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THF ( tetrahydrofuran)
This is what you do, i just tryed this 2 minutes before typing this so it works. Take the pipe cemen ...
18-12-2004 at 13:06
by: Darkfire
Hydrochloric / sulphuric acid question
HCl can be used in dehydration reaction even at consentrations less than that found in the muratic a ...
16-12-2004 at 18:01
by: Darkfire
Bromate oxidation of THF to GBL
Rhodium used to have a page on this but its a pdf and webarchive didnt get it.

Im electrolising ...
16-12-2004 at 17:57
by: Darkfire
THF ( tetrahydrofuran)
Lo Voc has 50%-70% THF.

If its just resin, THF, and cylcohexanone distilation should work well.

...
13-12-2004 at 22:06
by: Darkfire
legal absolute ethanol
I think the methanol thing with moonshine was from people trying to distill ethanol from denatured a ...
13-12-2004 at 19:31
by: Darkfire
legal absolute ethanol
Distiling of ethanol is illegal.
12-12-2004 at 19:29
by: Darkfire
What happened to PrimoPyro?
Primopyro was sick of his godly figure in the hive and here. Threads would die after his posts, so h ...
9-12-2004 at 22:16
by: Darkfire
Oxydation of Ethylamine into Nitroethane?
Yuor gonna want clear stuff, you can distill it it, or just get clean clear anti-freezee, thats what ...
7-12-2004 at 14:21
by: Darkfire
Oxydation of Ethylamine into Nitroethane?
Search for DMDO i belive it is, its a ketone peroxide of some sort, simple and high yeilding.
7-12-2004 at 13:59
by: Darkfire
n-butylamine
The amount of MeNH2 is very low. I prepared 2.5 grams of MeNH2*HCl distilled it in MeOH with NaOH a ...
1-12-2004 at 14:33
by: Darkfire
n-butylamine
Same way i wanna make the Nitroethane. And the thing with the MeNH2 is that it doesnt need to be re ...
30-11-2004 at 14:45
by: Darkfire
n-butylamine
[quote][i]Originally posted by Nosferatu[/i]
[quote][i]Originally posted by Darkfire[/i]
For certa ...
29-11-2004 at 17:40
by: Darkfire
n-butylamine
How are you getting the nitro ethane?

MeNH2 is the best way ive seen so far, beats cyclohexamine, ...
28-11-2004 at 15:20
by: Darkfire
n-butylamine
Its down for upgrades or just fixing errors.

Your doing a aldahyde and nitromethane condensation ...
27-11-2004 at 10:52
by: Darkfire
Ethyl Iodide
Anyone thought of h2so4 and NaI in DMSO then the ethanol or ether?
16-11-2004 at 15:57
by: Darkfire
bis(salicylaldehyde)ethylenediamine copper(II) and styrene
The use of per(acetic/formic) acid or oxone is the best OTC choice for epoxidation.
16-11-2004 at 15:53
by: Darkfire
chloral hydrate synthesis
Chloral hydrate is just a more illegal and complicated version of chlorobutanol, they will both yeil ...
18-9-2004 at 11:58
by: Darkfire
cleavage or hydrolosis of methoxy groups
MDMA is only similar to meth by its structure not by its action on the body. Theres basicly 2 ways t ...
18-9-2004 at 07:19
by: Darkfire
cleavage or hydrolosis of methoxy groups
Ive talked to primo pyro and madsci, and seen a link from rhodium somewhere that saffrole is illegal ...
15-9-2004 at 14:07
by: Darkfire
cleavage or hydrolosis of methoxy groups
The facist DEA isnt trying to ban it, they already did, they catch you with safrole, your sayin good ...
14-9-2004 at 17:59
by: Darkfire
cleavage or hydrolosis of methoxy groups
Thats what i figured you wanted to do, i really dont think thats possible without breaking or removi ...
14-9-2004 at 14:50
by: Darkfire
THF ( tetrahydrofuran)
Thats an intresting idea THF to GBL is a known synth, but that still shouldnt affect the price of sh ...
15-8-2004 at 20:45
by: Darkfire
Exotic thermites & analogs
I dont see why it would have to be powderd, i dont think Li has an extreme melting point, just heat ...
22-7-2004 at 09:23
by: Darkfire
Nitrogen cylinder, welding experience required?
I have a tank of nitrogen which was gotten somehow with out going through the welding industry. Im n ...
14-7-2004 at 09:59
by: Darkfire
Strange Draincleaner and Stickytack
If its a strong acid baking soda isnt really gonna work that well. A [b]solution[/b] of KMnO4 is add ...
4-7-2004 at 22:55
by: Darkfire
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