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Distillation Setup for 1100°C (High Tmperature)?
Glassware starts to soften around 500, so 1100 is out of the question. Steel.
30-1-2020 at 12:38
by: DraconicAcid
Making uranium and thorium by electrolysis?
[rquote=630283&tid=154784&author=nagyepf]
I am not sure if uranium and thorium form amalgam ...
30-1-2020 at 10:54
by: DraconicAcid
Cobalt blue (and violet and pink)
For Thenard's blue, I made a solution of sodium aluminate by reacting aluminum with sodium hydroxide ...
29-1-2020 at 19:48
by: DraconicAcid
Making uranium and thorium by electrolysis?
Cotton and Wilkinson say....

The [actinide] metals may all be prepared by a method applicable on ...
28-1-2020 at 14:58
by: DraconicAcid
Potassium Nitronickelate(s); help with synthesis?
Yes, it does form- I've made it. A fellow named Chemstudent sent me the prep- not sure if he's stil ...
25-1-2020 at 15:56
by: DraconicAcid
Azelaic acid
I remember my first-year organic prof telling us that mnemonic, but he didn't expect us to actually ...
16-1-2020 at 12:47
by: DraconicAcid
anyway to make [Ag(NH3)2]Cl? (having trouble)
Light blue colour? That would indicate a copper impurity- silver ions have a full d subshell (rathe ...
16-1-2020 at 11:45
by: DraconicAcid
Attempts to make calcium iodide
In the absence of iodine, acetone will react with magnesium (and possibly calcium) to give pinacol. ...
15-1-2020 at 22:18
by: DraconicAcid
anyway to make [Ag(NH3)2]Cl? (having trouble)
Almost any silver compound will be soluble in ammonia, apart from the really insoluble ones such as ...
14-1-2020 at 11:23
by: DraconicAcid
Formula for dark green chromium acetate
It's obviously chromium(III) acetate- if it was a rarer oxidation state, they would have specified. ...
10-1-2020 at 20:19
by: DraconicAcid
Acetate Salts From Vinegar For Synthesis of Acetic Acid
You have a very small amount of sodium carbonate (Na2CO3)? You can buy it dirt cheap as washing sod ...
9-1-2020 at 18:23
by: DraconicAcid
Removing charcoal from evaporating dish
I find that boiling nitric acid easily cleans out char left over from screaming gummi bear reactions ...
8-1-2020 at 06:50
by: DraconicAcid
anyway to make [Ag(NH3)2]Cl? (having trouble)
To quote wikipedia:

"Silver nitride was formerly referred to as fulminating silver, but this can ...
7-1-2020 at 12:52
by: DraconicAcid
anyway to make [Ag(NH3)2]Cl? (having trouble)
You need ammonia, not ammonium chloride.
6-1-2020 at 22:28
by: DraconicAcid
Extraction of diethyl ether — impurities?
What are you using the ether for? It's possible that they won't interfere with your planned reactio ...
2-1-2020 at 15:36
by: DraconicAcid
Everyday Chemistry
Really? I thought the Brita filters only had activated charcoal.....
2-1-2020 at 14:46
by: DraconicAcid
Extraction of diethyl ether — impurities?
The "sweetened petroleum gases" may contain things like butanes or pentanes, which would distill ove ...
2-1-2020 at 13:44
by: DraconicAcid
Report on making Aluminium Iodide
If you made it in water, it's not going to be AlI3. At best, it will be hydrated AlI3; at worst, a ...
1-1-2020 at 23:48
by: DraconicAcid
Cobalt bromide complexes
It should work.

https://www.degruyter.com/view/j/ncrs.1999.214.issue-3/ncrs-1999-0348/ncrs-1999-0 ...
28-12-2019 at 15:26
by: DraconicAcid
O-Cresol from Salicylic acid
Reducing a carboxylic acid to an alkane is not easy. You'd have to turn it into an ester, use lithi ...
26-12-2019 at 12:58
by: DraconicAcid
is there any resonably avalible ways to make copper (III) (any purple copper compund/complex)
Woelen made a copper(III) periodate complex.

https://woelen.homescience.net/science/chem/exps/CuI ...
23-12-2019 at 13:58
by: DraconicAcid
Organic Electrochemistry Questions
[rquote=628455&tid=154611&author=Mar-Vell]What about when a reference says, for example, "-1 ...
23-12-2019 at 11:22
by: DraconicAcid
Organic Electrochemistry Questions
[rquote=628431&tid=154611&author=Mar-Vell]Thank you all for your answers.

In other textbo ...
22-12-2019 at 21:46
by: DraconicAcid
Separation question
Well, coming up with a separation scheme may be fun. And it's probably been too long for the OP to ...
22-12-2019 at 19:58
by: DraconicAcid
Separation question
[rquote=628377&tid=154612&author=fusso]Can open the pdf, but cant see anything except the co ...
21-12-2019 at 21:40
by: DraconicAcid
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