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Bromomethane and Formamide from DMF
That would not work. DMF can hydrolyze to formic acid and dimethylamine salt, but there is no good w ... |
15-4-2017 at 09:58
by: Crowfjord |
What in the world happened
Wow. Glad to hear you're okay. I'm not sure what happened, but it sure sounds like a run away reac ... |
8-4-2017 at 11:58
by: Crowfjord |
Ethyl acetoacetate with Mg(OEt)2 catalyst
Sometimes wet magnetic stirring doesn't work very well to remove the oxide layer. Grinding the magn ... |
8-4-2017 at 07:27
by: Crowfjord |
hofmann rearrangement on Ibuprofen?
Sounds like a good project. Have you seen [url=http://www.sciencemadness.org/talk/viewthread.php?tid ... |
11-3-2017 at 16:27
by: Crowfjord |
The Short Questions Thread (4)
Chlorine might work, but I am not sure. That's a little out of my realm of expertise. By the way, hy ... |
1-2-2017 at 18:37
by: Crowfjord |
The Short Questions Thread (4)
[rquote=473328&tid=25055&author=TheNerdyFarmer]I made some aluminum Chloride by dissolving a ... |
31-1-2017 at 19:32
by: Crowfjord |
Dimethylation of tryptamine via formaldehyde/STAB
I have heard that Tetrahedron's credibility is hit and miss, but the theory seems sound to me as far ... |
29-1-2017 at 12:30
by: Crowfjord |
Dimethylation of tryptamine via formaldehyde/STAB
Likewise, in my research into reduction of the indolene double bond, I found a paper detailing the s ... |
28-1-2017 at 10:31
by: Crowfjord |
L-tryptophan decarboxylation
An airlock is usually a bubbler with mineral oil employed as the liquid, which allows gas to escape ... |
28-1-2017 at 10:17
by: Crowfjord |
L-tryptophan decarboxylation
Hi chemgirl. Nice first post, and welcome to Sciencemadness.
It looks like you managed to get som ... |
23-1-2017 at 15:55
by: Crowfjord |
The Short Questions Thread (4)
It would yield an aldehyde, which could be oxidized to a carboxylic acid. |
12-1-2017 at 18:27
by: Crowfjord |
Nitrogen adds to Double Bond
[rquote=471139&tid=71658&author=Eddygp]
I thought Michael was reserved exclusively for en ... |
7-1-2017 at 07:42
by: Crowfjord |
Nitrogen adds to Double Bond
It's definitely a 1,4 addition and it works due to the electronic withdrawing nature of the carbonyl ... |
6-1-2017 at 18:02
by: Crowfjord |
Handy tips thread??
The older tips and tricks thread can be found [url=http://www.sciencemadness.org/talk/viewthread.php ... |
11-12-2016 at 06:06
by: Crowfjord |
acetoxy-methoxy exchange from acetylsalicylic acid? [edit]
Anisole can indeed be made from aspirin, but the way you propose wouldn't get you there. That might ... |
6-11-2016 at 13:02
by: Crowfjord |
Formaldehyde from Acetaldehyde and Formic Acid
I haven't seen anything of decent quality OTC in stores, though it might exist. I get mine from Phot ... |
1-10-2016 at 06:53
by: Crowfjord |
Formaldehyde from Acetaldehyde and Formic Acid
I see your reasoning there, but I think if a reaction proceeded between acetaldehyde and formic acid ... |
30-9-2016 at 19:21
by: Crowfjord |
Tired of reporting spam
[rquote=459387&tid=16937&author=wg48][rquote=457578&tid=16937&author=Crowfjord]Mods ... |
3-9-2016 at 19:11
by: Crowfjord |
Quick Questions Thread: No Easy Answers Edition
[quote]
Basically I am wondering if the bands refered to in spectroscopic readings are essentiall ... |
21-8-2016 at 06:55
by: Crowfjord |
Tired of reporting spam
"Trusted members" are those who have been added to a list in the forums spam removal algorithm. I th ... |
13-8-2016 at 05:26
by: Crowfjord |
Tired of reporting spam
Mods don't need to be online. If two trusted members report spam, it will be automatically deleted b ... |
12-8-2016 at 12:52
by: Crowfjord |
No More Ethyl Acetate
Same problem here. I haven't seen ethyl acetate nail polish remover in quite a while, and since Klea ... |
2-8-2016 at 14:01
by: Crowfjord |
How do you decide what you want to synthesize?
A lot of people usualy have a goal molecule in mind, and will work toward that goal through a series ... |
23-7-2016 at 09:12
by: Crowfjord |
unexpected biphasic mother liquor
I'm a little confused as to what you mean, where the ethanol and naphtha are concerned. Was the naph ... |
20-7-2016 at 10:27
by: Crowfjord |
O-alkyl eugenols and derivatives
[u][b]O-propyl eugenol (3-methoxy-4-propoxy-allylbenzene)[/b][/u]
O-propyl eugenol was prepared d ... |
19-7-2016 at 14:33
by: Crowfjord |
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