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(subsituted) phenol to halobenzene I do not think the reaction between phenol and HCl/ZnCl[sub]2[/sub] is viable. This mixture is capab ... |
4-1-2015 at 12:12 by: ParadoxChem126 |
White smoke upon addition of HCl to Aniline/H2O. Any ideas? I have witnessed the same white fumes in the synthesis of chlorobenzene detailed here:
http://ww ... |
1-1-2015 at 14:37 by: ParadoxChem126 |
selling sodium metal U2U sent. |
1-9-2014 at 16:06 by: ParadoxChem126 |
Chlorobenzene from Aniline via the Sandmeyer Reaction Thanks. I acquired my aniline from Elemental Scientific, but you do have to pay for the UPS exemptio ... |
21-8-2014 at 22:55 by: ParadoxChem126 |
Chlorobenzene from Aniline via the Sandmeyer Reaction August 21, 2014
By ParadoxChem126
[b]Introduction[/b]
Chlorobenzene is a useful chemical in org ... |
21-8-2014 at 19:36 by: ParadoxChem126 |
ethyl acetate catalyst Dilute acid is not only less effective as a catalyst; it can also be destructive to the yield of eth ... |
31-3-2014 at 00:08 by: ParadoxChem126 |
Rubber stoppers, or Glass Joints? Teflon tape can also be used to seal ground joints. In some ways, it is better than grease because i ... |
27-3-2014 at 20:09 by: ParadoxChem126 |
Uses of Urea - Carbamide - CO(NH2)2 It can be used to convert benzoic acid into benzamide. Aniline can then be made from benzamide via t ... |
26-3-2014 at 19:41 by: ParadoxChem126 |
Joint size Yes, the 24 refers to the diameter of the joint at its largest point (in millimeters) and the other ... |
26-3-2014 at 18:09 by: ParadoxChem126 |
Sigma-Aldrich [rquote=324168&tid=29684&author=thesmug]
Oh yeah, I bought a reagent kit from them and it c ... |
25-3-2014 at 20:24 by: ParadoxChem126 |
Bad days in the lab or with glassware? Today I was taking apart a lithium battery to recover the lithium. At one point the battery shorted ... |
21-3-2014 at 15:55 by: ParadoxChem126 |
iodobenzene [rquote=320508&tid=29143&author=Galinstan]using Cu(1)I to make iodobenzene.[/rquote]
Gene ... |
24-2-2014 at 16:19 by: ParadoxChem126 |
Pretty Pictures (2) Nothing special, just iodine sublimating and depositing onto a round-bottom flask full of ice.
[ ... |
3-2-2014 at 22:28 by: ParadoxChem126 |
Pretty Pictures (2) Steam-distilling crude chlorobenzene out of Sandmeyer reaction waste.
[file]29455[/file] |
3-2-2014 at 08:06 by: ParadoxChem126 |
Aniline Reactions Prepare phenyldiazonium chloride from the aniline. First, react the aniline with hydrochloric acid. ... |
2-1-2014 at 17:45 by: ParadoxChem126 |
Preparation of Phenol from Salicylic Acid I did not formulate this idea, I got it from page 128-129 of this book:
http://books.google.com/b ... |
30-11-2013 at 17:13 by: ParadoxChem126 |
Preparation of Phenol from Salicylic Acid A similar method of making phenol from acetylsalicylic acid was discussed here:
http://www.scienc ... |
30-11-2013 at 16:17 by: ParadoxChem126 |
Separating bromine gas from water vapor For the carbon electrode:
http://www.youtube.com/watch?v=knc1lSupAwQ |
28-10-2013 at 20:58 by: ParadoxChem126 |
Bad days in the lab or with glassware? To separate the ground glass joint:
http://www.sciencemadness.org/talk/viewthread.php?tid=9251
|
26-10-2013 at 22:54 by: ParadoxChem126 |
Sodium Sulfide You can buy it from elemental scientific.
http://www.elementalscientific.net/store/scripts/default. ... |
24-7-2013 at 15:25 by: ParadoxChem126 |
Ethyl acetate synthesis and mushroom extraction There should not be any significant side products. The sodium sulfate forms in the neutralization of ... |
23-7-2013 at 08:34 by: ParadoxChem126 |
Ethyl acetate synthesis and mushroom extraction [rquote=293400&tid=25256&author=Hockeydemon]You can purchase M.E.K substitute from any hardw ... |
22-7-2013 at 21:09 by: ParadoxChem126 |
Ethyl acetate synthesis and mushroom extraction [quote]sulfuric acid is truly a catalyst in this reaction so i dont have to worry about any possible ... |
22-7-2013 at 21:07 by: ParadoxChem126 |
Ethyl acetate synthesis and mushroom extraction I have a video on making ethyl acetate. Reagent ACS grade 98% sulfuric acid should be suitable. The ... |
22-7-2013 at 17:00 by: ParadoxChem126 |
Ether Preparation If you wash your ether with calcium chloride solution, the CaCl2 will complex with any ethanol. Then ... |
19-7-2013 at 15:28 by: ParadoxChem126 |
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