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Synthesis of phenyl-2-ethanol
Riddle me this, Cryolite. My reaction mechanisms, and stereochemistry, are largely misremembered.
...
30-1-2018 at 14:05
by: zed
Color of Phenylacetone
Been a long time, but I may have seen a commercial product, that was basically a colorless or nearly ...
30-1-2018 at 13:48
by: zed
1000ml Beakers that i touch explode
Which brings us to a topic, I have been wondering about.

Coffee pots. Tough durable. Can take ...
28-1-2018 at 15:00
by: zed
Synthesis of phenyl-2-ethanol
Similar to the reaction is used on Aminoacids to form halo-acids.

Produces oxides-of-nitrogen. I ...
28-1-2018 at 14:31
by: zed
new way of PCB via plating
Yup! Most experiments fail.:D
28-1-2018 at 14:23
by: zed
Heavy water
Probably not. But, it is an interesting idea.

Seems like I read somewhere, that there are deep o ...
28-1-2018 at 14:21
by: zed
Issues with Soxhlet set up
When working with LiAlH4, it is important to be a control freak.

Therein I am not wild about usin ...
26-1-2018 at 15:01
by: zed
Copper chromite wanted to buy..need sent to nz
Well, one of the guys has a prep for Copper-Chromite, on u-tube.

Probably better to make it fresh ...
25-1-2018 at 13:24
by: zed
Issues with Soxhlet set up
Peyote cacti have been in high demand, for generations in the US.

Once upon a time, they grew la ...
16-1-2018 at 16:06
by: zed
Synthetic Quartz Crystals - Alternate methods?
Raw feedstocks?

Seems to me, the feedstock of choice in the old days, was chunks of dirt-cheap Br ...
13-1-2018 at 14:07
by: zed
Fire & Explosion risk vs. scale
Experience is good, but it doesn't totally vaccinate against making a dumb mistake.

So many varia ...
11-1-2018 at 15:46
by: zed
Synthesis of 2-Nitropropane-1-ol
Ummm. Might be a handy precursor to Alanol.

The alternative, reducing the ester of the aminoaci ...
10-1-2018 at 17:07
by: zed
DMT synthesis from indole and DMAE
Aww. This kinda stuff has mostly been tried.

The bromo material you suggest, figures to be not f ...
10-1-2018 at 13:49
by: zed
Can butane melt silver?
What? You don't want to be electrocuted?

Perhaps you have a point.

Once upon a time, jewelers ...
9-1-2018 at 18:56
by: zed
Drying IPA
Depends on what you consider dry. If that isopropylalcohol needs to be really really dry, treatment ...
9-1-2018 at 14:39
by: zed
Can butane melt silver?
Now, if you have an old microwave oven or two, and a lantern battery, you might want to try this. h ...
9-1-2018 at 14:21
by: zed
Hydrogenation of isopropanol
Nope, the substrate is reduced by isopropylalcohol.

http://www.organic-chemistry.org/namedreactio ...
9-1-2018 at 13:54
by: zed
DMT synthesis from indole and DMAE
There are better approaches. Read.
9-1-2018 at 13:42
by: zed
Can butane melt silver?
Yup. The butane or propane, you are using, is about as good as anything. Just need a better deliv ...
8-1-2018 at 16:47
by: zed
Phosphorous pentoxide from phosphate?
P2O5 may occasionally be purchased. It is not legally restricted.

Might not be possible to desic ...
8-1-2018 at 16:37
by: zed
Hydrogenation of isopropanol
Reducing Isopropyl Alcohol, is pretty difficult under normal conditions.

Makes a pretty good redu ...
8-1-2018 at 16:28
by: zed
Found an old Aldrich catalog.
Oh, I have a more recent one. Prices still weren't horrible. Just had to buy larger lots.

In th ...
8-1-2018 at 16:18
by: zed
Need help with Urea-formaldehyde resins
I found some references for Urea-Acetaldehyde resins, but they do seem to utilize some formaldehyde. ...
8-1-2018 at 16:08
by: zed
Substitute for piperidine in this reaction
Piperidine might be a tough "get" nowadays.

Easy to make pyridine. Might not be hard to reduce. ...
7-1-2018 at 13:58
by: zed
Schiffs base / imine with an amine salt?
Yup. Amine salts of strong acids, are usually neutralized before attempting to react with ketones o ...
7-1-2018 at 13:05
by: zed
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