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Al acetate from Al metal and acetic acid
Infact Aluminium Triacetate lead to Aluminium hydroxide acetate hydrate in aqueous solution.it will ...
19-2-2018 at 00:36
by: Waffles SS
Al acetate from Al metal and acetic acid
Aluminium triacetateAl(O2CMe)3,can be prepared by heating AlCl3 or al powder with a mixture of aceti ...
17-2-2018 at 22:12
by: Waffles SS
Preparation of Oleum by Use of Phosphoric Acid
That is great Magpie,

If you sure that you made pure HPO3 then it should be very interesting to t ...
5-2-2018 at 06:14
by: Waffles SS
Synthesis of dopamine from catechol
I worked with glyoxylic acid for more than 3 years.i tried many method for synthesis it.(Periodate m ...
27-10-2017 at 01:39
by: Waffles SS
Synthesis of dopamine from catechol
Synthesis of 3,4-dihydroxybenzaldehyde(Protocatechuic aldehyde) from catechol
DE105798
US4165341
...
25-10-2017 at 08:23
by: Waffles SS
Acetic anhydride preparation
[rquote=495309&tid=9&author=hissingnoise][quote]It's mildly annoying to watch people spend t ...
22-10-2017 at 07:29
by: Waffles SS
Sulforaphane synthesis for the amateur
All possible way for synthesis Sulforaphane by reaxys
5-8-2017 at 00:08
by: Waffles SS
Acetic anhydride preparation

[quote]
Acetamide (0.2 mol) was dissolved in acetic acid (40 mL)and cooled in an ice bath. Then a ...
3-8-2017 at 22:05
by: Waffles SS
Acetic anhydride preparation
[rquote=489560&tid=9&author=clearly_not_atara]

Plus it might not have been fully characte ...
3-8-2017 at 11:13
by: Waffles SS
Acetic anhydride preparation
For making AcCl from Acetonitrile The only reference that i can find is this(i dont have access to r ...
3-8-2017 at 10:27
by: Waffles SS
Acetic anhydride preparation
*Even if not much of the Ac2O was consumed , all reactant and product are soluble in CH2Cl2 and this ...
2-8-2017 at 00:01
by: Waffles SS
Acetic anhydride preparation
Sulfated Zirconia method is bullshit,

Anhydride make ester in reaction of Alcohol or Diol even at ...
29-7-2017 at 19:09
by: Waffles SS
Synthesis of Indole-3-butyric acid (rooting hormone) - how difficult is this?

Reaxys search of IBA
[file]60298[/file]
15-7-2017 at 18:58
by: Waffles SS
Easy Route to Acetonedicarboxylic acid?
Thanks ronstark.
I read first reference and it seems second reference is not available online.


...
19-6-2017 at 07:01
by: Waffles SS
Easy Route to Acetonedicarboxylic acid?
[rquote=485040&tid=7546&author=ronstark]
Maybe a simple distillation or a dry one @ 175°C ...
8-6-2017 at 08:02
by: Waffles SS
Easy Route to Acetonedicarboxylic acid?

[quote]
ethyl cyanoacetoacetate ester which I presume is available via a mixed Claissen condensat ...
7-6-2017 at 12:07
by: Waffles SS
Easy Route to Acetonedicarboxylic acid?
Chemi Pharma provide interesting patent and i think making diester of citric acid is only possible b ...
7-6-2017 at 10:37
by: Waffles SS
Easy Route to Acetonedicarboxylic acid?
I dont think NaIO4 can do it.you can try oxidation by peroxomonosulphate.This method mentioned by @S ...
6-6-2017 at 07:31
by: Waffles SS
Easy Route to Acetonedicarboxylic acid?
According to reference that i provide in my last post this reaction can proceed by some route.You sh ...
6-6-2017 at 05:56
by: Waffles SS
Easy Route to Acetonedicarboxylic acid?
Oxidation of Citric acid by KMNO4/H2SO4 result different route.are you sure you got Acetonedicarboxy ...
5-6-2017 at 19:14
by: Waffles SS
What happened?
42 g of copper(II) chloride are dissolved in 100 ml of hot water containing 32 g metallic copper (gr ...
4-6-2017 at 20:51
by: Waffles SS
Effective way for synthesis of Ethyl ester of carboxylic acids
[rquote=484634&tid=74518&author=soma]I'm about to run an esterification reaction using n-ace ...
4-6-2017 at 01:35
by: Waffles SS
Acetic anhydride preparation
Theory should be true according to chemistry laws and should be logical.This thread based on logical ...
20-5-2017 at 10:36
by: Waffles SS
Acetic anhydride preparation
[rquote=483638&tid=9&author=theAngryLittleBunny]

That might be true, but luckly, succinic ...
20-5-2017 at 07:21
by: Waffles SS
Acetic anhydride preparation
[rquote=483604&tid=9&author=byko3y]Succinic anhydride dehydrates more readily than acetic ac ...
20-5-2017 at 01:22
by: Waffles SS
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