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Nitroalkane syntheses ?
You both think about "cold reaction"?Can it work that way?

[Edited on 24-2-2017 by sulfuric acid is ...
23-2-2017 at 15:41
by: sulfuric acid is the king
Nitroalkane syntheses ?
@PHILOU Zrealone
Thanks for the answers.
Can you explain me how high pressure is not needed when e ...
22-2-2017 at 16:12
by: sulfuric acid is the king
Sodium Ethyl Sulfate


[Edited on 23-2-2017 by sulfuric acid is the king]
22-2-2017 at 16:02
by: sulfuric acid is the king
Sodium Ethyl Sulfate
What i know so far is that it has no pungent smell like sulphate when i made it by h2so4/nacl method ...
22-2-2017 at 16:00
by: sulfuric acid is the king
Sodium Ethyl Sulfate
Nah...It's to easy... :/
I just touched crystals to get them out,poured remained liquid first,and t ...
22-2-2017 at 15:46
by: sulfuric acid is the king
Sodium Ethyl Sulfate
@JJay
This is from the first try that i mentioned before,solution with misterios ultra soluble salt ...
22-2-2017 at 14:58
by: sulfuric acid is the king
Nitroalkane syntheses ?
What about ethyl iodide and sodium nitrite under high pressure?
22-2-2017 at 11:39
by: sulfuric acid is the king
Sodium Ethyl Sulfate
I use marble as a calcium carbonate source,i hope that's not a problem,i tested it disolving in hydr ...
22-2-2017 at 04:47
by: sulfuric acid is the king
Nitroalkane syntheses ?
If i try to do nitration of butane with NO2 in regular steel pipes can they sustain that for just on ...
21-2-2017 at 17:28
by: sulfuric acid is the king
Sodium Ethyl Sulfate
Ok,when you have calcium ethyl sulfate,how you add sodium carbonate,in solution or in powder form?
...
21-2-2017 at 17:24
by: sulfuric acid is the king
abnormal nitration of styrene
Yes i know for condensation reaction,but i don't have nitroalkanes...
This second reaction that you ...
20-2-2017 at 06:14
by: sulfuric acid is the king
abnormal nitration of styrene
Why not when it's very interesting :D
I though to distill/steam distill to obtain b nitro,but i thi ...
19-2-2017 at 12:16
by: sulfuric acid is the king
abnormal nitration of styrene
More info please.
Physical properties of other products of this reaction etc...
19-2-2017 at 10:37
by: sulfuric acid is the king
Sodium Ethyl Sulfate
I found this "With excess sulfuric acid, the equilibrium can
be shifted to the right."
But how muc ...
19-2-2017 at 03:45
by: sulfuric acid is the king
Sodium Ethyl Sulfate
Really?Nice then...I must try...
I added calcium carbonate but it was mess...
You have good expiri ...
18-2-2017 at 13:16
by: sulfuric acid is the king
Sodium Ethyl Sulfate
Hmmm so you have done it by acid alcohol methode...
Great.But can you tell me some details...Percen ...
18-2-2017 at 08:23
by: sulfuric acid is the king
Sodium Ethyl Sulfate
[rquote=445013&tid=1113&author=JJay]Oh and of course, here is a picture of the crude product ...
18-2-2017 at 07:21
by: sulfuric acid is the king
Sodium Ethyl Sulfate
Where can i get solubility table for NaEtSO4?
Do you have more info now?
16-2-2017 at 16:03
by: sulfuric acid is the king
Sodium Ethyl Sulfate
You got crystals,but i got nothing,and now temperature of the solution is little above zero,and noth ...
16-2-2017 at 15:32
by: sulfuric acid is the king
Sodium Ethyl Sulfate
Near anhydrous,about 15-20C before adding distilled water which was at room temperature.
I will sa ...
16-2-2017 at 14:05
by: sulfuric acid is the king
Sodium Ethyl Sulfate
I am back :D
I had no time for foruming...
Ok,today i made EtSO4 by acid/ethanol mehod,i neutraliz ...
16-2-2017 at 08:08
by: sulfuric acid is the king
Sodium Ethyl Sulfate
Simply.When i said totally used i thought reacted to form ethylsulfuric acid,diethyl sulfate,diethyl ...
15-1-2017 at 15:20
by: sulfuric acid is the king
Sodium Ethyl Sulfate
@JJay
Thanks so much.
Is there any method to know when is sulfuric acid totally used?
And what ab ...
15-1-2017 at 09:00
by: sulfuric acid is the king
Sodium Ethyl Sulfate
Aha,thanks.
But do i need oleum or just concetrated acid,what about ethanol,must be anhydrous or ca ...
14-1-2017 at 16:47
by: sulfuric acid is the king
Sodium Ethyl Sulfate
I have both.
Btw i wonder which method JJay use,'couse of materials...
14-1-2017 at 15:24
by: sulfuric acid is the king
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