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Help needed, failed hydroxylation of alpha ketones. [rquote=684016&tid=159559&author=ErgoloidMesylate]
It says less than 30, you ran it at 30.[ ... |
13-5-2023 at 04:13 by: SplendidAcylation |
Proline decarboxylations [rquote=585685&tid=113054&author=Pumukli]
Acetophenone: time to 50% conversion: 131 min, to ... |
12-5-2023 at 03:33 by: SplendidAcylation |
Michler's Ketone [rquote=683965&tid=158821&author=Boffis]I have just spotted an interesting compound in relat ... |
11-5-2023 at 13:20 by: SplendidAcylation |
Ethylamine Synthesis I haven't read the whole thread so I apologise if I am repeating what others have said, but has the ... |
7-5-2023 at 13:16 by: SplendidAcylation |
Preparation of dimethylamine @opylation, I wish that these amine salt weedkillers were available here where I live, it would have ... |
6-5-2023 at 13:15 by: SplendidAcylation |
Preparation of Ketones by Calcium salt Pyrolysis [rquote=683683&tid=159494&author=Organikum][rquote=683644&tid=159494&author=Splendid ... |
4-5-2023 at 01:34 by: SplendidAcylation |
Preparation of Ketones by Calcium salt Pyrolysis [rquote=683650&tid=159494&author=Boffis]Hi Guys, thankyou for the comments. I have been busy ... |
2-5-2023 at 01:43 by: SplendidAcylation |
Preparation of Ketones by Calcium salt Pyrolysis [rquote=683438&tid=159494&author=Fery]Boffis as well SplendidAcylation well done both experi ... |
1-5-2023 at 03:59 by: SplendidAcylation |
Are you guys using ChatGPT [rquote=683519&tid=159514&author=violet sin]Personally, I'm steering clear of the AI wave.[/ ... |
27-4-2023 at 03:09 by: SplendidAcylation |
TheVespiary downed? Here we are again, folks! |
26-4-2023 at 12:47 by: SplendidAcylation |
Preparation of Ketones by Calcium salt Pyrolysis [rquote=683362&tid=159494&author=Boffis]
@SplendidAcylation. Did your iron filings + benz ... |
24-4-2023 at 01:28 by: SplendidAcylation |
Lab clearance for sale on eBay (UK) Just saw this on eBay, wondered if this is a member; Anyway, if anyone is in the Manchester area the ... |
21-4-2023 at 13:22 by: SplendidAcylation |
DEET hydrolysis with HCl to diethylamine and toluic acid Thanks for the info, this is really interesting; I recently did this reaction using sodium hydroxide ... |
19-4-2023 at 02:45 by: SplendidAcylation |
Preparation of Ketones by Calcium salt Pyrolysis What a coincidence! While refluxing some iron powder with benzoic acid and acetic acid in a test-tub ... |
19-4-2023 at 02:43 by: SplendidAcylation |
Simple Reactions with Fluorobenzoic Acid [rquote=683249&tid=159482&author=clearly_not_atara]Benzene is quite carcinogenic; chlorobenz ... |
16-4-2023 at 13:22 by: SplendidAcylation |
Simple Reactions with Fluorobenzoic Acid I think fluorobenzene is a lot safer than benzene!
You could turn it into the amide, using ure ... |
12-4-2023 at 13:21 by: SplendidAcylation |
Hydration of styrene [rquote=673837&tid=158580&author=Texium][rquote=673835&tid=158580&author=Keras][rquo ... |
6-4-2023 at 01:34 by: SplendidAcylation |
Preparation of isobutyrophenone by the addition of isopropyl Grignard reagent to benzonitrile (Photo-assay) [rquote=682868&tid=159451&author=Texium]I wouldn’t recommend plastic syringes with rubber ... |
6-4-2023 at 01:25 by: SplendidAcylation |
Warfarin syntheses [rquote=682875&tid=159453&author=DocX][b]Background[/b]
But the internal bleedings caused ... |
2-4-2023 at 13:17 by: SplendidAcylation |
PDF version Thanks Tex!
That's a good idea; Do you suppose plastic syringes will be able to handle ether?
I ... |
2-4-2023 at 06:12 by: SplendidAcylation |
Preparation of isobutyrophenone by the addition of isopropyl Grignard reagent to benzonitrile (Photo-assay) Hi,
As promised, I have finally completed my write-up for this reaction!
The write-up below is c ... |
31-3-2023 at 04:05 by: SplendidAcylation |
Calcium cyanurate ---> Cyanamide [rquote=682819&tid=8594&author=clearly_not_atara]Sulfur would have to come from hydrogen sul ... |
30-3-2023 at 13:12 by: SplendidAcylation |
Calcium cyanurate ---> Cyanamide [rquote=682802&tid=8594&author=clearly_not_atara]This would also lead to guanidine and possi ... |
29-3-2023 at 12:46 by: SplendidAcylation |
Write-up Hi,
I have repeated the procedures detailed here, and I have had some success in the preparation ... |
29-3-2023 at 01:32 by: SplendidAcylation |
For those in the UK: kiss goodbye to N2O I can already see the Daily Mail headlines:
"Air To Be Banned Amid Nitrous Oxide Synthesis Fears" ... |
28-3-2023 at 13:09 by: SplendidAcylation |
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