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Preparation of weak hydroiodic acid(for making NaI)
[rquote=628996&tid=154650&author=Tsjerk]Yes, that looks like there is a bit of iodine contam ...
6-1-2020 at 10:53
by: B.D.E
Preparation of weak hydroiodic acid(for making NaI)
Tsjerk & woelen, thank you for the explanation. I tried this route and I'm pretty sure it worked ...
3-1-2020 at 11:52
by: B.D.E
Preparation of weak hydroiodic acid(for making NaI)
[rquote=628729&tid=154650&author=Tellurium]Well you could also make iodine and reduce that u ...
1-1-2020 at 13:18
by: B.D.E
Golden rain experiment ruined . Did not recrystallise out on cooling
have you tried evaporating some of the water? as mentioned above, maybe it's still dissolved in solu ...
29-12-2019 at 13:44
by: B.D.E
Preparation of weak hydroiodic acid(for making NaI)
Hey there, so I need some sodium iodide for the "Finkelstein reaction".

This is what I have:
Iod ...
29-12-2019 at 08:01
by: B.D.E
Ammonium formate from Ammonium chloride
Thanks for all the tips and advices, but I'm quite happy to say that after about 2 days of slow evap ...
21-11-2019 at 11:08
by: B.D.E
Ammonium formate from Ammonium chloride
[rquote=626424&tid=154078&author=Tsjerk]Toluene will just give you a two phase system, nothi ...
19-11-2019 at 14:41
by: B.D.E
Ammonium formate from Ammonium chloride
[rquote=626411&tid=154078&author=Tsjerk]How do you generate ammonia from ammonium chloride? ...
19-11-2019 at 04:37
by: B.D.E
Ammonium formate from Ammonium chloride
[rquote=626360&tid=154078&author=mackolol][rquote=626316&tid=154078&author=B.D.E]Scr ...
18-11-2019 at 14:13
by: B.D.E
Ammonium formate from Ammonium chloride
Screw that shit. I'll just buy ammonium carbonte or urea(for NH3 gas generator). I spent way too muc ...
16-11-2019 at 15:13
by: B.D.E
Ammonium formate from Ammonium chloride
[rquote=626230&tid=154078&author=unionised]I'm fairly sure that mixing solutions of sodium f ...
15-11-2019 at 09:02
by: B.D.E
Ammonium formate from Ammonium chloride
UPDATE:
Well.. I tried bubbling ammonia gas trough formic acid solution(<99%) and I got jack shi ...
14-11-2019 at 12:25
by: B.D.E
Vigreux column: 200mm vs. 300mm
Alright then, copper mash it is!(I am also buying the hollow beads, just because they're cheap af :) ...
18-10-2019 at 21:56
by: B.D.E
Vigreux column: 200mm vs. 300mm
[rquote=624580&tid=154163&author=Sulaiman][rquote=624576&tid=154163&author=B.D.E]... ...
18-10-2019 at 05:04
by: B.D.E
Vigreux column: 200mm vs. 300mm
Thanks for all the replies.
I Looked into buying some spheres/rings on Ebay, and although they were ...
18-10-2019 at 03:42
by: B.D.E
Vigreux column: 200mm vs. 300mm
Knowing that I'm rethinking if it's even worth buying. I Can instead just buy air condenser and use ...
13-10-2019 at 13:11
by: B.D.E
Vigreux column: 200mm vs. 300mm
So my 300mm Vigreux column just broke and I'm looking to buy a new one. Because the 300mm length was ...
12-10-2019 at 11:35
by: B.D.E
Ammonium formate from Ammonium chloride
Thanks for the new information everyone! :)
I'll probably go with the "bubbling ammonia method".

...
26-9-2019 at 00:17
by: B.D.E
Ammonium formate from Ammonium chloride
[rquote=623498&tid=154078&author=draculic acid69][rquote=623497&tid=154078&author=B. ...
25-9-2019 at 07:06
by: B.D.E
Ammonium formate from Ammonium chloride
[rquote=623493&tid=154078&author=hodges]Mix the ammonium chloride with a strong base such as ...
24-9-2019 at 18:07
by: B.D.E
Ammonium formate from Ammonium chloride
Hey there,

So I need to get some ammonium formate for the Leuckart reaction, and the only ammoniu ...
24-9-2019 at 16:34
by: B.D.E
Hydride shift in Safrole halogenation
Hey there,
First thing first, it's seems like an awesome forum and I'm very glad to have found it : ...
5-8-2019 at 21:24
by: B.D.E

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