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Azelaic acid
Interesting. I know azelaic acid is nonanedioic acid because I recently compiled a list of the arch ...
21-12-2019 at 12:26
by: DraconicAcid
Separation question
If you actually had such a solution, separating the various metals from each other is the basis of s ...
21-12-2019 at 12:19
by: DraconicAcid
Organic Electrochemistry Questions
[quote]1. Often I have seen in the literature the terms "constant voltage" and "constant potential" ...
21-12-2019 at 12:11
by: DraconicAcid
Trying to prepare sort of Aqua regia, but wonder if I will be fast enough before it decomposes
[rquote=628313&tid=154602&author=Abromination]If you can make nitryl chloride (and safely at ...
20-12-2019 at 16:02
by: DraconicAcid
Trying to prepare sort of Aqua regia, but wonder if I will be fast enough before it decomposes
From what I can tell, you want to generate nitryl chloride by reacting chlorine with nitrogen dioxid ...
20-12-2019 at 10:53
by: DraconicAcid
Possible easy thionyl chloride synthesis
[rquote=628176&tid=154560&author=Dan Vizine]Draconic acid, it's unique, isn't it? The smell ...
18-12-2019 at 19:45
by: DraconicAcid
Possible easy thionyl chloride synthesis
[rquote=628162&tid=154560&author=Dan Vizine]In contrast to what woelen had suggested, merely ...
18-12-2019 at 13:38
by: DraconicAcid
dcm / methanol /ammonium hydroxide
The DCM is there to dissolve the plant alkaloids.
The aqueous ammonia is there to make sure that th ...
18-12-2019 at 09:15
by: DraconicAcid
dcm / methanol /ammonium hydroxide
I'm sure the OP is referring to concentrated aqueous ammonia when he says "ammonium hydroxide". It' ...
17-12-2019 at 16:27
by: DraconicAcid
FC alkylation?
You can't acylate benzene with chloroacetone- it's not an acyl halide. You can use acetyl chloride ...
17-12-2019 at 13:01
by: DraconicAcid
FC alkylation?
I have a good prep for t-butylation of biphenyl with FeCl3 as a catalyst. You don't get over-alkyla ...
17-12-2019 at 11:48
by: DraconicAcid
Report on making Copper iodide
You can also take CuI and dissolve it in concentrated KI(aq). Keep it in a sealed vial with a small ...
15-12-2019 at 10:47
by: DraconicAcid
Magpie has died
Damn. He shall be missed.
12-12-2019 at 18:13
by: DraconicAcid
Copper disposal issues
[rquote=627700&tid=154551&author=nimgoldman]I just realised the reaction I used the copper f ...
9-12-2019 at 20:07
by: DraconicAcid
Synthesis of Hexaammine nickel II chloride
You can also add methanol to help precipitate the complex.
8-12-2019 at 16:50
by: DraconicAcid
Synthesis of Hexaammine nickel II chloride
No, ammonium chloride is not needed. Perhaps it increases the chloride concentration so that you ge ...
8-12-2019 at 12:15
by: DraconicAcid
Why can't I find amorphous P on ebay?
Since red phosphorus is a controlled substance and white phosphorus is quite dangerous, I'd be very ...
3-12-2019 at 17:26
by: DraconicAcid
Action of Nascent Hydrogen on Hypochlorite
Nascent hydrogen can reduce hypochlorite to chloride? What a discovery!

This solves all my chall ...
3-12-2019 at 12:02
by: DraconicAcid
Report on making Aluminium Iodide
Hydrated aluminum iodide is probably said to be yellow because it's almost always contaminated with ...
2-12-2019 at 06:49
by: DraconicAcid
Report on making Aluminium Iodide
I doubt the yellow colour is from reaction with moisture (since you made the compound in aqueous sol ...
1-12-2019 at 22:44
by: DraconicAcid
Pan Rescue: The Case of Burnt Oatmeal
[rquote=627253&tid=154508&author=G-Coupled]
Your username is an anagram of 'A JOKER'. [/rqu ...
1-12-2019 at 10:30
by: DraconicAcid
Pan Rescue: The Case of Burnt Oatmeal
Did you try it without the salt? Or did you just assume that it had to be there for your imagined fr ...
30-11-2019 at 17:04
by: DraconicAcid
Pan Rescue: The Case of Burnt Oatmeal
[rquote=627186&tid=154508&author=AJKOER]This is a fair comment, but my personal experience i ...
30-11-2019 at 15:19
by: DraconicAcid
Pan Rescue: The Case of Burnt Oatmeal
The carbon burnt to the bottom of the pot isn't pure carbon, but a mixture of carbon and high-carbon ...
30-11-2019 at 11:36
by: DraconicAcid
Report on attempt to make Cromium Iodide
[rquote=627143&tid=154507&author=j_sum1]This is so true that it is worth highlighting.

[r ...
29-11-2019 at 22:00
by: DraconicAcid
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