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Cleaning sodium metal?
Congrats :) Some extra sodium is always nice
9-2-2010 at 15:21
by: mr.crow
Cleaning sodium metal?
Have you read Len1's excellent sodium thread? https://www.sciencemadness.org/whisper/viewthread.php? ...
8-2-2010 at 08:08
by: mr.crow
other good science/chemistry forums?
http://www.versuchschemie.de

I don't know German, but they still have tons of amazing synthesises ...
4-2-2010 at 20:05
by: mr.crow
Benzoquinone from Paracetamol
[rquote=171078&tid=8250&author=Taoiseach]http://www.versuchschemie.de/topic,13634,-Synthese+ ...
4-2-2010 at 11:01
by: mr.crow
Sulfuric Acid at Home
Try searching youtube :p http://www.youtube.com/watch?v=QOKX6Dn-K_w

I hope you change your mind t ...
2-2-2010 at 15:31
by: mr.crow
Preparation of cyanides
[rquote=170776&tid=23&author=Myfanwy]ok i done the experiment. i made 64 pictures and movies ...
30-1-2010 at 16:31
by: mr.crow
phenylacetic acid
Whats that old saying, honey attracts more flies then vinegar?

I wonder if the OP was that clever
26-1-2010 at 09:25
by: mr.crow
Laboratory Tips and Tricks
Perhaps you could push the magnet further into the tube, seal it then push it back to the end with a ...
23-1-2010 at 20:06
by: mr.crow
Ozonelabs- Synthesis of 1,4-Bis(3-chloropropoxy)benzene
[rquote=170201&tid=13299&author=Jor]So what do you want to make with this compound? :D

No ...
23-1-2010 at 16:50
by: mr.crow
Ozonelabs- Synthesis of 1,4-Bis(3-chloropropoxy)benzene
Excellent work :)

When you get the yield you can see if any of the chlorine reacted forming bypro ...
23-1-2010 at 15:00
by: mr.crow
Western Australia laws - buying glassware
I think we should have a subforum specifically for chemistry in different countries.

I have heard ...
16-1-2010 at 18:46
by: mr.crow
Diethylsulfide from potassium ethylsulfate and sodium sulfide
Cool some more videos :)

I thought sodium ethyl sulfate hydrolyzed easily and you use water in yo ...
16-1-2010 at 15:19
by: mr.crow
Preparation of solid aluminium isopropoxide
Klute is back in the lab :)

Rubbing alcohol also comes in a 99% grade with a small amount of mine ...
15-1-2010 at 07:21
by: mr.crow
Diethylsulfide from potassium ethylsulfate and sodium sulfide
Awesome videos. The official music of science videos is now 009 Sound System.

I'm glad no one cal ...
13-1-2010 at 20:18
by: mr.crow
Obtaining glyoxylic acid
I am interested in glyoxylic acid too, can make vanillin with it!

Obvious answer: chemical suppli ...
11-1-2010 at 17:11
by: mr.crow
Mystery of the yellow benzophenone
Chlorination will be too much like dioxin or PCBs :o

The Baeyer-Villiger reaction is the one I wa ...
11-1-2010 at 10:06
by: mr.crow
Mystery of the yellow benzophenone
The IR spectra peaks vaguely match the ones from Sigma, so it doesn't confirm or deny anything. 300% ...
11-1-2010 at 07:51
by: mr.crow
Questions regarding the recycling of DCM
How about using mercury to remove sulfides? I think it can break disulfides bonds.

Ok mercury is ...
8-1-2010 at 12:18
by: mr.crow
Fuming Nitric Acid
I am sure your business is already set up as a laboratory, so a fume hood with a distillation appara ...
4-1-2010 at 13:11
by: mr.crow
Bad days in the lab or with glassware?
I guess glass breaks when it wants to :(

Does anyone think the adapter is still usable or is it f ...
4-1-2010 at 07:07
by: mr.crow
Aldol Condensation of Piperonal with Acetone
So its the aldol reaction, then hydrogenation

You should read the PDF in this thread, very well d ...
3-1-2010 at 19:09
by: mr.crow
Aldol Condensation of Piperonal with Acetone
Well it is rather fun thinking of synthetic routes, even dubious ones...

What would be better wou ...
3-1-2010 at 17:34
by: mr.crow
Benzyl chloride from Benzyl acetate
I was also thinking of the possibility of turning esters into alkyl halides.

The general procedur ...
22-12-2009 at 21:21
by: mr.crow
Mystery of the yellow benzophenone
I acquired some benzophenone on ebay that is supposed to be used for absorbing UV light in cosmetic ...
21-12-2009 at 11:49
by: mr.crow
Latest chemical order?

- 50g sodium metal
- 0.5g platinum wire
- 5g palladium
- 1g of gold

Nice little collection : ...
15-12-2009 at 07:32
by: mr.crow
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