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Fractional distillation questions
Without knowing the scale of your distillations, ie, the quantity to be distilled, your question is ...
2-3-2016 at 12:57
by: Magpie
When Chemistry Goes Wrong
Here is my solution to the failed shelf support. This was for the cabinet that has primarily equipm ...
1-3-2016 at 16:18
by: Magpie
When Chemistry Goes Wrong
For me this was "when chemical storage goes wrong."

A shelf failed in one of my two large storag ...
29-2-2016 at 08:48
by: Magpie
What is in Walgreen's Instant Cold Packs?
This may not be practical for some but I bought a 50 lb bag of urea at a weed & feed store for $ ...
29-2-2016 at 08:30
by: Magpie
n-amyl alcohol
I took the 3.4g of n-amyl alcohol and made n-amyl acetate using the procedurel in Pavia for iso-pent ...
28-2-2016 at 13:47
by: Magpie
Methanol and Nitric Acid?
[rquote=440237&tid=65433&author=ave369]
Addendum: NO2-phobia is a medical condition that pl ...
28-2-2016 at 09:40
by: Magpie
Hydrogen halides by phosphoric acids?
This is a nice discussion. I can add my experience in making HI according to the method of Argox (R ...
28-2-2016 at 09:26
by: Magpie
Camphor oxidation
As you know, camphor is a cyclic ketone. What reaction product are you expecting upon its oxidation ...
27-2-2016 at 10:21
by: Magpie
n-amyl alcohol
[rquote=440092&tid=65422&author=UC235]I find it rather interesting that every intro organic ...
26-2-2016 at 20:38
by: Magpie
n-amyl alcohol
I recently finished a protracted synthesis of n-amyl alcohol. This utilized a Grignard reaction wit ...
26-2-2016 at 17:19
by: Magpie
r/chemistry Mercilessly Crushes Sciencemadness Member
[rquote=440063&tid=65412&author=TheAlchemistPirate]
"Synthetic Chemists above all, really f ...
26-2-2016 at 16:25
by: Magpie
Grignard successes and failures
Yes, of course. I don't turn the water on prematurely for that reason. I just had no idea that is ...
26-2-2016 at 14:04
by: Magpie
Grignard successes and failures
R-MgX + H2O ---> RH + MgXOH

This not only is true for water but for any chemical with a suffic ...
26-2-2016 at 09:23
by: Magpie
Grignard successes and failures
It's an adapter, 24/40 to 19/22.

[rquote=439966&tid=65348&author=CaptainPike]
I don't im ...
25-2-2016 at 22:27
by: Magpie
electrical safety problem
As stated above, after removing the 13yr old fluorescent light I no longer have an impressed or indu ...
25-2-2016 at 15:04
by: Magpie
3-nitrophthalic acid fail (EVERY TIME)
shivam, I hope this one incident does not prevent you from further participation in this forum. May ...
25-2-2016 at 08:50
by: Magpie
alcohols test
Vogel's 3rd edition (forum library) gives some tests for alcohols. Two of them are: 1) make an acet ...
24-2-2016 at 15:56
by: Magpie
Solubility Data
Thanks! I have also bookmarked this.
24-2-2016 at 08:54
by: Magpie
Sulfur Trioxide by m-Phosphoric Acid route (success)
The chemistry of this method for making SO3 is very interesting and I'm in no way trying to discoura ...
23-2-2016 at 09:29
by: Magpie
Tour My Lab
[rquote=439548&tid=4777&author=Zephyr ]... I have a metal basin and faucet, although I still ...
22-2-2016 at 11:05
by: Magpie
Tour My Lab
Your lab is awesome! That must be a 6' hood?

Do you have a sink? If not, you will surely want o ...
21-2-2016 at 19:59
by: Magpie
electrical safety problem
This morning I measured the voltage on the hood with the light on. It was 2vac. :(

I can't specu ...
21-2-2016 at 14:55
by: Magpie
lab art
Do you ever find yourself in this situation? I do.:

[file]48257[/file]
[b]'An Alchemist at work ...
21-2-2016 at 11:55
by: Magpie
lab art
[rquote=439489&tid=65368&author=CharlieA]...it is also a room with a view!....[/rquote]

Y ...
21-2-2016 at 09:09
by: Magpie
electrical safety problem
[rquote=439467&tid=65356&author=IrC]Sounds like the ballast is not a problem but the current ...
20-2-2016 at 21:58
by: Magpie
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