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Organo nickel compounds by Transmetalation
I suspect that a simple dialkyl nickel will be quite prone to decomposition to nickel hydride and hy ...
26-4-2011 at 05:11
by: ScienceSquirrel
furfural
I think you might do a little better if you added some salt to the collection vessel. The solubility ...
26-4-2011 at 04:58
by: ScienceSquirrel
Non Electrolyic Chlorate Production
You are going to have to run this on a fairly big scale and it will consume a lot of chemicals. It i ...
26-4-2011 at 04:50
by: ScienceSquirrel
H2o2 from sodium persulfate
Sorry about the insult but going to www.netscape.co.uk and typing in 'persulfate chemistry' yields ...
25-4-2011 at 17:52
by: ScienceSquirrel
H2o2 from sodium persulfate
You seem like an idle sod that will do nothing for themself.
I am not going to feed you anymore and ...
25-4-2011 at 17:08
by: ScienceSquirrel
H2o2 from sodium persulfate
The reactions of persulphate salts and the reactive species at a given pH are exhaustively described ...
25-4-2011 at 17:04
by: ScienceSquirrel
need help with oxidation conditions
[rquote=207809&tid=16108&author=spirocycle]wouldn't you get some aldol products using acidif ...
24-4-2011 at 17:07
by: ScienceSquirrel
What level of exposure to methanol is safe?
It will depend on the individual.
I have had a lot more exposure to methanol than that during my ca ...
24-4-2011 at 15:25
by: ScienceSquirrel
Making sulfur from sulfates
Don't do it!
The only time it has even been considered is under war time conditions when sulphur ha ...
24-4-2011 at 12:59
by: ScienceSquirrel
Removing blu-tack?
I would suggest light petrol as commonly sold for use in cigarette lighters, etc.
Ronsonol sell th ...
24-4-2011 at 12:47
by: ScienceSquirrel
another way to form sodium carbonate?
The aim of preparative chemistry is to convert cheap and readily available materials in to more expe ...
24-4-2011 at 12:42
by: ScienceSquirrel
making reducting agent
Steel wool in combination with hydrochloric, sulphuric or acetic acid in aqueous or alcoholic soluti ...
22-4-2011 at 16:01
by: ScienceSquirrel
Tour My Lab
Some time ago I promised that I would post a picture or two showing my brewing activities.
This pic ...
21-4-2011 at 12:55
by: ScienceSquirrel
Total synthesis for beginner
The synthesis of quinine before the existence of much in the way of instrumental analysis involved t ...
21-4-2011 at 12:01
by: ScienceSquirrel
Total synthesis for beginner
[rquote=207485&tid=16044&author=NurdRage]Do you want a slideshow or not?

I don't think un ...
21-4-2011 at 08:48
by: ScienceSquirrel
Total synthesis for beginner
[rquote=207481&tid=16044&author=NurdRage]@ScienceSquirrel
So you want me to post a slide sh ...
21-4-2011 at 08:30
by: ScienceSquirrel
Making Mg3P2 from Mg and red P?
Have you thought about making aluminium phosphide instead?
It is a standard material used to get ri ...
21-4-2011 at 07:11
by: ScienceSquirrel
Total synthesis for beginner
I mean a written description with yields, melting points as characterisation, etc.
This is my descr ...
21-4-2011 at 06:15
by: ScienceSquirrel
Composition of Nail Polish Remover?
If you distill the nail polish remover using a column etc, you wil get rid of all the crap and get a ...
21-4-2011 at 04:25
by: ScienceSquirrel
ibuprofen and it's derivatives
[rquote=207461&tid=16085&author=blogfast25][rquote=207293&tid=16085&author=Jor]
I h ...
21-4-2011 at 04:21
by: ScienceSquirrel
Extraction of platinum metal from Sperrylite (PtAs2)
Nice sperrylite is worth a fortune.
http://cgi.ebay.co.uk/HUGE-11MM-SPERRYLITE-CRYSTAL-NORILSK-RUSS ...
21-4-2011 at 04:11
by: ScienceSquirrel
Cromate
No, a Darwin Award;

http://www.darwinawards.com/

I think Salman with his chromate fusion and ...
21-4-2011 at 03:52
by: ScienceSquirrel
Cromate
But Salman does not seem to have a clue.
He seems to be thinking of heating a large quantity of chr ...
21-4-2011 at 03:44
by: ScienceSquirrel
Total synthesis for beginner
[rquote=207426&tid=16044&author=NurdRage]total synthesis of luminol with OTC chemicals

ht ...
21-4-2011 at 03:12
by: ScienceSquirrel
Non Electrolyic Chlorate Production
If you want a small amount of potassium chlorate to demonstrate its properties it can be made from b ...
21-4-2011 at 03:09
by: ScienceSquirrel
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