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2,4-dihydroxybenzoic acid from resorcinol
I found this
Comprehensive Practical Organic Chemistry: Preparations And Quantitative Analysis
By ...
31-5-2020 at 10:58
by: Fery
2,4-dihydroxybenzoic acid from resorcinol
Hi Boffis, using the baloon is great idea. I observed that bubbles of CO2 evolved slowly during the ...
25-5-2020 at 05:54
by: Fery
ethyl formate - esterification by reactive distillation
Cou that's why I prefer hexane instead of benzene though the efficiency of hexane is much lower. Tol ...
25-5-2020 at 02:10
by: Fery
Concentrating phosphoric acid
Mateo_swe is right, boroglass 3.3 is not resistant against hot conc H3PO4
that's why Magpie suggest ...
24-5-2020 at 23:47
by: Fery
2,4-dihydroxybenzoic acid from resorcinol
here a method with somewhat better yield (3,0 g instead of previous 1,9 g)

5,5 g resorcinol
25 g ...
24-5-2020 at 23:20
by: Fery
n-propyl acetate - pear essence - esterification by reactive distillation
Initially the reactants were calculated as:
2 mol 1-propanol M=60,01 g/mol, 120,0 g
3 mol acetic a ...
24-5-2020 at 11:15
by: Fery
ethyl formate - esterification by reactive distillation
Cou, if you don't have Graham condenser I would use Liebig through which I would circulate a water f ...
23-5-2020 at 23:55
by: Fery
ethyl formate - esterification by reactive distillation
Cou methyl formate should be produced the same way too, just use efficient condenser (Graham, not Li ...
23-5-2020 at 03:37
by: Fery
Help in synthesis of Benzoic acid from Benzaldehyde
wibbzlab, such a pitty converting benzaldehyde to benzoic acid... you can oxidize more available tol ...
22-5-2020 at 04:43
by: Fery
ethyl formate - esterification by reactive distillation
Hi Bedlasky, of course it could be done using simple distillation apparatus, in that case just don't ...
20-5-2020 at 22:24
by: Fery
ethyl formate - esterification by reactive distillation
Surprisingly this esterification experiment is not yet posted in the SC forum although both reagents ...
20-5-2020 at 11:14
by: Fery
Natural equivalents of an antidepressant nmda antagonist
I have never seen any antidepressant based on NMDA receptors yet. Current antidepressants increase s ...
20-5-2020 at 05:28
by: Fery
butyl butyrate
DraconicAcid is right, I recognize butyl butyrate as tutti-frutti, very pleasant. Best pineapple sce ...
18-5-2020 at 23:06
by: Fery
2,4-dihydroxybenzoic acid from resorcinol
Kolbe-Schmitt synthesis - carboxylation of phenols (addition of CO2).

Phenol reacts with CO2 at h ...
15-5-2020 at 05:06
by: Fery
(Lab report) Making benzyl acetate by fischer esterification
j_sum1 - natural ylang-ylang is beautiful, one of my favorites (together with pear and pineapple), I ...
12-5-2020 at 23:00
by: Fery
CsICl4 caesium tetrachloroiodate
I added some excess of HCl and also let to release Cl2 for prolonged time as there is an equilibrium ...
12-5-2020 at 22:35
by: Fery
CsICl4 caesium tetrachloroiodate
woelen thank you very much
I can let my product to stay for some time and determine possible weigh ...
12-5-2020 at 22:12
by: Fery
Mercury mitigation
both Zn powder and S are good, but Zn is better
12-5-2020 at 21:35
by: Fery
CsICl4 caesium tetrachloroiodate
To 25 ml Erlenmeyer flask was added 7,0 g 35% HCl - approx 10% more than theoretically required 0,06 ...
12-5-2020 at 11:42
by: Fery
The synthesis of methyl sorbate
Syn the Sizer - very nice, thx for sharing !
11-5-2020 at 04:10
by: Fery
Sorbic acid esters
Thx Boffis, yes, I should convert sorbic acid into sorbyl chloride.

Here they used thionyl chlori ...
11-5-2020 at 04:05
by: Fery
Sodium Sulfate Solution turned cloudy when heated
max solubility at 30 C and then decreases on heating (inverted solubility curve) - maybe this is you ...
10-5-2020 at 11:10
by: Fery
Sorbic acid esters
Hi Syn the Sizer, looking forward your method. I tried allyl sorbate via allyl alcohol + sorbic acid ...
10-5-2020 at 11:04
by: Fery
Synthesis of NaI from KI - how to wash away KOH?
something similar discussed here:
https://www.sciencemadness.org/whisper/viewthread.php?tid=154650
9-5-2020 at 22:14
by: Fery
Experiments with Cesium chloride?
I've bought some CsCl just only for demonstration of flame coloring, thanks for everyone for a lot o ...
4-5-2020 at 09:49
by: Fery
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