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Sulfur trioxide (SO3) misshap (and fix)
[b]It was a cold and stormy day so I decided to go outside and make some oleum...[/b]

Scroll down ...
28-11-2021 at 09:34
by: Monoamine
Mercury-free Clemmensen reduction?
[rquote=462500&tid=69602&author=Melgar]This PDF seems to claim that mercury isn't necessary ...
13-10-2021 at 18:14
by: Monoamine
Stereochemistry of the ibogaloid catharanthine
Ah got it. Thanks. I guess what confused me is that in clearsynth picture the methyl bridge from the ...
13-10-2021 at 15:28
by: Monoamine
Stereochemistry of the ibogaloid catharanthine
I got interest in catharanthine, since the non aromatic pi bond should allow for some interesting ch ...
12-10-2021 at 13:30
by: Monoamine
Alibaba
One thing I forgot to mention is that recently Alibaba has set new internal guidelines that make it ...
10-10-2021 at 18:48
by: Monoamine
Alibaba
[rquote=665436&tid=157141&author=Mush]Do buyers get bombarded with promotional stuff from ...
10-10-2021 at 18:42
by: Monoamine
Alibaba
If you need a specific chemical or reagent you can also try "chemical book". Just put in a quest for ...
10-10-2021 at 18:39
by: Monoamine
Hexamine tablet extraction - what happened?
Well, do you know if the temperature was really evenly distributed? What temperature was the hotplat ...
4-10-2021 at 16:13
by: Monoamine
Preparation of NaH from sodium metal.
[rquote=665849&tid=157640&author=walruslover69]Monoamine - is it possible that the brown/bla ...
3-10-2021 at 21:16
by: Monoamine
Preparation of NaH from sodium metal.
[rquote=665838&tid=157640&author=S.C. Wack]Sodium is melted and shaken in xylene if one want ...
3-10-2021 at 20:57
by: Monoamine
Just for fun
All this talk about beta-eliminations made me drop a small piece of Na into EtBr and cover it with p ...
2-10-2021 at 19:46
by: Monoamine
Preparation of NaH from sodium metal.
[rquote=662125&tid=157640&author=rockyit98]Sodium react with hydrogen to produce sodium hydr ...
2-10-2021 at 19:04
by: Monoamine
Preparation of NaH from sodium metal.
[rquote=662147&tid=157640&author=Bedlasky][rquote=662128&tid=157640&author=Monoamine ...
2-10-2021 at 18:57
by: Monoamine
Sodium hydride purification (NaH)
Thank you for the tip unionised! I will try that.

Also, I was looking at how Sigma sells NaH, and ...
5-9-2021 at 04:25
by: Monoamine
Sodium hydride purification (NaH)
I'm planning on trying out a NaH synthesis that was suggested to me by a member of the forum. The ad ...
4-9-2021 at 08:38
by: Monoamine
Zn-Hg amalgam safety
Oh jeez... Well, good thing I haven't dragged any on shore yet.

Does make me wonder about that s ...
25-8-2021 at 21:30
by: Monoamine
Shulgis Laboratory
Great stuff!
24-8-2021 at 12:25
by: Monoamine
Protecting groups for tertiary amines
[rquote=663424&tid=157678&author=zed]As stated previously. Under some circumstances a prote ...
13-8-2021 at 22:49
by: Monoamine
Thionly chloride from batteries
[rquote=663839&tid=157643&author=karlosĀ³]If its something corroding, that gives off HCl fum ...
10-8-2021 at 06:39
by: Monoamine
Thionly chloride from batteries
[rquote=663790&tid=157643&author=teodor]"Also, as for safety equipment, as long as you're wo ...
9-8-2021 at 16:01
by: Monoamine
Update
For the sake of safety I feel I have to give a quick update on later developments.
So, as I said, ...
9-8-2021 at 15:53
by: Monoamine
Collecting and storing gases
While some gases are cheap enough to make that it's fine to just make them as needed while others ca ...
9-8-2021 at 15:28
by: Monoamine
Thionly chloride from batteries
[rquote=663742&tid=157643&author=Prepic]Very impressive Monoamine, love to see a guide on ho ...
8-8-2021 at 10:49
by: Monoamine
What kind of gas mask should I buy for chlorine/SCl2
A military grade gas mask will do the trick. If you can find one with NATO filters then you're prett ...
8-8-2021 at 10:40
by: Monoamine
Disposal of solvents
I collect my organic waste in a gasoline can, and keep a log book so I know what I put in there.
I ...
8-8-2021 at 10:32
by: Monoamine
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