain analytical ...
28-6-2016 at 17:09
by: zed
Reagents for the preparation of acid chlorides: pros and cons
Well, one of you clever monkeys came up with this.....AcetylChloride from Acetonitrile, AceticAcid, ...
26-6-2016 at 13:38
by: zed
Patents-flawed or followable?
Well, back in the old days, me and some of the other fellers down at the general store, usta compare ...
25-6-2016 at 13:44
by: zed
Tin corrugated roofing - % of tin and other metals present??
Though there are decorative ceiling panels, which actually MIGHT be Tin. Victorian stuff, I don't s ...
25-6-2016 at 13:03
by: zed
oily magnesium turnings
Ether didn't work well? Might try Acetone, or the cheapest of all common non-polar solvents...Gasol ...
23-6-2016 at 12:59
by: zed
Alkylation of amides
Amides can be alkylated by Alcohols, at elevated pressures and temperature. Somewhere, via the sear ...
21-6-2016 at 18:54
by: zed
Protecting metal or glass cookware from flame residue (wood fire/oil fire)
Yup! We used to rub liquid detergent on the bottoms of our campfire cooking pots, before we used ' ...
19-6-2016 at 15:53
by: zed
Extraction of benzaldehyde from imitation almond extract
Steam distillation is possible.
17-6-2016 at 16:54
by: zed
Bottling hcl gas?
Easy to make, and hard to store. In my opinion; storing is a bad idea. Not worth the trouble, and ...
17-6-2016 at 16:47
by: zed
Borohydride synth?

"Bromine is dangerous, but the reaction of a tiny amount of bromine with titanium can't be too bad ...
13-6-2016 at 13:47
by: zed
Aniline
"Isn't aniline usually prepared from nitrobenzene though? The process is pretty straight forward I b ...
6-6-2016 at 18:52
by: zed
How to download (pdf) books for free without using google search?
Copyrights and Patents, are not universally recognized. Different countries, have different laws. ...
4-6-2016 at 15:28
by: zed
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