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Strange phenomenon whilst preparing Isopropyl nitrite
is there any chance that the sulphuric acid oxidised the nitrite to nitrate ?

also ,since nitrous ...
6-12-2014 at 04:14
by: CuReUS
Hybrid aqua regia from NaNO3?
IIRC ,instant cold packs contain ammonium nitrate ( NH[sub]4[/sub]NO[sub]3[/sub] )

and myst 32 ha ...
3-12-2014 at 05:53
by: CuReUS
Chlorination of tertiary amino alcohol
what about PCl[sub]5[/sub] or PCl[sub]3[/sub] ?

[url]http://en.wikipedia.org/wiki/Phosphorus_pent ...
1-12-2014 at 00:57
by: CuReUS
Preparation of ε-Caprolactam
magpie ,you could also treat cyclohexanone directly with hydrazoic acid(sodium azide +H[sub]2[/sub]S ...
29-11-2014 at 05:39
by: CuReUS
Best of SM
this is from another forum ,mostly run by junkies
[url]http://forum.opiophile.org/archive/index.php ...
27-11-2014 at 08:41
by: CuReUS
Short question / quick answer - Thread
[rquote=370689&tid=26572&author=Chemosynthesis]I was always taught that deactivation only re ...
25-11-2014 at 22:22
by: CuReUS
Sober Etaoin Shrdlu Challenge #1 - OTC TEMPO
[rquote=368557&tid=45844&author=Jylliana]All I want to say here is that I love TEMPO because ...
24-11-2014 at 09:20
by: CuReUS
Sober Etaoin Shrdlu Challenge #1 - OTC TEMPO
i made a slight error while naming a compound in my previous post.
when you oxidize 5-hydroxypentan ...
23-11-2014 at 09:23
by: CuReUS
Sober Etaoin Shrdlu Challenge #1 - OTC TEMPO
what about this method

start from lysine -can be obtained at nutrient stores

[url]http://www. ...
22-11-2014 at 02:50
by: CuReUS
Selenic Acid from Se and H2O2, electrochemistry and other pure and efficient methods
from where did you get selenium
did you buy it on ebay or did you extract it from OTC materials

...
21-11-2014 at 04:54
by: CuReUS
Microwave-made Nitric Acid
could this be used for vapor phase nitration
[url]http://www.google.com/patents/US4347389[/url]

...
21-11-2014 at 04:50
by: CuReUS
Sober Etaoin Shrdlu Challenge #1 - OTC TEMPO
[rquote=367337&tid=45844&author=Cheddite Cheese]Yeah, sodium amide probably wouldn't work; y ...
20-11-2014 at 09:30
by: CuReUS
Sober Etaoin Shrdlu Challenge #1 - OTC TEMPO
chemosynthesis ,i am very sorry:(:(

you can dehydrate aldoximes to nitriles ,not hydroxyl amines
...
18-11-2014 at 09:00
by: CuReUS
Sober Etaoin Shrdlu Challenge #1 - OTC TEMPO
i was completely disheartened after seeing that TEMPO could be made so easily from acetone and ammon ...
18-11-2014 at 05:42
by: CuReUS
the hunt for the reducing agent
in the hope of reviving this thread ,i ask a question that is bothering me for quite sometime now

...
15-11-2014 at 21:44
by: CuReUS
Synthesis of marfanil from toluene
it would be better to first halogenate the sp[sub]3[/sub] carbon using TCCA or passing chlorine thr ...
15-11-2014 at 21:05
by: CuReUS
Short question / quick answer - Thread
[rquote=364861&tid=26572&author=PHILOU Zrealone]Grignard with a nitroaromatic?
Would'nt the ...
15-11-2014 at 20:27
by: CuReUS
can fictional chemicals have a real life counterpart?
after reading about thiotimoline ,i was completely blown away :o
even if it is a fictitious compoun ...
10-11-2014 at 05:11
by: CuReUS
Thiol vs. alcohol as a nucleophile
you can see this video ,it is very helpful

[url]https://www.khanacademy.org/science/organic-chemi ...
10-11-2014 at 04:45
by: CuReUS
Life after detonation
for more information on explosions and the mistakes that people committed while making and handling ...
10-11-2014 at 03:32
by: CuReUS
Short question / quick answer - Thread
[rquote=363075&tid=26572&author=Cheddite Cheese] We ground up the magnesium metal immediatel ...
8-11-2014 at 06:31
by: CuReUS
Short question / quick answer - Thread
[rquote=362810&tid=26572&author=chemrox]IMHO a Grignard approach is usually indicated when m ...
7-11-2014 at 21:57
by: CuReUS
Preparation of acetic acid?
[rquote=362896&tid=29096&author=Awesomeness]Well, I don't seem to be dead after testing the ...
7-11-2014 at 21:00
by: CuReUS
Short question / quick answer - Thread
actually i came across this in my lab record from my undergrad days .i think we had a synthesis chal ...
7-11-2014 at 09:48
by: CuReUS
Acetic Acid Synth. Easy Home Version.
[rquote=324448&tid=29728&author=Have2Know]. I just use a big stainless steel beaker, with an ...
7-11-2014 at 03:22
by: CuReUS
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