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Vacuum distillation flask limits
My friend warned that using larger than 500ml flasks in vacuum distillation is very hazardous and ma ...
17-7-2012 at 19:48
by: chucknorris
Nitroethane from ethylsulfate, Desseigne variation.
Ok I did make some half a kilo of ethyl sulfate recently.

What I did was that I measured about 1: ...
2-5-2012 at 18:14
by: chucknorris
Fuck "Pyrex"
Just blew up a process when heating (luckily powder form) stuff by using the flat PYREX jug. The hea ...
2-5-2012 at 13:50
by: chucknorris
Sodium Ethyl Sulfate
Is there even a theoretical risk that when producing sodium ethyl sulfate using sodium bisulfate and ...
23-4-2012 at 07:45
by: chucknorris
Benzyl Alcohol -> Benzaldehyde via Silica Gel Supported Jones Reagent
[rquote=76095&tid=6671&author=Hilski]Dry silica gel (5 g) was placed in a 100-mL round-botto ...
20-4-2012 at 12:28
by: chucknorris
toluene --> benzaldehyde
Ok I have been cooking some benzaldehyde stuff recently. First I just mixed 300 grams of toluene, 70 ...
20-4-2012 at 06:21
by: chucknorris
Stainless steel pot ok?
Ok I have some processes where glass cannot be used, for ex KOH NaOH fluorine compounds etc. harsh s ...
13-4-2012 at 18:27
by: chucknorris

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