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p-benzoquinone HELP!!!
I used Fisher IPA, sigma Aldrich iodine chips, 30% Fisher ACS H2O2 and photograde hydroquinone. Foll ...
21-11-2012 at 08:27
by: Ephesian
Successful "green" PTC-mediated methylation of syringaldehyde to 3,4,5 trimethoxybenzaldehyde using DMC without press
Great write up! We need characterization data, at least I want to see it.
18-11-2012 at 18:17
by: Ephesian
Analytical Chem before Physical Chem?
I took Physical Chemistry, Inorganic Chemistry, Advanced Organic Chemistry, Seminar, and Linear Alge ...
8-11-2012 at 17:59
by: Ephesian
Selling it all!
due to an under aged (who told me they were 21) sale, I am no longer posting or dealing with sales t ...
1-11-2012 at 14:48
by: Ephesian
New Compound
turn it into a salt, get a crystal structure, bam! publication
31-10-2012 at 11:06
by: Ephesian
Methyl / Ethyl Iodide
I'll trade MeI for dimethyl sulfate
29-10-2012 at 15:48
by: Ephesian
alkylating agents
I didn't mean to make a new thread, but here is a good review of the mechanistic behavior of alkylat ...
29-10-2012 at 04:06
by: Ephesian
HOCOCOOH.2H2O AND (COOH)2.2H2O
What's in a name? That which we call a rose
By any other name would smell as sweet.
28-10-2012 at 09:00
by: Ephesian
Vilsmeier-Haack Piperonal Synthesis
@DJF90

Thank you, as for the Reference to methylenation:

Bonthrone, W; Cornforth, J.W. The Met ...
25-10-2012 at 09:26
by: Ephesian
Seismologists Were Found Guilty of Manslaughter
[quote]
Or even the Pope! Surely he, as the closest link Christians have to God, could have forecas ...
24-10-2012 at 15:57
by: Ephesian
Vilsmeier-Haack Piperonal Synthesis
Part I. Benzodioxole Synthesis

In a 2L-round bottom flask with three necks equipped with reflux ...
24-10-2012 at 14:12
by: Ephesian
Distillation of Ethanol Problems
simple sugar fermentation shouldn't produce methanol as a byproduct.

24-10-2012 at 08:03
by: Ephesian
Is nitromethane hygroscopic?
demand kristofvagyok' Karl fischer data.
22-10-2012 at 19:11
by: Ephesian
How long can I wait before I take NMR?
I assume you used CDCl3

and yes, it should be fine



but if you don't want to trust me, save ...
22-10-2012 at 10:54
by: Ephesian
Is nitromethane hygroscopic?
I've overlooked some MSDS data sheets and a Mereck Index and the only nitromethane that was shown to ...
22-10-2012 at 09:12
by: Ephesian
do you make notes of your experiments?
This is chemistry 101. Everything that you do in the lab should be written in detail in your lab not ...
22-10-2012 at 06:06
by: Ephesian
hypochlorite solution with crystals in it
what bottle are we talking about here...

[Edited on 18-10-2012 by Ephesian]
18-10-2012 at 13:25
by: Ephesian
Part II. Demethylation of eugenol


Microwave irradiation was carried out on eugenol (4-Allyl-2-methoxyphenol) using a home microwav ...
17-10-2012 at 06:26
by: Ephesian
Selling it all!
United States, South

[Edited on 12-10-2012 by Ephesian]
12-10-2012 at 10:32
by: Ephesian
interesting sep. funnel adaptation
Pretty cool euh? Sep funnels have come a long way :)
12-10-2012 at 09:32
by: Ephesian
Selling it all!
[rquote=261997&tid=21764&author=tetrahedron]and the courtroom fight over who gets to keep th ...
12-10-2012 at 07:48
by: Ephesian
Selling it all!
I'm thinking about cleaning out and hanging up the towel, home experimentalism is taking up too much ...
12-10-2012 at 01:43
by: Ephesian
How to obtain dermatogens?

[quote]
Liquid nitrogen cryotherapy (by my doctor) failed after multiple treatment attempts, as d ...
9-10-2012 at 15:53
by: Ephesian
Nitrostyrene-like reduction

[quote]
Obvious cooks looking for info are shown little shrift here!
[/quote]

Why is there ...
4-10-2012 at 07:55
by: Ephesian
Facing eviction because of experiment 20 months ago.

[quote]
from what little I have seen online about it that vinegar is not involved nor the smell o ...
3-10-2012 at 02:21
by: Ephesian
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