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Iodine and H2SO4
If we agree, we must both be wrong!:D
3-11-2009 at 13:11
by: entropy51
diethyl ether
[quote]To prevent the formation of peroxides I will only use a bottle for one year[/quote]If you mak ...
3-11-2009 at 06:42
by: entropy51
Iodine and H2SO4
[quote]Why the heck was the iodine boiling and making a reflux ring with the acid present?[/quote]Be ...
1-11-2009 at 18:12
by: entropy51
Iodine and H2SO4
[rquote=165243&tid=12999&author=mr.crow]The H2SO4 absorbs the water rather violently, then c ...
1-11-2009 at 17:25
by: entropy51
Iodine and H2SO4
[rquote=165241&tid=12999&author=mr.crow]
When I was trying to re-sublime it the remaining w ...
1-11-2009 at 16:46
by: entropy51
What happened here????
I was thinking of pyridine too, but I checked and the denatured I used is Formula 19, which accordin ...
1-11-2009 at 14:57
by: entropy51
What happened here????
[rquote=164793&tid=12975&author=entropy51] My recollection is that KOH in pure EtOH doesn't ...
1-11-2009 at 12:30
by: entropy51
Thiosemicarbazide Synthesis
A nice prep, benzylchloride1. Not relevant to your method, but to the thread topic, I've had occais ...
1-11-2009 at 11:36
by: entropy51
Favourite organic text
The old versions of Fieser & Fieser are pretty good, as are the older versions of Noller. In th ...
1-11-2009 at 10:22
by: entropy51
Reaction of toluene with acetic acid
That volume of Gazzetta chimica Italiana is on books.google.com but they aren't allowing full view b ...
1-11-2009 at 10:09
by: entropy51
Reaction of toluene with acetic acid
[rquote=165201&tid=12993&author=Satan]I would be pleased if somebody proves that I am wrong, ...
1-11-2009 at 08:25
by: entropy51
Preparation of ionic nitrites
Sedit, I have used the nitrite test you showed above and it works well, but it is so sensitive that ...
31-10-2009 at 15:17
by: entropy51
Preparation of ionic nitrites
[url=http://books.google.com/books?id=ZkoJsQIhDWkC&pg=PT61&lpg=PT61&dq=%22reduction+of+s ...
31-10-2009 at 14:37
by: entropy51
Extraction of the "good stuff" from herbal highs (Salvia etc)
[quote]It produces a quality you just can not find in commercial oils that provides all the subtile ...
30-10-2009 at 05:39
by: entropy51
Extraction of the "good stuff" from herbal highs (Salvia etc)
[rquote=165077&tid=12990&author=Mafoon]I grow salvia (which is legal where i am in U.K.) and ...
29-10-2009 at 14:52
by: entropy51
Making glacial acetic acid
Runningbear, SC Wack posted that patent a couple of months ago. I gave it a shot with an aspirator ...
29-10-2009 at 13:35
by: entropy51
Starting out - glassware in Australia
[quote]they already had a very large file on me consisting of myspace pictures, user accounts used, ...
29-10-2009 at 13:30
by: entropy51
Starting out - glassware in Australia
[quote]I'm wondering if we all don't have "files" on us. LE likely looks at it this way: why else wo ...
28-10-2009 at 16:11
by: entropy51
Starting out - glassware in Australia
Sorry to hear about your misfortune, but it sounds like you've fared better than I would expect had ...
28-10-2009 at 08:50
by: entropy51
Possible convenient way of making phosphates and h2o2 OTC
[quote]That would mean i could get decent quality hydrogen peroxide just by dissolving dishwashing p ...
28-10-2009 at 08:42
by: entropy51
cant be real
[quote]Whatever you do---don't change a thing. [/quote]

I was taught that these sorts of things a ...
28-10-2009 at 06:52
by: entropy51
Making glacial acetic acid
Runningbear, you can distill the stop bath just to get rid of the indicator it contains, which remai ...
28-10-2009 at 06:40
by: entropy51
Possible convenient way of making phosphates and h2o2 OTC
[quote]Any suggestions or comments?[/quote]

I don't know where you're located, but in many areas ...
28-10-2009 at 06:27
by: entropy51
Starting out - glassware in Australia
[quote]Basically similar items to the WA list.
Maximum penalty 15 years jail . My god what is this ...
26-10-2009 at 17:37
by: entropy51
H2O2. 2.5 years and still 35%
[rquote=164937&tid=10470&author=angelhair]Jesus Christ, The question is simple.

How much ...
26-10-2009 at 17:28
by: entropy51
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