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[rquote=245200&tid=19722&author=GreenD]How do you guys find the "original" papers?[/rquote]
... |
13-4-2012 at 07:20
by: Nicodem |
2-(propylsulfanyl)benzene-1,4-diol mp?
71-73 °C from benzene according to DOI:10.1248/cpb.16.195 |
12-4-2012 at 10:35
by: Nicodem |
Favorskii rearrangement question
[rquote=245009&tid=19690&author=Qadira]Anyway I don't read Italian but maybe they have other ... |
11-4-2012 at 13:23
by: Nicodem |
Favorskii rearrangement question
[rquote=245002&tid=19690&author=Qadira]See this scheme from Italian paten.[/rquote]
Which p ... |
11-4-2012 at 10:59
by: Nicodem |
Need help! who knows the mechanism of Kharasch-Brown Reaction
It was not easy to find, but this is apparently the seminal paper for this reaction:
[b]Carboxyla ... |
11-4-2012 at 08:13
by: Nicodem |
Ozonelabs- Synthesis of 2-Iodobenzoic Acid
It is not [i]solely[/i] the melting [i]point[/i] that gives a conclusive information in regard to th ... |
11-4-2012 at 07:37
by: Nicodem |
Favorskii rearrangement question
[rquote=244930&tid=19690&author=Qadira]Has anyone tried this reaction on aromatic chlorometh ... |
11-4-2012 at 07:29
by: Nicodem |
wet aminative reduction
Thank you very much for your effort.
I don't think the filtering was necessary - those solids would ... |
11-4-2012 at 06:28
by: Nicodem |
Nitrostyrene from polystyrene?
[rquote=244790&tid=19674&author=math]would it be possible to make nitrostyrene from commerci ... |
10-4-2012 at 06:43
by: Nicodem |
Opening a lactone - Easy?
I always find it amusing when I see younger people having a lousier memory than myself, but sometime ... |
6-4-2012 at 06:53
by: Nicodem |
So it's hydrated silica gel and... what?
I doubt there would be much magnesium whatever in such a basic solution. The solubility of Mg(OH)2 i ... |
5-4-2012 at 07:04
by: Nicodem |
wet aminative reduction
DrNoiZeZ, thanks for sharing your results. Now that you have the methodology in place, could you inv ... |
5-4-2012 at 06:55
by: Nicodem |
Chlorination of an aromatic ring
[rquote=243810&tid=19581&author=mycotheologist]I assume the amino group will form an interme ... |
4-4-2012 at 08:43
by: Nicodem |
copper silicate?
Barley81 brought to our attention the reaction of acidic colored metal salts with waterglass. I was ... |
3-4-2012 at 08:20
by: Nicodem |
New Energetic Materials - Current Research
[rquote=243740&tid=1970&author=franklyn]That is a gem of a paper.
The essential reaction ... |
3-4-2012 at 07:14
by: Nicodem |
First attempt at the rearrangement of 2-phenylpropanal
[rquote=243545&tid=19505&author=Asphyxiated]From p2p I have seen before this looks like pure ... |
2-4-2012 at 06:44
by: Nicodem |
Vanillin Demethylation
[rquote=243643&tid=19468&author=niertap]Have you considered going balls to the wall and micr ... |
2-4-2012 at 06:23
by: Nicodem |
copper silicate?
[rquote=243396&tid=19542&author=blogfast25]Nicodem:
A tad harsh, I feel.[/rquote]
The ha ... |
31-3-2012 at 13:18
by: Nicodem |
Making sodium iodide from iodine
[rquote=243377&tid=19546&author=garage chemist]I thought about doing it as follows: Slowly a ... |
31-3-2012 at 09:33
by: Nicodem |
Forest of amines! (saccharin to cyclic and asymmetric amines)
That's an impressive purity, worthy of the two recrystallizations. Have you weighted the crude produ ... |
31-3-2012 at 08:16
by: Nicodem |
Energetic derivatives of cyanuric acid?
No it is not.
But you can still UTFSE if you are unable to use the direct link!  |
31-3-2012 at 07:06
by: Nicodem |
Energetic derivatives of cyanuric acid?
I always suspected nobody ever UTFSE! Now I see it is indeed so:
https://www.sciencemadness.org/whi ... |
31-3-2012 at 07:00
by: Nicodem |
First attempt at the rearrangement of 2-phenylpropanal
[rquote=242973&tid=19505&author=Asphyxiated]Hey there,
I posted on here a couple weeks ag ... |
31-3-2012 at 06:57
by: Nicodem |
Forest of amines! (saccharin to cyclic and asymmetric amines)
Have you taken the mp of your product? It could as well be unreacted saccharin.
Keep in mind that N ... |
31-3-2012 at 06:37
by: Nicodem |
copper silicate?
[rquote=243319&tid=19542&author=AJKOER]I would try reacting Sodium Silicate, Na2SiO3, which ... |
31-3-2012 at 06:08
by: Nicodem |
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