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Preparation of Methyl Iodide Using HCl Gas Actually KiWiki, theres a nice write up in the Prepublications section on the preparation of MeI usi ... |
19-12-2017 at 08:40 by: DJF90 |
Diethylamine Hydrochloride Synthesis Apologies, I clearly misread the target wrong.
In any case, you might be better off running the ... |
17-12-2017 at 16:07 by: DJF90 |
Diethylamine Hydrochloride Synthesis [rquote=490416&tid=24131&author=JJay]I'm doing a simple distillation right now, but I don't ... |
17-12-2017 at 15:23 by: DJF90 |
Large Li-ion battery packs, compact jump starters and truth in advertising? The one I have doesn't require any "warm-up period" - you hook it up and turn the ignition. It has n ... |
16-12-2017 at 09:05 by: DJF90 |
Large Li-ion battery packs, compact jump starters and truth in advertising? I have one of these: https://www.amazon.co.uk/gp/aw/d/B01KZFUW98?psc=1&ref=yo_pop_mb_pd
I bou ... |
15-12-2017 at 15:12 by: DJF90 |
Addition of HCl to Propenoic acid [rquote=499905&tid=78823&author=LearnedAmateur]I know it's not the same mechanism as what is ... |
9-12-2017 at 14:44 by: DJF90 |
Preparation of Diethyl Sulfate Magpie, the reference for the paper is [i]JACS[/i] [b]1924[/b] [i]46[/i] (4) pp. 999 to 1001. I've a ... |
8-12-2017 at 03:17 by: DJF90 |
Preparation of Diethyl Sulfate Nice work Magpie. If you have the paper perhaps you could attach it to your post for convenience (al ... |
7-12-2017 at 11:40 by: DJF90 |
can anyone describe the smell of hbr or hydrobromic acid? I find it smells quite fruity actually, but you'd want to avoid breathing it if possible |
5-12-2017 at 14:23 by: DJF90 |
Cobalt compounds [rquote=499490&tid=78561&author=Tetra][rquote=499435&tid=78561&author=DraconicAcid][ ... |
5-12-2017 at 09:11 by: DJF90 |
The Trouble with Boron Melting means less surface area which means incomplete dehydration to boric oxide. There is a prepar ... |
4-12-2017 at 11:19 by: DJF90 |
Preparation of Thionyl Chloride [rquote=499360&tid=78645&author=AJKOER]
Per Watts, a curious lesser known path to SOCl2 cla ... |
4-12-2017 at 10:10 by: DJF90 |
Making an induction heater for fastener removal? I feel your pain, Bert. With the information you've provided, I don't think you'll be able to acheiv ... |
4-12-2017 at 03:03 by: DJF90 |
Preparation of methyl tosylate, safe methylating agent http://orgsyn.org/demo.aspx?prep=cv1p0145
See note 4. |
2-12-2017 at 13:54 by: DJF90 |
Protecting weak secondary amines - driving me crazy! [rquote=498651&tid=78225&author=clearly_not_atara]I know that esters sometimes react with am ... |
26-11-2017 at 07:58 by: DJF90 |
Preparation of Quinoline I can vouch for the ZnCl2 complex method, and it gives a clean product by 1H-NMR. Instructions can b ... |
24-11-2017 at 10:23 by: DJF90 |
Protecting weak secondary amines - driving me crazy! So you're on a forum for amateur science asking for advice/solutions to your commercial problems? Do ... |
24-11-2017 at 05:22 by: DJF90 |
Preparation of S2Cl2 [rquote=497697&tid=78027&author=aga][rquote=497692&tid=78027&author=clearly_not_atar ... |
16-11-2017 at 12:14 by: DJF90 |
Protecting weak secondary amines - driving me crazy! [rquote=497566&tid=78225&author=Sigmatropic]What I'm saying is that, based on pKa values, on ... |
15-11-2017 at 09:31 by: DJF90 |
Protecting weak secondary amines - driving me crazy! [rquote=497493&tid=78225&author=hexabio] NaH is a pretty brutal reagent just for depronating ... |
14-11-2017 at 10:47 by: DJF90 |
Protecting weak secondary amines - driving me crazy! [rquote=497430&tid=78225&author=hexabio] I have never seen NaH used in BOC protections, can ... |
14-11-2017 at 09:24 by: DJF90 |
Protecting weak secondary amines - driving me crazy! What you're referring to is not a secondary amine, but an indole. Two quite separate things.
I'd ... |
13-11-2017 at 12:36 by: DJF90 |
[UK] TLC plates needed I think you will have a hard time sourcing any that are 60 cm long, considering the standard "full-s ... |
6-11-2017 at 12:01 by: DJF90 |
Preparation of S2Cl2 Nice work Magpie. Good to see you're still busy in the lab
What was the rational for using conc su ... |
4-11-2017 at 15:25 by: DJF90 |
Vigreux and reflux column combo. Custom piece I can't think of any possible use for this. From my perspective, it is nonsensical and certainly can ... |
4-11-2017 at 09:30 by: DJF90 |
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