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Preparation of Sodium Bisulphite n stuff
You need "a lot" of heat. See the thread on "ionic nitrites."

I would make sure that your nitrit ...
21-6-2016 at 11:44
by: Magpie
Preparation of Sodium Bisulphite n stuff
Thanks for posting this synthesis of SO2. I haven't needed one yet but might in the future.

Sodi ...
21-6-2016 at 10:34
by: Magpie
Unable to access site from the main page
Yes, I've been having similar problems. I usually use a link from "most visited" but this was not w ...
20-6-2016 at 21:52
by: Magpie
"It's time to start hoarding before TSCA kicks in"
This is the title of two letters submitted to the editor of today's [i]Wall Street Journal[/i]. Her ...
16-6-2016 at 18:03
by: Magpie
Preparation of elemental phosphorus
Here's a good thread to review ("Carbon Arc Furnace"):

http://www.sciencemadness.org/talk/viewthr ...
16-6-2016 at 08:59
by: Magpie
Preparation of elemental phosphorus
The Landis design does not show any kind of disk for the crucible electrode. I'm not sure one is ne ...
13-6-2016 at 18:09
by: Magpie
Preparation of elemental phosphorus
The Landis water seal for the carbon electrode might be a good option.

You could install a 50a br ...
13-6-2016 at 13:22
by: Magpie
What to do with chlorine gas ?
[rquote=451741&tid=66219&author=NEMO-Chemistry]
So is it worth getting a mask when the wors ...
13-6-2016 at 13:08
by: Magpie
Preparation of elemental phosphorus
Sounds good. I don't recall any previous use of an arc furnace. This will be a very interesting ex ...
11-6-2016 at 21:18
by: Magpie
Preparation of elemental phosphorus
[rquote=451527&tid=65&author=Magpie]
I assume you are going to want to reuse the carbon cru ...
11-6-2016 at 16:05
by: Magpie
Preparation of elemental phosphorus
@careysub: Yes, I think the 5-gallon size would be big enough. Minimizing the internal volume woul ...
11-6-2016 at 12:47
by: Magpie
Preparation of elemental phosphorus
I think your basic idea is sound. As you say the challenge is to develop a [i]safe[/i] and [i]econ ...
11-6-2016 at 09:13
by: Magpie
preparation of congo red
@aga:

I recommend that you follow the Kline procedure from the [i]Journal of Chemical Education[/ ...
7-6-2016 at 17:57
by: Magpie
preparation of congo red
The purification procedure from [i]Fundamentals Processes of Dye Chemistry [/i]by Fierz-David & ...
7-6-2016 at 12:55
by: Magpie
preparation of congo red
Thanks for that information SC.

I don't know that there is any propensity for the diazonium compo ...
5-6-2016 at 13:35
by: Magpie
preparation of congo red
[rquote=450782&tid=66391&author=gdflp] Why was your naphthionate solution so dark, it appear ...
4-6-2016 at 13:02
by: Magpie
preparation of congo red
This is an update on my attempted purification of homemade congo red. The method I am using is that ...
4-6-2016 at 10:17
by: Magpie
Chemical Tanker Seen on Highway
I saw a new placard on the highway yesterday on a ss tanker:

[file]51212[/file]

This is for h ...
3-6-2016 at 08:46
by: Magpie
preparation of congo red
Thanks to all. I'm still working on the purification. The ethanol extract has just reached dryness ...
2-6-2016 at 17:52
by: Magpie
preparation of congo red
[b]Introduction[/b]
Congo Red is an azo dye formed from the coupling of benzidine HCl and Na napthi ...
31-5-2016 at 14:19
by: Magpie
Sipohn flow rate
[rquote=450185&tid=66363&author=blogfast25]

$$Q_v \approx \frac{\pi}{4}D^2\sqrt{2gy}$$

...
28-5-2016 at 08:40
by: Magpie
preparation of naphthionic acid
Nice work gdflp - the pictures are familiar. ;)

When I first weighed the naphthionic acid filter ...
27-5-2016 at 14:54
by: Magpie
preparation of naphthionic acid
The α-nitronaphthalene was homemade (ref 2).
27-5-2016 at 13:01
by: Magpie
preparation of naphthionic acid
Thanks aga. Yes, this will be used to make congo red, an acid-base indicator that changes from blue ...
27-5-2016 at 12:46
by: Magpie
preparation of naphthionic acid
[b]Introduction[/b]
Napthionic acid can be prepared from α-nitronaphthalene using the Piria reacti ...
27-5-2016 at 12:23
by: Magpie
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