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Lithium (Per)Chlorate cell
ARGGGGGGGGGGGG
still no perchlorate . It really starts to piss me off.
I increased the voltage an ...
26-2-2008 at 07:46
by: hashashan
Multilayer Metal Oxide / Titanium Anodes for Chlorate/Perchlorate
Why is it going to wear away? LD doesnt wear away that easily
24-2-2008 at 20:55
by: hashashan
More on PbO2 electrodes
as I know you cant make persulfates with PbO2 .... the sulfuric acid will destroy the anode
20-2-2008 at 20:37
by: hashashan
Lithium (Per)Chlorate cell
Its a 6-7 mol cell ... the 6-7 is due to the fact that I added more lithium chloride as the solution ...
17-2-2008 at 23:28
by: hashashan
Lithium (Per)Chlorate cell
Well its been 20 days already
no perchlorate has yet formed ... Is it possible that a cell with a ...
17-2-2008 at 15:56
by: hashashan
Perchloric acid preparation
Dude, i dont need the anhydrous ... I am after the azetropic acid.
I was told that It is possible ...
6-2-2008 at 11:41
by: hashashan
Home made chlorine donors
try DCB, it can be easily purchased anywhere as moth retardant

http://en.wikipedia.org/wiki/1,4-D ...
6-2-2008 at 08:04
by: hashashan
Perchloric acid preparation
Guys, what will happen if one attempts to make HClO4 out of KClO4 and H2SO4 distillation
suppose, ...
6-2-2008 at 04:28
by: hashashan
More on PbO2 electrodes
definitly a materpiece :) a great LD coating.. very smooth... no bumps(how did you do that BTW?)
5-2-2008 at 23:50
by: hashashan
Ammonium Perchlorate manufacture
Yes this is a good idea, but I don't have NaClO3 also :) I make the perchlorate right out of NaCl.
...
29-1-2008 at 15:24
by: hashashan
Ammonium Perchlorate manufacture
HCl is nice ... but it is absolutely unacceptable if the chlorate levels are high.
and all other m ...
29-1-2008 at 13:23
by: hashashan
Ammonium Perchlorate manufacture
I wanted to know the final products to know if they are soluble or not.
and to know how to extract ...
29-1-2008 at 10:49
by: hashashan
Ammonium Perchlorate manufacture
That I already seen
but i meant a more specific formula
as i understand the Cl- is the NaCl but ...
29-1-2008 at 08:42
by: hashashan
how much money did you spend?
I think i spent something like 3K$ .. mostly because the cheap shops here are far away and the close ...
29-1-2008 at 03:43
by: hashashan
Ammonium Perchlorate manufacture
Never seen it in an agricultural supply here .. but I believe It wont cost too much in a chem shop. ...
29-1-2008 at 03:39
by: hashashan
Ammonium Perchlorate manufacture
Damn this AP ... I already precipitated the ClO4 as the K salt.
Anyway ... Suppose I make my perch ...
28-1-2008 at 15:51
by: hashashan
Ammonium Perchlorate manufacture
@chloric : the ClO4 was refered to garage chemist with the Li production.

now about what you sai ...
28-1-2008 at 14:58
by: hashashan
Lithium (Per)Chlorate cell
Well lowered it to about 150ma/cm2 ..... Ill lower it to 100 just in case and let it run for a day
...
28-1-2008 at 14:15
by: hashashan
Lithium (Per)Chlorate cell
the density is not too high
about 300ma/cm^2
28-1-2008 at 13:44
by: hashashan
Ammonium Perchlorate manufacture
Ok guys ... suppose I got a NaClO4 + NaCl + Na2SO4 solution .... how can I get AP from it.
Adding ...
28-1-2008 at 13:27
by: hashashan
Lithium (Per)Chlorate cell
Guys, something weired is going on.
I installed my LD anode into a LiCl cell. wil average conc. ab ...
28-1-2008 at 11:16
by: hashashan
More on PbO2 electrodes
Dude I'm giving you a smaller Ti strip because the big one is currently in use .. so As I'm thinking ...
26-1-2008 at 01:15
by: hashashan
Lithium (Per)Chlorate cell
Actually If you use a saturated LiCl solution the LiClO4*3H2O should crystallize out of the solution ...
21-1-2008 at 14:38
by: hashashan
Lithium (Per)Chlorate cell
Anyway, dont you think that your solution was too diluted?
I am planning to run a Li perchlorate c ...
21-1-2008 at 06:22
by: hashashan
Lithium (Per)Chlorate cell
isnt the carbonae Li2CO3?
21-1-2008 at 04:10
by: hashashan
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