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toluene --> benzaldehyde
1 kg cinnamon oil feedstock
[img]http://www.sciencemadness.org/scipics/P4160045.JPG[/img]
Either ... |
17-4-2013 at 06:41
by: CycloKnight |
toluene --> benzaldehyde
Volumetric flask making itself useful
[img]http://www.sciencemadness.org/scipics/P4170061.JPG[/img] ... |
17-4-2013 at 06:33
by: CycloKnight |
toluene --> benzaldehyde
General setup:
[img]http://www.sciencemadness.org/scipics/P4160049.JPG[/img]
Between the free oi ... |
17-4-2013 at 06:23
by: CycloKnight |
toluene --> benzaldehyde
No problem, any and all input appreciated. 
I plan to first run through the 1 kg of oil using th ... |
16-4-2013 at 08:52
by: CycloKnight |
toluene --> benzaldehyde
Not sure what about a "peach style", but I can do a CycloKnight style retro-aldol follow up to my ea ... |
15-4-2013 at 09:58
by: CycloKnight |
toluene --> benzaldehyde
Sometime this week I'll be revisiting the cinnamon oil to benzaldehyde method utilizing insitu steam ... |
15-4-2013 at 06:29
by: CycloKnight |
toluene --> benzaldehyde
[rquote=232141&tid=2223&author=questions]I love benzaldehyde, not just for it's broad uses, ... |
17-2-2012 at 06:15
by: CycloKnight |
Manganous-Ammonium alum and derivatives for use of toluene oxidation to benzaldehyde
Nice work Hilski, lots of potential with this manganous-alum route. Great pics BTW !
This thread su ... |
13-2-2007 at 15:31
by: CycloKnight |
toluene --> benzaldehyde
[quote] CycloKnight, I don´t understand why you use a not even insulated Vigreux in your steamdisti ... |
11-8-2006 at 02:46
by: CycloKnight |
Amino alcohol via Akabori, trial run
Sorry maybe I should have explained that better.
I was only referring to aerosol carry over. Using ... |
10-8-2006 at 13:13
by: CycloKnight |
Amino alcohol via Akabori, trial run
[quote][i]Originally posted by daFlo[/i]
why using a column, when boiling off the water? the PPA is ... |
11-7-2006 at 21:24
by: CycloKnight |
Amino alcohol via Akabori, trial run
[quote][i]Originally posted by Maja[/i]
From one forum, one guy told that benzaldehyde can be repla ... |
8-7-2006 at 16:20
by: CycloKnight |
Update
The yield of PPA given in the previous reaction was no more than about 50% of the final crystallised ... |
21-6-2006 at 23:25
by: CycloKnight |
Product composition.
The freebase hasn't yet been isolated on its own in sufficient purity for a mp test. Any suggestion( ... |
10-6-2006 at 19:42
by: CycloKnight |
Blaster, nice pictures !
I recently made up a small batch of this powder, and I'm quite impressed with the results  .
The m ... |
10-6-2006 at 14:56
by: CycloKnight |
Akabori runs
........only the reports of failure that were posted a couple of years ago by somebody named 'DRIVEN ... |
10-6-2006 at 13:56
by: CycloKnight |
NI3
iirc Seymour Lecker mentions this explosive in his book "improvised explosives" as one of the 10 exp ... |
9-6-2006 at 18:07
by: CycloKnight |
Amino alcohol via Akabori, trial run
Recently I’ve been experimenting with the Akabori reaction, just curious to see if the process for ... |
8-6-2006 at 11:40
by: CycloKnight |
Acetaldehyde
There is another route to acetaldehyde that I didn't see mentioned in the posts above.
This is the ... |
7-6-2006 at 12:28
by: CycloKnight |
Cinnamon oil to benzaldehyde update.
Hi peeps, been off the forum a good while but its good to be back .
I’ve significantly impro ... |
6-6-2006 at 11:47
by: CycloKnight |
toluene --> benzaldehyde
[quote][i]Originally posted by groaner[/i]
You are certainly right there bio2. Murphy is always lur ... |
2-5-2006 at 00:40
by: CycloKnight |
Recent outage
I was beginning to fear the worst!
So, so relieved it was just temporary.
BTW, is it just me or ... |
2-3-2005 at 01:29
by: CycloKnight |
Another leap forward...
Very good work psychokitty!
I don't know how you found that, but that looks pretty darned goo ... |
13-2-2005 at 02:06
by: CycloKnight |
Not too shabby!
Well, there you have it folks - the end of chapter 1. Now go forth and be fruitful!
I would be ve ... |
11-2-2005 at 15:18
by: CycloKnight |
toluene --> benzaldehyde
Okay, this is what the mix looks like after the steam distillation.
http://www.sciencemadness.org/s ... |
11-2-2005 at 14:12
by: CycloKnight |
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